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11. 发明授权

US4358431A Production of magnetic iron oxides 失效
标题翻译：生产磁性氧化铁
公开(公告)号：US4358431A
公开(公告)日：1982-11-09
申请号：US286134
申请日：1981-07-23
申请人： Horst Brunn , Peter Kiemle , Franz Hund , Heribert Bade
发明人： Horst Brunn , Peter Kiemle , Franz Hund , Heribert Bade
IPC分类号： C01G49/02 , C01G49/06 , G11B5/706 , H01F1/10 , H01F1/11 , C01G49/08
CPC分类号： G11B5/70642 , C01G49/06 , C01P2004/03 , C01P2004/10 , C01P2004/61 , C01P2006/42
摘要： In the production of needle-shaped magnetic iron oxide pigments by treating iron with a nitro-aromatic in the presence of .alpha.-FeOOH nuclei to form .alpha.-FeOOH particles and an amino-aromatic, and thereafter dehydrating the .alpha.-FeOOH particles and reducing them, the improvement which comprises forming the .alpha.-FeOOH nuclei at about 0.degree. to 90.degree. C. in a suspension of metallic iron, an iron-(II)-salt and a nitro-aromatic by adding a basic precipitant in about 10 to 95% of the amount required for the complete precipitation of the iron in the iron-(II)-salt. Advantageously the metallic iron comprises cast iron, the nitro-aromatic comprises nitrobenzene, the amino-aromatic comprises aniline, the basic precipitant comprises at least one of ammonia and a basically reacting alkali metal, alkaline earth metal or ammonium salt, the nuclei formation is carried out at about 10.degree. to 60.degree. C., and the basic precipitant is added in about 20 to 80% of the amount required for the complete precipitation of the iron in the iron-(II)-salt, additional iron and nitrobenzene being added to the suspension of precipitated nuclei to form the .alpha.-FeOOH particles.
摘要翻译：在通过在α-FeOOH核的存在下用硝基芳族化合物处理铁以形成α-FeOOH颗粒和氨基芳族化合物来生产针状磁性氧化铁颜料，然后使α-FeOOH颗粒脱水并还原包括在金属铁，铁 - （II） - 盐和硝基 - 芳族化合物的悬浮液中在约0至90℃下形成α-FeOOH核的改进，通过在约10至95 在铁 - （II） - 铁中完全沉淀铁所需的量的％。有利地，金属铁包括铸铁，硝基芳族包括硝基苯，氨基 - 芳族包括苯胺，碱性沉淀剂包括氨和基本上反应的碱金属，碱土金属或铵盐中的至少一种，承载核形成在约10℃至60℃下加入碱性沉淀剂，其中添加铁（II） - 铁中完全沉淀所需的量的约20至80％，添加额外的铁和硝基苯到析出的核的悬浮液以形成α-FeOOH颗粒。

12. 发明授权

US4156613A Anti-corrosion pigments 失效
标题翻译：防腐颜料
公开(公告)号：US4156613A
公开(公告)日：1979-05-29
申请号：US796505
申请日：1977-05-12
申请人： Franz Hund , Gunter Linde , Peter Kresse
发明人： Franz Hund , Gunter Linde , Peter Kresse
IPC分类号： C01G45/00 , C09C1/00 , C09C1/02 , C09C1/04 , C09C1/22 , C09C1/40 , C09D5/08
CPC分类号： C09D5/084 , C09C1/00 , C09C1/02 , C09C1/04 , C09C1/22 , C09C1/40 , C01P2002/52
摘要： A pigment of high anti-corrosion properties comprises(a) about 30 to 70 mole percent of at least one of MgO, ZnO and CaO, and(b) about 70 to 30 mole percent of Me.sub.2 O.sub.3 wherein Me.sub.2 O.sub.3 has the approximate molar percent compositionFe.sub.2 O.sub.3 : 0-100, preferably 0.5-100, most preferably 1-95, mole %Al.sub.2 O.sub.3 +Mn.sub.2 O.sub.3 : 0-100, preferably 0.5-100, most preferably 1-95, mole %Cr.sub.2 O.sub.3 : 0-20 mole %Is produced by calcining such oxides or compounds yielding such oxides at from about 200.degree. .RTM. to 650.degree. C. with the option of going up to about 950.degree. C. if the Al+Mn+Cr oxides total 10 mole % or more.
摘要翻译：具有高抗腐蚀性能的颜料包括（A）MgO，ZnO和CaO的至少30-70摩尔％，和（B）约70至30摩尔％的Me 2 O 3，其中Me 2 O 3具有近似的摩尔百分数组成Fe 2 O 3 ：0-100，优选0.5-100，最优选1-95摩尔％Al2O3 + Mn2O3：0-100，优选0.5-100，最优选1-95摩尔％Cr2O3：0-20摩尔％通过计算生产如果Al + Mn + Cr氧化物总量为10摩尔％以上，则这种氧化物或化合物在大约200℃至650℃之间的这种氧化物可以选择高达约950℃。

