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11. 发明授权

US4644021A Sustained release antimicrobial agents and methods of fouling control using the same 失效
标题翻译：持续释放的抗微生物剂和使用其的污染控制方法
公开(公告)号：US4644021A
公开(公告)日：1987-02-17
申请号：US766845
申请日：1985-08-16
申请人： Fumio Toda , Masaru Okamoto , Fujiaki Mochizuki
发明人： Fumio Toda , Masaru Okamoto , Fujiaki Mochizuki
IPC分类号： A01N25/00 , A01N25/08 , A01N25/18 , A01N25/22 , A01N25/32 , A01N33/20 , A01N33/26 , A01N35/06 , A01N37/48 , A01N43/80 , A01N47/40 , A01N59/00 , C01B21/16 , C07C27/00 , C07C33/28 , C07C67/00 , C09D5/16 , C09D5/14 , C02F1/68
CPC分类号： C09D5/1625 , A01N25/08 , A01N33/20 , A01N33/26 , A01N35/06 , A01N37/48 , A01N43/80 , A01N47/40
摘要： Sustained release antimicrobial agents comprising a clathrate compound composed of a water-soluble antimicrobial agent, and 1,1,6,6-tetraphenyl-2,4-hexadiyne-1,6-diol or 1,1-di(2,4-dimethylphenyl)-2-propyne-1-ol, and methods of fouling control using the same.
摘要翻译：包含由水溶性抗微生物剂组成的包合物和1,1,6,6-四苯基-2,4-己二炔-1,6-二醇或1,1-二（2,4-二氯苯基）二甲基苯基）-2-丙炔-1-醇，以及使用其进行污染控制的方法。

12. 发明授权

US5091400A Clathrate compound 失效
标题翻译：复合化合物
公开(公告)号：US5091400A
公开(公告)日：1992-02-25
申请号：US563945
申请日：1990-08-07
申请人： Minoru Yagi , Fumio Toda
发明人： Minoru Yagi , Fumio Toda
IPC分类号： A01N25/22 , A01N43/80 , C07C29/40 , C07C33/26
CPC分类号： C07C33/26
摘要： 2,2'-Bis(.alpha.-hydroxydiphenylemthyl)biphenyl of formula: ##STR1## Clathrate compound is composed of the above compound as the host compound and a microbicide, 5-chloro-2-methyl-4-isothiazolin-3-one as the guest compound. The compound is formed such that, where diphenic acid is reacted with an alcohol for diesterification and then reacted with a Grignard reagent comprising a phenylmagnesium halide.

13. 发明授权

US5043495A Process of separation and purification of a propargyl alcohols 失效
标题翻译：炔丙醇的分离和纯化方法
公开(公告)号：US5043495A
公开(公告)日：1991-08-27
申请号：US475892
申请日：1990-01-30
申请人： Fumio Toda , Koichi Tanaka , Kikuo Ataka
发明人： Fumio Toda , Koichi Tanaka , Kikuo Ataka
IPC分类号： C07C29/88 , C07B57/00 , C07C27/00 , C07C29/76 , C07C33/30 , C07C33/48 , C07C67/00 , C07D295/02 , C07D295/03 , C07D487/04
CPC分类号： C07D295/03 , C07C29/76 , C07C33/48 , C07D487/04 , C07B2200/07
摘要： A process of separation and purification of a propargyl alcohol which comprises treating a propargyl alcohol represented by Formula (I): ##STR1## wherein each of R.sub.1 and R.sub.2 represents a substituent which is different from each other, and is selected from the group consisting of a C.sub.1 -C.sub.8 alkyl group, a phenyl group; a halophenyl group, a phenyl group having at least one methyl substituent, an aralkyl group and a cycloalkyl group,which is chemically or optically impure,with a tertiary diamine represented by Formula (II): ##STR2## wherein each of R.sub.3, R.sub.4, R.sub.5 and R.sub.6 may be the same or different and represents an aralkyl group or an alkyl group having 1 to 6 carbon atoms; and R.sub.3, R.sub.4, R.sub.5 and R.sub.6 may be bonded to each other,to form a crystalline complex compound of the propargyl alcohol represented by Formula (I) and the tertiary diamine represented by Formula (II), separating and purifying the resulting compound, and treating the resultant compound with an acid to isolate the propargyl alcohol represented by Formula (I).

