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11. 发明授权

US5254722A Process for the production of triglycerides 失效
标题翻译：甘油三酯生产工艺
公开(公告)号：US5254722A
公开(公告)日：1993-10-19
申请号：US195995
申请日：1988-05-19
申请人： Eberhard Peukert , Horst Rutzen , Gerhard Wollmann
发明人： Eberhard Peukert , Horst Rutzen , Gerhard Wollmann
IPC分类号： C07C67/03 , B01J27/232 , C07B61/00 , C07C69/18 , C07C69/30
CPC分类号： C07C67/03
摘要： A process for the production of triglycerides of C.sub.1 -C.sub.4 alkyl esters of C.sub.6 -C.sub.22 fatty acids:a) where dry sodium carbonate catalyst is dissolved in glycerol and mixed with a molar excess of preferably the methyl ester of C.sub.6 -C.sub.22 fatty acid at a temperature between about 150.degree. C. and 250.degree. C. at less than atmospheric pressure and under substantially anhydrous conditions to produce an initial reaction mixture containing the corresponding triglycerides of said fatty acids, and partially reacted glycerol with unreacted hydroxyl groups (OH values 10-40),b) thereafter, a portion of the initial reaction mixture is reacted with additional C.sub.1 -C.sub.4 alkyl ester of C.sub.6 -C.sub.22 fatty acid under conditions to achieve substantially full conversion of said unreacted hydroxyl groups (OH values of 5 or less), andc) a product containing the corresponding triglycerides of said fatty acids is separated from unreacted alkyl ester and from the sodium carbonate catalyst. Improved light colored triglyceride products are achieved and can be separated readily from the sodium carbonate catalyst by filtration.
摘要翻译：制备C 6 -C 22脂肪酸的C 1 -C 4烷基酯的甘油三酸酯的方法：a）其中将干燥的碳酸钠催化剂溶解在甘油中，并与摩尔过量的优选C6-C22脂肪酸的甲酯在温度在约150℃至250℃之间，低于大气压和基本无水条件下，以产生含有所述脂肪酸的相应甘油三酸酯和部分反应的甘油与未反应的羟基的初始反应混合物（OH值10- 40），b）此后，一部分初始反应混合物与另外的C 6 -C 22脂肪酸的C 1 -C 4烷基酯在使所述未反应的羟基基本上完全转化（OH值为5以下）的条件下反应，和c）含有所述脂肪酸的相应甘油三酯的产物与未反应的烷基酯和碳酸钠催化剂分离。实现了改进的浅色甘油三酸酯产物，并且可以通过过滤容易地与碳酸钠催化剂分离。

12. 发明授权

US4923642A Quaternary ammonium compounds, their production and use in fabric aftertreatment preparations 失效
标题翻译：季铵化合物，其生产和用于织物后处理制剂
公开(公告)号：US4923642A
公开(公告)日：1990-05-08
申请号：US121267
申请日：1987-11-16
申请人： Horst Rutzen , Horst Baumann , Bert Gruber
发明人： Horst Rutzen , Horst Baumann , Bert Gruber
IPC分类号： D06M13/46 , C07C219/06 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/463
CPC分类号： C11D1/62 , D06M13/463 , D06M2200/50
摘要： Quaternary ammonium compounds containing one or two long-chain ester or amide radicals of etherified hydroxycarboxylic acids and, for the remainder, short-chain radicals, which are liquid to pasty substances that may readily be dissolved or dispersed in water or alcohol/water mixtures. They may be used in dilute or concentrated, storable form for softening fabrics without the absorbency of the treated fabrics being adversely affected. The quaternary ammonium compounds are obtained by reaction of epoxyfatty acid esters with amines and subsequent quaternization.
摘要翻译：含有一个或两个醚化羟基羧酸的长链酯或酰胺基团的季铵化合物，以及其余的短链基团，其是易于溶解或分散在水或醇/水混合物中的液态至糊状物质。它们可以以稀释或浓缩，可储存的形式用于软化织物，而不会对被处理织物的吸收性受到不利影响。季铵化合物通过环氧脂肪酸酯与胺的反应和随后的季铵化反应获得。