13. 发明授权

US4153465A CaZn.sub.2 (PO.sub.4).sub.2 .2H.sub.2 O anticorrosion pigment 失效
标题翻译： CaZn {hd 2 {b（PO {HD 4 {B）{HD 2 {B.2H {HD 2 {B O防腐颜料
公开(公告)号：US4153465A
公开(公告)日：1979-05-08
申请号：US855482
申请日：1977-11-28
申请人： Franz Hund , Peter Kresse
发明人： Franz Hund , Peter Kresse
IPC分类号： C09C1/00 , C01B25/45 , C09C1/04 , C09D5/08
CPC分类号： C01B25/45 , C09C1/046 , C09D5/084 , C01P2002/30 , C01P2006/12
摘要： An anticorrosion pigment suited for paints and lacquers and consisting of CaZn.sub.2 (PO.sub.4).sub.2 . 2H.sub.2 O crystallizing in the Scholzite lattice and having a specific surface according to BET of from 0.1 to 50 m.sup.2 /g is produced by a process wherein(a) (i) a salt solution containing calcium and zinc cations in a ratio of about 1:2 is normally, inversely or simultaneously precipitated in air at temperatures of up to about 100.degree. C. with an equivalent or substantially equivalent quantity of a solution containing an alkali metal or ammonium phosphate ion; or (ii) compounds of calcium and zinc, which can be decomposed with relatively strong acids or neutralized with acids, in a ratio of about 1:2, have phosphoric acid or ammonium phosphate added to them in approximately the quantity which is required for decomposition or neutralization, or in a slight excess of that quantity, at temperatures of up to about 100.degree. C.; and(b) the suspension obtained in accordance with (a) (i) or (ii) is heated in air to a temperature of up to about 100.degree. C. or in an autoclave to a temperature of up to about 175.degree. C. over a period of up to about 10 hours, e.g. about 1 to 8 hours, the pigment suspension obtained is washed, filtered off and dried.
摘要翻译：一种适用于油漆和漆的防腐颜料，由CaZn2（PO4）2组成。通过其中（A）（I）含有约1：2比例的钙和锌溶液的盐溶液的方法制备了在Scholzite晶格中结晶并具有0.1至50m 2 / g的BET比表面积的2H 2 O 2 在相当于或基本上相当量的含有碱金属或磷酸铵离子的溶液的情况下，正常地，相反地或同时地在空气中降解高达约100℃的温度。或（ii）钙和锌的化合物，其可用相对较强的酸分解或用酸中和，以约1:2的比例分解，其中添加了大约为分解所需量的磷酸或磷酸铵或中和，或略高于该量，在高达约100℃的温度下