14. 发明授权

US4918190A Crystalline complex compounds of propargyl alcohols and tertiary diamines, and process of separation and purification of propargyl alcohols using the same 失效
标题翻译：炔丙醇和叔二胺的结晶复合化合物，以及使用其的炔丙醇的分离和纯化方法
公开(公告)号：US4918190A
公开(公告)日：1990-04-17
申请号：US79821
申请日：1987-07-30
申请人： Fumio Toda , Koichi Tanaka , Kikuo Ataka
发明人： Fumio Toda , Koichi Tanaka , Kikuo Ataka
IPC分类号： C07C29/88 , C07B57/00 , C07C27/00 , C07C29/76 , C07C33/30 , C07C33/48 , C07C67/00 , C07D295/02 , C07D295/03 , C07D487/04
CPC分类号： C07D295/03 , C07C29/76 , C07C33/48 , C07D487/04 , C07B2200/07
摘要： Disclosed are a crystalline complex compound of a propargyl alcohol represented by Formula (I): ##STR1## wherein each of R.sub.1 and R.sub.2 represents a substituent which is different from each otherand a tertiary diamine represented by Formula (II): ##STR2## wherein A represents a group having two carbon atoms as a chain member which may be branched; each of R.sub.3, R.sub.4, R.sub.5 and R.sub.6 may be the same or different and represents an aralkyl group or an alkyl group having 1 to 6 carbon atoms; and A, R.sub.3, R.sub.4, R.sub.5 and R.sub.6 may be bonded to each other,and a process of separation and purification of the propargyl alcohol using the crystalline complex compound described above.
摘要翻译：公开了由式（I）表示的炔丙醇的结晶配位化合物：其中R 1和R 2各自表示彼此不同的取代基和由式（II）表示的叔胺：（II）其中A表示具有两个碳原子的可作为支链的链状成员的基团; R 3，R 4，R 5和R 6可以相同或不同，表示芳烷基或碳原子数1〜6的烷基。并且A，R 3，R 4，R 5和R 6可以彼此键合，并且使用上述结晶复合化合物分离和纯化炔丙醇的方法。

15. 发明授权

US4780317A Sustained release antimicrobial agents and method of fouling control using the same 失效
标题翻译：持续释放抗菌剂及使用其的防污方法
公开(公告)号：US4780317A
公开(公告)日：1988-10-25
申请号：US006050
申请日：1987-01-22
申请人： Ayako Sekikawa , Hideo Sugi , Kenji Tahara , Fumio Toda
发明人： Ayako Sekikawa , Hideo Sugi , Kenji Tahara , Fumio Toda
IPC分类号： A01N25/22 , A01N25/12 , A01N43/80 , A01N59/00 , C02F1/50 , A61K9/22 , C09D5/16 , C23F11/04
CPC分类号： C02F1/50 , A01N25/12 , A01N43/80 , A01N59/00 , Y10S514/964
摘要： A sustained release antimicrobial agent comprises a clathrate compound composed of a water-soluble microbicide and at least one of the compounds shown at (I) to (V) below:(I) 1,1'-bi-2-naphthol;(II) 1,1,4,4-tetraphenyl-2-butyn-1,4-diol;(III) 9,10-di(4-methylphenyl)-9,10-dihydroznthracene-9,10-diol;(IV) 1,1-bis(4-hydroxyphenyl)-cyclohexane; and(V) 1,1,6,6-tetra(2,4-dimethylphenyl)-2,4-hexadiyne-1,6-diol.A method which uses it for preventing the fouling of a water system is also disclosed.
摘要翻译：持续释放的抗微生物剂包括由水溶性杀微生物剂和下列（I）至（V）所示的至少一种化合物组成的包合物：（I）1,1'-双-2-萘酚; （II）1,1,4,4-四苯基-2-丁炔-1,4-二醇; （III）9,10-二（4-甲基苯基）-9,10-二氢吖啶-9,10-二醇; （IV）1,1-双（4-羟基苯基） - 环己烷; 和（V）1,1,6,6-四（2,4-二甲基苯基）-2,4-己二炔-1,6-二醇。还公开了一种用于防止水系统结垢的方法。