13. 发明授权

US4492802A Process for manufacture of quaternary ammonium compounds 失效
标题翻译：制备季铵化合物的方法
公开(公告)号：US4492802A
公开(公告)日：1985-01-08
申请号：US369760
申请日：1982-04-19
申请人： Horst Rutzen , Peter Nikolaus , Martin Bischoff , Rudolf Lehmann
发明人： Horst Rutzen , Peter Nikolaus , Martin Bischoff , Rudolf Lehmann
IPC分类号： D06M13/46 , A01N33/12 , B01J31/02 , C07B61/00 , C07C67/00 , C07C213/00 , C07C213/04 , C07C215/40 , C07C217/50 , C07D453/02 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/463 , D06M13/47 , D06M13/477 , C07C89/02
CPC分类号： A01N33/12 , C11D1/62 , D06M13/385 , D06M13/463 , D06M2200/50
摘要： Process for the manufacture of quaternary ammonium compounds by reacting a compound having a terminal epoxide troup with a salt of a tertiary amine in the presence of a quaternary ammonium compound as catalyst.
摘要翻译：通过在季铵化合物作为催化剂存在下使具有末端环氧化物团的化合物与叔胺的盐反应来制备季铵化合物的方法。

14. 发明授权

US4421932A Manufacture of quaternary ammonium compounds 失效
标题翻译：季铵化合物的制造
公开(公告)号：US4421932A
公开(公告)日：1983-12-20
申请号：US369810
申请日：1982-04-19
申请人： Horst Rutzen , Manfred Petzold
发明人： Horst Rutzen , Manfred Petzold
IPC分类号： C09K3/16 , A01N33/12 , C07B31/00 , C07B43/04 , C07C67/00 , C07C213/00 , C07C213/04 , C07C215/40 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/385 , D06M13/46 , D06M13/463 , C07C89/00
CPC分类号： C11D1/62 , A01N33/12 , D06M13/385 , D06M13/463 , D06M2200/00 , D06M2200/50
摘要： Process for the manufacture of quaternary ammonium compounds by reacting a compound having a terminal epoxy group with a tertiary amine which is partly present as the free amine and partly present in the form of a salt, followed by the addition of sufficient acid at the end of the reaction to complete salt formation of the quaternary ammonium compound.
摘要翻译：通过使具有末端环氧基的化合物与作为游离胺部分存在并部分以盐形式存在的叔胺反应制备季铵化合物的方法，然后在末端加入足够的酸完成季铵化合物盐形成的反应。

15. 发明授权

US4179393A Stable aqueous suspension of water-insoluble, calcium-binding aluminosilicates and organic suspending agents 失效
标题翻译：稳定的水不溶性，钙结合铝硅酸盐和有机悬浮剂的水性悬浮液
公开(公告)号：US4179393A
公开(公告)日：1979-12-18
申请号：US764854
申请日：1977-02-02
申请人： Hans Andree , Dieter Jung , Martin Bischoff , Jens Conrad , Josef Huppertz , Gunter Jakobi , Peter Krings , Dieter Kuhling , Herbert Reuter , Wolfgang Rupilius , Horst Rutzen , Harald Schnegelberger
发明人： Hans Andree , Dieter Jung , Martin Bischoff , Jens Conrad , Josef Huppertz , Gunter Jakobi , Peter Krings , Dieter Kuhling , Herbert Reuter , Wolfgang Rupilius , Horst Rutzen , Harald Schnegelberger
IPC分类号： B01F17/42 , C01B39/00 , C01B39/04 , C01B39/06 , C11D1/44 , C11D3/00 , C11D3/12 , C01B33/28 , C11D1/48
CPC分类号： C11D3/1286 , C11D1/44 , Y10S516/07
摘要： Stable, pumpable, aqueous suspensions of water-insoluble, calcium-binding aluminosilicates suitable as stock suspensions comprising (A) from 20% to 55% by weight of at least one finely-divided, water-insoluble silicate compound having a calcium-binding power of at least 50 mg CaO/gm of anhydrous active substance and having the formula, combined water not shown(M.sub.2/n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is aluminum or boron, and y is a number from 0.8 to 6, (B) from 0.2% to 5% by weight of at least one organic dispersing agent as follows:(1) lower alkylene oxide or glycide adducts of an N-higher alkyl/alkenyl-alkylenediamine,(2) lower alkylene oxide or glycide adducts of the reaction product of .epsilon.-caprolactam with an N-mono- or di-higher alkyl/alkenyl-alkylenediamine,(3) ethylene or propylene oxide adducts of long chain vicinal aminoalkanols,(4) the reaction product of ethylene glycol and a higher epoxyalkane and ethylene oxide adducts thereof.
摘要翻译：稳定的，可泵送的水不溶性钙结合铝硅酸盐的水性悬浮液，其适合作为原料悬浮液，其包含（A）20重量％至55重量％的至少一种具有钙结合力的细分的水不溶性硅酸盐化合物至少50mg CaO / gm的无水活性物质，并具有下式，组合水未示出（M2 / nO）x。 Me2O3。（SiO 2）y其中M是价数为n的阳离子，可与钙交换，x为0.7至1.5的数，Me为铝或硼，y为0.8至6的数，（B）为0.2％至5重量％的至少一种有机分散剂如下：（1）N-高级烷基/烯基 - 亚烷基二胺的较低的环氧烷或缩水甘油加成物，（2）ε的反应产物的低级环氧烷或缩水甘油基加成物（3）长链连位氨基链烷醇的乙烯或环氧丙烷加成物，（4）乙二醇与较高环氧烷烃的环氧乙烷加成物的反应产物。