14. 发明授权

US4378252A Magnetic separation to improve purity of iron oxide pigments 失效
标题翻译：磁选分离提高氧化铁颜料的纯度
公开(公告)号：US4378252A
公开(公告)日：1983-03-29
申请号：US268291
申请日：1981-05-29
申请人： Peter Kiemle , Franz Hund , Ingo Pflugmacher , Wolfgang Rambold
发明人： Peter Kiemle , Franz Hund , Ingo Pflugmacher , Wolfgang Rambold
IPC分类号： C09C1/00 , B03C1/00 , C01B13/16 , C01G49/06 , C09C1/22 , C09C1/24 , C09C3/04
CPC分类号： C01G49/06 , B03C1/00 , C01B13/16 , C09C1/24 , C09C3/04 , C01P2006/60 , C01P2006/62 , C01P2006/65
摘要： A process for increasing the color purity of iron oxide pigment particles admixed with color-modifying impurities and obtained by the Penniman process or the aniline process, comprising introducing the particles into a magnetic field, and removing from the magnetic field two fractions of different magnetizability, the first fraction being iron oxide pigment particles of increased color purity and the second fraction being enriched in impurities.
摘要翻译：一种用于提高与改色杂质混合并通过Penniman方法或苯胺方法获得的氧化铁颜料颗粒的颜色纯度的方法，包括将颗粒引入磁场，并从磁场中除去两种不同磁化性的部分，第一部分是增加色纯度的氧化铁颜料颗粒，第二部分富含杂质。

15. 发明授权

US4140538A Iron oxide-based anti-corrosion pigments 失效
标题翻译：氧化铁基防腐颜料
公开(公告)号：US4140538A
公开(公告)日：1979-02-20
申请号：US713480
申请日：1976-08-11
申请人： Franz Hund , Gunter Linde , Peter Kresse
发明人： Franz Hund , Gunter Linde , Peter Kresse
IPC分类号： C09C1/00 , C09C1/02 , C09C1/04 , C09C1/22 , C09C1/24 , C09C1/34 , C04B31/02
CPC分类号： C09C1/24 , C09C1/34 , C01P2004/82 , C01P2006/12
摘要： An anti-corrosion pigment comprising about 30 to 70 mole % of an oxide of at least one metal selected from the group consisting of magnesium, calcium and zinc, about 70 to 30 mole % of Fe.sub.2 O.sub.3, and up to about 20 mole % of Cr.sub.2 O.sub.3, the pigment having a specific surface of about 1 to 30 m.sup.2 /g and exhibiting a weight loss of less than about 0.05% per gram of pigment by the Thomson corrosion test, is produced by calcining the corresponding metal oxides. The temperature is about 200 to 650.degree. C. in the absence of chromium and about 200 to 900.degree. C. when chromium is present.
摘要翻译：一种抗蚀颜料，其包含约30至70摩尔％的选自镁，钙和锌的至少一种金属的氧化物，约70至30摩尔％的Fe 2 O 3，以及至多约20摩尔％的Cr 2 O 3 通过汤姆森腐蚀试验，通过煅烧相应的金属氧化物来制造具有约1至30m 2 / g的比表面积并且通过Thomson腐蚀试验显示小于约0.05％的每克颜料的重量损失的颜料。不存在铬时，温度约为200〜650℃，铬存在时温度约为200〜900℃。

16. 发明授权

US4036662A Metal additions to pigments of pseudobrookite-titanium dioxide structure 失效
标题翻译：金属添加剂对假木炭素 - 二氧化钛结构的颜料
公开(公告)号：US4036662A
公开(公告)日：1977-07-19
申请号：US624214
申请日：1975-10-20
申请人： Jacob Rademachers , Henning Erfurth , Franz Hund
发明人： Jacob Rademachers , Henning Erfurth , Franz Hund
IPC分类号： C03C1/04 , C04B14/36 , C08K3/24 , C09C1/36 , C01G23/00 , C01G49/00 , C09C1/22
CPC分类号： C03C1/04 , C04B14/36 , C08K3/24 , C09C1/36 , C01P2002/30 , C01P2002/52
摘要： In the production of temperature-stable inorganic pigment of pseudobrookite-titanium dioxide structure having the composition Fe.sub.2 TiO.sub.5.sup.. x TiO.sub.2, wherein x is from 0 to about 15, by preparing a suspension of finely divided titanium dioxide or titanium dioxide hydrate and at least one of finely divided iron oxide, iron oxide hydroxide, iron hydroxide and iron carbonate, removing the aqueous phase of the suspension from a solid residue and calcining the residue at a temperature in the range of about 600.degree. to 1100.degree.C, the improvement which comprises including in the suspension or in the solid residue at least one compound of a metal selected from the group consisting of lithium, sodium, potassium, magnesium, zinc, calcium, aluminum, copper, vanadium, chromium, manganese, cobalt and nickel, the compound being present in a quantity to provide about 0.1 to 10 % by weight of metal based on the pigment. With the addition of compounds of lithium, sodium, potassium, magnesium, zinc, calcium or aluminum even in small amounts a much purer yellow color results.
摘要翻译：在通过制备细碎二氧化钛或二氧化钛水合物和至少之一中的至少一种制备具有组成为Fe2TiO5.x TiO2（其中x为0至约15）的假构铁矿 - 二氧化钛结构的温度稳定无机颜料细碎的氧化铁，氧化铁氢氧化物，氢氧化铁和碳酸铁，从固体残渣中除去悬浮液的水相，并在约600℃至1100℃的温度下煅烧残渣，其改进包括在悬浮液或固体残余物中，选自锂，钠，钾，镁，锌，钙，铝，铜，钒，铬，锰，钴和镍中的至少一种金属化合物，所述化合物为存在的量为基于颜料提供约0.1至10重量％的金属。即使少量添加锂，钠，钾，镁，锌，钙或铝的化合物，也会产生更纯净的黄色。