16. 发明授权

US5618978A Method of producing choline of a high purity 失效
标题翻译：生产高纯度胆碱的方法
公开(公告)号：US5618978A
公开(公告)日：1997-04-08
申请号：US622082
申请日：1996-03-26
申请人： Shunji Hyoda , Youichi Hasegawa , Fumio Toda
发明人： Shunji Hyoda , Youichi Hasegawa , Fumio Toda
IPC分类号： C07C213/08 , C07C213/10 , C07C215/40 , C25B3/00 , C07C209/84
CPC分类号： C07C213/10 , C25B3/00
摘要： A method of producing a choline having a high purity without containing by-products by using a molecule-inclusion complex of the choline as a starting material. A choline inclusion complex without containing by-products is obtained by reacting an aqueous solution of the choline containing, as by-products, those cholines to which are added ethylene oxides with host molecules such as of 1,1'-bis-.beta.-naphthol, and is further reacted with a carbon dioxide gas in order to obtain an aqueous solution of a choline carbonate and/or a choline bicarbonate of a high purity, which is then subjected to the electrolysis using a cation-exchange membrane as a diaphragm, in order to obtain an aqueous solution of the choline of a high purity without containing by-products. The choline that is obtained is a strongly basic compound having a high purity and is very useful as a photoresist-developing solution.
摘要翻译：通过使用胆碱的分子包合配合物作为起始原料，生产具有高纯度而不含有副产物的胆碱的方法。不含有副产物的胆碱包合络合物通过将含有作为副产物的胆碱的水溶液与添加有环氧乙烷的主链分子例如1,1'-双-β-萘酚并进一步与二氧化碳气体反应，以获得高纯度的碳酸胆碱和/或胆碱碳酸氢盐的水溶液，然后使用阳离子交换膜作为隔膜进行电解，以获得高纯度的胆碱水溶液而不含副产物。获得的胆碱是具有高纯度的强碱性化合物，并且作为光致抗蚀剂显影溶液是非常有用的。

17. 发明授权

US5334776A Compound and separating agent 失效
标题翻译：复合分离剂
公开(公告)号：US5334776A
公开(公告)日：1994-08-02
申请号：US30058
申请日：1993-03-12
申请人： Fumio Toda
发明人： Fumio Toda
IPC分类号： C07B57/00 , C07B63/02 , C07C33/28 , C07C33/48 , C07C45/78 , C07C49/643 , C07D307/33
CPC分类号： C07D307/33 , C07B57/00 , C07C33/28 , C07C33/48 , C07C33/486 , C07C45/78 , C07C49/643
摘要： A compound represented by the general formula (I) and a separating agent comprising the same: ##STR1## wherein Ar and Ar' are each an aromatic group; and the positional relationship of the two substituents on the central benzene ring may be any of ortho, meta and para.The above compound is effective in the separation and purification of many compounds and enables the provision of various compounds (such as intermediates of drugs) which are useful in the field of fine chemicals, particularly optically active substances, at high purities and in large amounts.
摘要翻译： PCT No.PCT / JP92 / 01083 Sec。 371日期1993年3月12日 102（e）1993年3月12日PCT PCT 1992年8月27日PCT公布。出版物WO93 / 05004 日本1993年3月18日。由通式（I）表示的化合物和包含其的分离剂：其中Ar和Ar'各自为芳族基团; 并且中心苯环上的两个取代基的位置关系可以是邻位，间位和对位中的任何一个。上述化合物对许多化合物的分离和纯化是有效的，并且能够以高纯度和大量提供可用于精细化学品，特别是光学活性物质领域的各种化合物（例如药物的中间体）。

18. 发明授权

US5276214A Optically active biphenyl derivative and process for optical resolution 失效
标题翻译：光学活性联苯衍生物和光学拆分方法
公开(公告)号：US5276214A
公开(公告)日：1994-01-04
申请号：US993116
申请日：1992-12-18
申请人： Fumio Toda
发明人： Fumio Toda
IPC分类号： C07D207/267 , C07B57/00 , C07C33/46 , C07C39/15 , C07C43/23 , C07C205/00 , C07C209/88 , C07C211/00 , C07C211/27 , C07C231/20 , C07C255/12 , C07C311/00 , C07C317/00
CPC分类号： C07B57/00 , C07C33/46
摘要： A biphenyl compound having the formula (I) is newly separated into its optical active compound, and useful as an optically separating agent: ##STR1## wherein W, X and Y are each an atom or atomic group selected from among H, F, Cl, Br, I, CH.sub.3, CF.sub.3, OH, OCH.sub.3, NH.sub.2 and N(CH.sub.3).sub.2 and Z is an atom or atomic group selected from among Cl, Br, I, CH.sub.3 and OCH.sub.3, R is an atomic group having 1 to 20 carbon atoms and containing a polar functional group selected from among ##STR2##
摘要翻译：具有式（I）的联苯化合物新分离成其光学活性化合物，可用作光学分离剂：（*化学结构*）（I）其中W，X和Y各自为选自在H，F，Cl，Br，I，CH3，CF3，OH，OCH3，NH2和N（CH3）2中，Z是选自Cl，Br，I，CH3和OCH3中的原子或原子团，R是含有1〜20个碳原子的原子团，含有选自（*化学结构*）（*化学结构*）中的极性官能团