16. 发明授权

US4832856A Aqueous fabric softener for the treatment of fabrics: containing alkylamine, hydroxyalkylamine or quaternary ammonium derivative and a carboxylic acid 失效
标题翻译：用于处理织物的水性织物柔软剂：含有烷基胺，羟烷基胺或季铵衍生物和羧酸
公开(公告)号：US4832856A
公开(公告)日：1989-05-23
申请号：US166360
申请日：1988-03-10
申请人： Horst Rutzen , Eric Sung
发明人： Horst Rutzen , Eric Sung
IPC分类号： D06M13/46 , C11D1/04 , C11D1/40 , C11D1/62 , C11D1/65 , C11D3/00 , C11D3/20 , C11D3/30 , D06M13/02 , D06M13/184 , D06M13/203 , D06M13/322 , D06M13/325 , D06M13/463
CPC分类号： C11D3/30 , C11D1/40 , C11D1/65 , C11D3/0015 , C11D3/2075 , C11D1/04 , C11D1/62
摘要： Fabric softeners intended for the treatment of fabrics after washing are disclosed. These softeners contain as active substance a combination of carboxylic acids and amines and/or quaternary ammonium compounds containing a long chain alkyl or alkenyl radical and comprise:(a) one or more amines corresponding to general formulae (I) and/or (II) below: ##STR1## in which: R.sup.1 and R.sup.2 may be the same or different and, independently of one another, represent hydrogen, straight-chain or branched C.sub.1 -C.sub.20 alkyl radicals, in addition to which R.sup.2 may represent a hydroxy group or a group corresponding to the following formula: ##STR2## where: R.sup.5 is hydrogen or a straight-chain or branched C.sub.1 -C.sub.6 alkyl radical; andR.sup.3 and R.sup.4 may be the same or different and, independently of one another, represent hydrogen, staight-chain or branched C.sub.1 -C.sub.6 alkyl radicals or hydroxyalkyl radicals containing from 1 to 6 carbon atoms in the straight-chain alkyl radical; andp and q are numbers of from 0 to 22, the sum (p+q) being in the range of 0 to 22; and/or one or more ammonium compounds derived from such amines by quaternization;(b) one or more straight-chain or branched, saturated or unsaturated C.sub.1 14 C.sub.24 carboxylic acids; and(c) optionally, other substances typically used in fabric softeners.This active-substance combination is readily and inexpensively available and provides the treated fabrics with a soft, full feel.
摘要翻译：公开了用于洗涤后织物处理的织物柔软剂。这些软化剂含有作为活性物质的羧酸和胺和/或含有长链烷基或烯基的季铵化合物的组合，并包含：（a）一种或多种对应于通式（I）和/或（II）的胺，（I）R1R3R4N（Ⅱ）其中：R1和R2可以相同或不同，并且彼此独立地表示氢，直链或支链C1-C20烷基，除此之外，R2 可以表示对应于下式的羟基或基团：其中：R 5是氢或直链或支链C 1 -C 6烷基; 并且R 3和R 4可以相同或不同，并且彼此独立地表示在直链烷基中含有1至6个碳原子的氢，直链或支链C 1 -C 6烷基或羟烷基; p和q为0〜22的数，和（p + q）为0〜22的范围。和/或一种或多种通过季铵化衍生自这些胺的铵化合物; （b）一种或多种直链或支链，饱和或不饱和C114C24羧酸; 和（c）任选地，通常用于织物柔软剂中的其它物质。这种活性物质的组合是容易和廉价的可用的，并且使经处理的织物具有柔软的，充分的感觉。