17. 发明授权

US4492600A Corrosion-inhibiting paints and lacquers 失效
标题翻译：防腐涂料和漆
公开(公告)号：US4492600A
公开(公告)日：1985-01-08
申请号：US398226
申请日：1982-07-14
申请人： Horst Brunn , Franz Hund , Wolfgang Rambold , Peter Kresse , Gerd von Szadkowski
发明人： Horst Brunn , Franz Hund , Wolfgang Rambold , Peter Kresse , Gerd von Szadkowski
IPC分类号： C09C3/00 , C09C1/00 , C09C3/08 , C09D5/08 , C04B9/02
CPC分类号： C09D5/082 , C09C1/00 , C01P2002/08 , C01P2004/84 , C01P2006/12
摘要： This invention relates to corrosion-inhibiting paints and lacquers containing pigments comprising an organic corrosion inhibitor intercalated into an inorganic matrix said pigment having the formula wherein ##EQU1## wherein Me(II)O is at least one divalent metal oxide;Me(III).sub.2 O.sub.3 is at least one trivalent metal oxide;A is at least one inorganic acid anhydride;I is at least one organic corrosion inhibitor;aq is from 0.5 to 9 moles of water; andx, y and z are whole or fractional numbers andx has a value of from 0 to 1,y has a value of from 0 to 0.7 andz has a value of from greater than 0 to 0.4,with the proviso that the organic corrosion inhibitor is at least 0.5% by weight of inorganic material a process for the production of these pigments and their use in paints, lacquers and lubricants.
摘要翻译：本发明涉及含有颜料的防腐涂料和含有颜料的漆，所述颜料包括插入无机基质中的有机腐蚀抑制剂，所述颜料具有下式：其中Me（II）O为至少一种二价金属氧化物; Me（III）2 O 3是至少一种三价金属氧化物; A是至少一种无机酸酐; 我至少有一种有机腐蚀抑制剂; 水溶液为0.5至9摩尔水; 并且x，y和z是整数或分数，x具有0至1的值，y具有0至0.7的值，z具有大于0至0.4的值，条件是有机防腐剂为无机材料的至少0.5重量％，用于生产这些颜料的方法及其在油漆，漆和润滑剂中的应用。