19. 发明授权

US4841081A Method of optically resolving a racemate or a diastereomeric mixture of glycidyl compound 失效
标题翻译：光学拆分缩水甘油基化合物的外消旋物或非对映体混合物的方法
公开(公告)号：US4841081A
公开(公告)日：1989-06-20
申请号：US918724
申请日：1986-10-14
申请人： Fumio Toda , Koichi Tanaka , Tetsuya Nakata
发明人： Fumio Toda , Koichi Tanaka , Tetsuya Nakata
IPC分类号： C07D303/16 , C07D303/28
CPC分类号： C07D303/28 , C07D303/16
摘要： A method of optically resolving a racemate, or a diastereomeric mixture, of a substituted or unsubstituted glycidyl ester or ether compound having at least one glycidylic structure represented by the formula ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3, independently from each other, represent H or CH.sub.3, and 1 to 3 asymmetric carbon atoms in the molecule, or a racemate of a beta-dihalohydrin ester compound, which comprises contacting said racemate or diastereomeric mixture with an optically active form of a compound having the following formula (I) ##STR2## wherein X represents a halogen atom, to form an inclusion complex compound having the optically active compound of formula (I) as a host, and separating the resulting complex compound.
摘要翻译：光学拆分取代或未取代的缩水甘油酯或醚化合物的外消旋物或非对映异构体混合物的方法，所述取代或未取代的缩水甘油酯或醚化合物具有由下式表示的至少一个缩水甘油基结构：其中R 1，R 2和R 3彼此独立地表示H 或分子中的1至3个不对称碳原子或β-二卤代醇酯化合物的外消旋体，其包括使所述外消旋体或非对映异构体混合物与光学活性形式的具有下式（I）的化合物接触

20. 发明授权

US4818771A Diphenic acid bis(dicyclohexylamide) for clothrate compound, process for producing the same 失效
标题翻译：二苯甲酸双（二环己基酰胺）用于布料化合物，其制备方法
公开(公告)号：US4818771A
公开(公告)日：1989-04-04
申请号：US941004
申请日：1986-12-12
申请人： Fumio Toda , Ayako Sekikawa , Hideo Sugi , Kenji Tahara
发明人： Fumio Toda , Ayako Sekikawa , Hideo Sugi , Kenji Tahara
IPC分类号： A01N37/18 , A01N25/08 , A61K47/48 , C07C67/00 , C07C231/00 , C07C233/65 , A61L3/00 , C02B1/18 , C07C103/24
CPC分类号： C07C233/65 , A01N25/08 , A61K47/48023 , C07C2101/14
摘要： Diphenic acid bis(dicyclohexylamide) represented by the following formula: ##STR1## A process for producing diphenic acid bis(dicyclohexylamide) represented by the above formula, which comprises dimerizing a diazonium salt of o-aminobenzoic acid in the presence of a reducing agent, followed by acidification to give 2,6'-dicarboxylbiphenyl; converting this dicarboxylic acid to 2,6'-dichloroformylbiphenyl by chlorination; and reacting this acid chloride with dicyclohexylamine.Sustained release antimicrobial compositions comprising a clathrate compound consisting of a microbial agent and diphenic acid bis(dicyclohexylamide) represented by the above formula.
摘要翻译：由下式表示的二苯酸双（二环己基酰胺）：由上式表示的二苯酸双（二环己基酰胺）的制造方法，其包括在还原剂存在下使邻氨基苯甲酸的重氮盐二聚，然后酸化得到2,6-二羧基联苯; 通过氯化将该二羧酸转化为2,6-二氯甲酰基联苯; 并使该酰氯与二环己基胺反应。包含由上式表示的微生物剂和二苯酸双（二环己基酰胺）组成的包合物的缓释抗微生物组合物。

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