17. 发明授权

US4829142A Aminofatty acid amides from the reaction of an epoxidized fatty acid ester width a polyfunctional amine, and use as a crosslinking agent 失效
标题翻译：来自环氧化脂肪酸酯宽度为多官能胺反应的氨基酸酰胺，并用作交联剂
公开(公告)号：US4829142A
公开(公告)日：1989-05-09
申请号：US86469
申请日：1987-08-18
申请人： Rene A. A. Gonzalez , Manfred Budnowski , Julius Herold , Horst Rutzen , Eberhard Schneider , Hans-Guenter Seltmann
发明人： Rene A. A. Gonzalez , Manfred Budnowski , Julius Herold , Horst Rutzen , Eberhard Schneider , Hans-Guenter Seltmann
IPC分类号： C08G59/54 , C08G59/64 , C09J163/00
CPC分类号： C08G59/54 , C08G59/64
摘要： Aminohydroxy fatty acid amides obtained by condensation from epoxidized fatty acid alkyl esters and polyfunctional aliphatic oligoamines may be employed as crosslinking agents for polyfunctional epoxide compounds used as adhesives and/or coating compositions.The preferred crosslinking agent represents the reaction product of(1) epoxidized stearic acid methyl ester and(2) ethylene diamine or diethylene triamine, and has the following formula: ##STR1##
摘要翻译：可以使用由环氧化脂肪酸烷基酯和多官能脂族低聚胺缩合得到的氨基羟基脂肪酸酰胺作为用作粘合剂和/或涂料组合物的多官能环氧化合物的交联剂。优选的交联剂代表（1）环氧化硬脂酸甲酯和（2）乙二胺或二亚乙基三胺的反应产物，具有下式： + TR

18. 发明授权

US4820507A Oral and dental hygiene preparations 失效
标题翻译：口腔和牙科卫生制剂
公开(公告)号：US4820507A
公开(公告)日：1989-04-11
申请号：US18762
申请日：1987-03-02
申请人： Hans-Juergen Klueppel , Walter Ploeger , Horst Rutzen , Rudolf Lehmann
发明人： Hans-Juergen Klueppel , Walter Ploeger , Horst Rutzen , Rudolf Lehmann
IPC分类号： A61K8/40 , A61K8/25 , A61K8/26 , A61K8/41 , A61K8/55 , A61Q11/00 , A61K7/22 , A61K7/16 , A61K7/24
CPC分类号： A61K8/416 , A61K8/55 , A61Q11/00 , Y10S514/835 , Y10S514/90 , Y10S514/901
摘要： Oral and dental hygiene preparations containing quaternary ammonium compounds of the formula ##STR1## wherein R.sup.1 is an n-alkyl group, preferably containing from 8 to 12 carbon atoms, R.sup.2 is hydrogen, a CH.sub.3 -group or a CH.sub.2 OH-group and R.sup.3 is a CH.sub.3 -group or a group of the formula --CH.sub.2 --CH(OH)--R.sup.2, A is an inorganic or organic acid anion and n is the basicity of the anion. The quaternary ammonium compounds of formula I can have a plaque inhibiting effect and show only slight antimicrobial activity. R.sup.1 is preferably an n-decyl group, R.sup.2 is hydrogen and R.sup.3 is a CH.sub.3 -group or a 2-hydroxyethyl group. The oral and dent al hygiene preparations also preferably contain fluorides and/or organophosphonates as the anion A.
摘要翻译：含有式（I）的季铵化合物的口腔和牙科卫生制剂，其中R 1是正烷基，优选含有8至12个碳原子，R 2是氢，CH 3 - 基或CH 2 OH基，和 R3是CH3-基团或式-CH2-CH（OH）-R2的基团，A是无机或有机酸阴离子，n是阴离子的碱性。式I的季铵化合物可以具有抑制斑块的作用并且仅显示轻微的抗微生物活性。 R 1优选为正癸基，R 2为氢，R 3为CH 3 - 基或2-羟基乙基。口服和牙齿卫生制剂还优选含有作为阴离子A的氟化物和/或有机膦酸盐。