18. 发明授权

US3974079A Production of gamma iron oxide 失效
标题翻译：生产γ氧化铁
公开(公告)号：US3974079A
公开(公告)日：1976-08-10
申请号：US412488
申请日：1973-11-02
申请人： Peter Woditsch , Kurt Hill , Franz Hund , Fritz Rodi
发明人： Peter Woditsch , Kurt Hill , Franz Hund , Fritz Rodi
IPC分类号： C01G49/06 , C09C1/24 , G11B5/706 , H01F1/113
CPC分类号： H01F1/113 , C01G49/06 , C09C1/24 , G11B5/70647 , G11B5/70652 , G11B5/70663 , C01P2004/10 , C01P2004/54 , C01P2004/62 , C01P2006/42 , C01P2006/80
摘要： Process for producing ferromagnetic iron oxides whereby a solution of a ferrous salt is oxidized in the presence of .alpha.-FeO(OH) seed, a basic precipitant, and phosphoric acid or a water soluble salt thereof to form .alpha.-FeO(OH), which can be dehydrated, optionally tempered, reduced and re-oxidized to needle-shaped .gamma.-Fe.sub.2 O.sub.3. The resulting product has high coercive force values which make it especially useful for magnetic impulse recording and reproduction.
摘要翻译：制备铁磁性氧化铁的方法，其中亚铁盐溶液在α-FeO（OH）种子，碱性沉淀剂和磷酸或其水溶性盐的存在下被氧化以形成α-FeO（OH），其中可以脱水，任选回火，还原和再氧化成针状γ-Fe2O3。所得到的产品具有高的矫顽力值，使其对于磁脉冲记录和再现特别有用。

19. 发明授权

US3947502A Production of finely divided acicular magnetic iron oxides 失效
标题翻译：精细分散的针状磁性氧化铁的生产
公开(公告)号：US3947502A
公开(公告)日：1976-03-30
申请号：US322819
申请日：1973-01-11
申请人： Lutz Leitner , Franz Hund
发明人： Lutz Leitner , Franz Hund
IPC分类号： C01G49/06 , G11B5/706 , H01F1/11 , C01G49/02
CPC分类号： G11B5/70663 , C01G49/06 , G11B5/70642 , G11B5/70657 , C01P2004/10 , C01P2006/42 , C01P2006/80
摘要： In the production of acicular, ferromagnetic iron oxide of high coercive force by oxidizing an iron (II)-hydroxide suspension with an oxygen-containing gas to form acicular iron (III) oxide hydroxide and dehydrating the iron (III) oxide hydroxide, optionally tempering, reducing and/or reoxidizing this into magnetic iron oxide, the improvement which comprises effecting the oxidation of the iron (II)-hydroxide suspension at a pH of at least about 13, the suspension including SiO.sub.2 in the form of a sol or soluble salt, the resulting iron (III) oxide hydroxide having SiO.sub.2 deposited thereon.
摘要翻译：在通过用含氧气体氧化铁（II） - 氢氧化物悬浮液以形成氧化氢氧化物的针状铁（III）和使氧化氢（III）氢氧化物脱水，生产具有高矫顽力的铁磁性氧化铁，任选回火，将其还原和/或再氧化成磁性氧化铁，其改进包括在至少约13的pH下进行铁（II） - 氢氧化物悬浮液的氧化，所述悬浮液包括溶胶或可溶性盐形式的SiO 2 ，所得到的沉积有SiO 2的氧化铁（III）氢氧化物具有SiO 2。

20. 发明授权

US4443264A Halogen-free zinc ferrite yellow pigments containing alumina and phosphorus oxide and production 失效
标题翻译：无卤锌铁氧体黄色颜料含氧化铝和氧化磷并生产
公开(公告)号：US4443264A
公开(公告)日：1984-04-17
申请号：US413002
申请日：1982-08-30
申请人： Franz Hund , Willi Hennings , Horst Brunn , Peter Kresse , Wolfgang Rambold
发明人： Franz Hund , Willi Hennings , Horst Brunn , Peter Kresse , Wolfgang Rambold
IPC分类号： C08K9/00 , C01B25/37 , C01G49/00 , C08K3/10 , C09C1/00 , C09C1/22 , C09C1/24 , C09C1/40 , C09D7/00 , C09D7/12 , C04B31/02
CPC分类号： C08K3/10 , C09C1/22 , C09C1/40 , C01P2002/08 , C01P2006/60
摘要： A zinc ferrite pigment comprising, by weight, about 99.8 to 90% of ZnFe.sub.2 O.sub.4 and about 0.2 to 10% of the component system (1-x)Al.sub.2 O.sub.3 and xP.sub.2 O.sub.5 wherein 0
摘要翻译：一种锌铁氧体颜料，其包含按重量计约99.8至90％的ZnFe 2 O 4和约0.2至10％的组分体系（1-x）Al 2 O 3和xP 2 O 5，其中0

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