19. 发明授权

US4744977A Quaternary ammonium compound hair conditioners 失效
标题翻译：季铵化合物头发调理剂
公开(公告)号：US4744977A
公开(公告)日：1988-05-17
申请号：US798201
申请日：1985-11-14
申请人： Hermann Hensen , Horst Rutzen , Peter Busch , Dagmar Stuhrmann , Klaus Thiele
发明人： Hermann Hensen , Horst Rutzen , Peter Busch , Dagmar Stuhrmann , Klaus Thiele
IPC分类号： A61K8/00 , A61K8/40 , A61K8/41 , A61K8/46 , A61Q5/00 , A61Q5/02 , A61Q5/12 , A61K7/06 , A61K7/08 , A61K7/11
CPC分类号： A61Q5/02 , A61K8/416 , A61Q5/12 , Y10S424/01 , Y10S424/02 , Y10S424/04 , Y10S514/88 , Y10S514/881 , Y10S514/904
摘要： A hair care preparation containing a hair conditioning effective amount of a compound of the formula: ##STR1## wherein: R.sup.1 is a C.sub.12-16 -n-alkyl;R.sup.2 is a C.sub.1-4 -n-alkyl;is a C.sub.1-4 -hydroxyalkyl;R.sup.4 is a C.sub.1-4 -n-alkyl or a C.sub.2-4 -hydroxyalkyl;A is an inorganic or organic acid anion; andn is the valence of said anion.
摘要翻译：一种含有头发调理有效量的下式化合物的护发制剂：其中：R1是C12-16-正烷基; R2是C1-4-正烷基; 是C 1-4 - 羟基烷基; R4是C1-4-正烷基或C2-4-羟基烷基; A是无机或有机酸阴离子; 并且n是所述阴离子的化合价。

20. 发明授权

US4264480A Stable aqueous suspension of water-insoluble, calcium-binding aluminosilicates and organic suspending agents 失效
标题翻译：稳定的水不溶性，钙结合铝硅酸盐和有机悬浮剂的水性悬浮液
公开(公告)号：US4264480A
公开(公告)日：1981-04-28
申请号：US052798
申请日：1979-06-28
申请人： Hans Andree , Dieter Jung , Martin Bischoff , Jens Conrad , Josef Huppertz , Gunter Jakobi , Peter Krings , Dieter Kuhling , Herbert Reuter , Wolfgang Rupilius , Horst Rutzen , Harald Schnegelberger
发明人： Hans Andree , Dieter Jung , Martin Bischoff , Jens Conrad , Josef Huppertz , Gunter Jakobi , Peter Krings , Dieter Kuhling , Herbert Reuter , Wolfgang Rupilius , Horst Rutzen , Harald Schnegelberger
IPC分类号： B01F17/42 , C01B39/00 , C01B39/04 , C01B39/06 , C11D1/44 , C11D3/00 , C11D3/12 , C11D1/66 , C11D17/08
CPC分类号： C11D3/1286 , C11D1/44 , Y10S516/07
摘要： Stable, pumpable, aqueous suspensions of water-insoluble, calcium-binding aluminosilicates suitable as stock suspensions comprising (A) from 20% to 55% by weight of at least one finely-divided, water-insoluble silicate compound having a calcium-binding power of at least 50 mg CaO/gm of anhydrous active substance and having the formula, combined water not shown(M.sub.2/n O).sub.x.Me.sub.2 O.sub.3.(SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is aluminum or boron, and y is a number from 0.8 to 6, (B) from 0.2% to 5% by weight of at least one organic dispersing agent as follows:lower alkylene oxide or glycide adducts of the reaction product of .epsilon.-caprolactam with an N-mono- or di-higher alkyl/alkenyl-alkylenediamine.
摘要翻译：稳定的，可泵送的水不溶性钙结合铝硅酸盐的水性悬浮液，其适合作为原料悬浮液，其包含（A）20重量％至55重量％的至少一种具有钙结合力的细分的水不溶性硅酸盐化合物至少50mg CaO / gm的无水活性物质，具有下式：组合水未显示（M2 / nO）x.Me2O3。（SiO2）y，其中M是价数为n的阳离子，可与钙交换，x为数量为0.7〜1.5，Me为铝或硼，y为0.8〜6，（B）0.2〜5重量％的至少一种有机分散剂，如下所示：低级环氧烷或缩水甘油基 ε-己内酰胺与N-单 - 或二 - 高级烷基/烯基 - 亚烷基二胺的反应产物的加合物。

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