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11. 发明授权

US5902442A Method for bonding lignocellulosic material with phenol-formaldehyde resin and carbon dioxide 失效
标题翻译：将木质纤维素材料与酚醛树脂和二氧化碳粘合的方法
公开(公告)号：US5902442A
公开(公告)日：1999-05-11
申请号：US487552
申请日：1995-06-07
申请人： Earl K. Phillips , William D. Detlefsen , Lewis D. Creel
发明人： Earl K. Phillips , William D. Detlefsen , Lewis D. Creel
IPC分类号： B27N3/00 , B27N3/08 , C08L97/02 , B32B31/12
CPC分类号： B32B37/12 , B27N3/002 , B27N3/086 , C08L97/02 , B32B2309/60 , B32B2317/16
摘要： Subjecting lignocellulosic components coated with an aqueous alkaline phenolic resole resin solution to carbon dioxide inhibits overpenetration of resin and improves bond strength when the coated components are heated to cure the resin by application of steam and pressure in the preparation of structural panels. Also, contact with carbon dioxide of high moisture resin coated lignocellulosic components accelerates the speed of cure and improves bond strength of panels cured under heat and pressure.
摘要翻译：将涂有碱性酚醛树脂水溶液的木质纤维素组分置于二氧化碳上时，抑制树脂的过度渗透，并且通过在制备结构面板时应用蒸汽和压力来加热涂覆组分以固化树脂，从而提高粘合强度。此外，与高湿度树脂涂层的木质纤维素组分的二氧化碳接触加速固化速度，并提高在热和压力下固化的板的粘合强度。

12. 发明授权

US5364902A Resorcinol-glutaraldehyde resin as an accelerator for curing phenol-formaldehyde resins 失效
标题翻译：间苯二酚 - 戊二醛树脂作为固化酚醛树脂的促进剂
公开(公告)号：US5364902A
公开(公告)日：1994-11-15
申请号：US991208
申请日：1992-12-15
申请人： David W. Shiau , William D. Detlefsen , Earl K. Phillips
发明人： David W. Shiau , William D. Detlefsen , Earl K. Phillips
IPC分类号： C08L61/06 , C08L97/02 , C08L51/00
CPC分类号： C08L61/06 , C08L97/02 , Y10T428/24099 , Y10T428/24132 , Y10T428/31946 , Y10T428/31957 , Y10T428/3196 , Y10T428/31989
摘要： The invention relates to the use of a resorcinol-glutaraldehyde reaction product as an accelerator for thermosetting phenolic resin and to a method of making the accelerator. Further, the invention relates to a resin blend comprising phenol-formaldehyde and the accelerator and a process for making cellulosic board, oriented strandboard and plywood wherein the binder for the cellulosic board, oriented strandboard and plywood in its uncured form comprises the resin blend of the invention. In another embodiment the accelerator for thermosetting resin comprises resorcinol and glutaraldehyde.
摘要翻译：本发明涉及间苯二酚 - 戊二醛反应产物作为热固性酚醛树脂的促进剂的用途及其制备方法。此外，本发明涉及包含苯酚 - 甲醛和促进剂的树脂共混物以及用于制备纤维素板，定向刨花板和胶合板的方法，其中用于纤维素板，定向刨花板和未固化形式的胶合板的粘合剂包括：发明。在另一个实施方案中，热固性树脂促进剂包括间苯二酚和戊二醛。

13. 发明授权

US06699958B1 Colorless phenol-formaldehyde resins that cure colorless 失效
标题翻译：无色酚醛树脂固化无色
公开(公告)号：US06699958B1
公开(公告)日：2004-03-02
申请号：US10365873
申请日：2003-02-13
申请人： William D. Detlefsen
发明人： William D. Detlefsen
IPC分类号： C08G1408
CPC分类号： C08G8/32
摘要： The present invention is directed to compositions and a process leading to colorless or light colored aqueous phicinol-formaldelhyde resoles. Unlike previous technologies, these compositions lead to clear storage stable fast curing, high molecular weight resins. These materials are also capable of producing composite wood panels with superior water absorption and thickness swell test results when soaked in water. The invention essentially consists of an aqueous copolymer of phenol, formaldehyde, and a phenolic carboxylate (e.g. salicylic acid). Methylol phenols are formed under alkaline conditions in the presence of metal chelating agents. These are then condensed into a polymer under alkaline, neutral or acidic conditions. The finished aqueous polymer solution is then acidified to the desired pH using a benzoic acid or a phelnol-carboxylic acid.
摘要翻译：本发明涉及组合物和一种导致无色或浅色的含有精氨酸 - 正癸醛水溶液的方法。与以前的技术不同，这些组合物导致清晰的储存稳定快速固化，高分子量树脂。这些材料也可以生产复合木板，当浸泡在水中时具有优异的吸水性和厚度溶胀试验结果。本发明基本上由苯酚，甲醛和酚羧酸酯（例如水杨酸）的含水共聚物组成。在金属螯合剂存在下，在碱性条件下形成羟甲基酚。然后将它们在碱性，中性或酸性条件下浓缩成聚合物。然后使用苯甲酸或吡咯烷羧酸将最终的聚合物水溶液酸化至所需的pH。

14. 发明授权

US06541576B1 Composition and method for curing a resorcinol resin 有权
标题翻译：用于固化间苯二酚树脂的组合物和方法
公开(公告)号：US06541576B1
公开(公告)日：2003-04-01
申请号：US09068510
申请日：1998-08-11
申请人： Earl K. Phillips , Arthur J. Garwood , William D. Detlefsen
发明人： Earl K. Phillips , Arthur J. Garwood , William D. Detlefsen
IPC分类号： C08F28300
CPC分类号： C08L61/06 , C08F283/00 , C08F283/006 , C08L61/12 , C08L61/14 , Y10T428/31989
摘要： A catalyst curing system or hardener for resorcinolic resins, such as resorcinol-formaldehyde or phenol-resorcinol-formaldehyde resins including methylolurea. The methylolurea may be used in combination with oxazolidine in ratios ranging from 5:95 to 95:, by molar basis. The hardener crosslinks the resins which permits reduction or “fuming” of formaldehyde as well as control of gel times of the resulting adhesive. The hardener of the present invention if of particular utility in adhesives for use in the forest products industry.
摘要翻译：用于间苯二酚树脂的催化剂固化体系或固化剂，例如间苯二酚 - 甲醛或酚 - 间苯二酚 - 甲醛树脂，包括羟甲基脲。羟甲基脲可与恶唑烷组合使用，比例范围为5:95至95:摩尔。固化剂交联树脂，其允许甲醛的还原或“发烟”以及控制所得粘合剂的凝胶时间。如果在用于森林产品工业的粘合剂中特别有用，则本发明的固化剂。

15. 发明授权

US06214265B1 Mixed PMDI/resole resin binders for the production of wood composite products 有权
标题翻译：用于生产木材复合材料的混合PMDI /树脂树脂粘合剂
公开(公告)号：US06214265B1
公开(公告)日：2001-04-10
申请号：US09213595
申请日：1998-12-17
申请人： James W. Rosthauser , William D. Detlefsen
发明人： James W. Rosthauser , William D. Detlefsen
IPC分类号： B27N300
CPC分类号： C08G18/7664 , B27N3/002 , C08G18/542 , C08G18/6492 , C08L97/02 , C08L2666/14
摘要： This invention relates to a process for the production of composite wood products. This process comprises a) applying a binder composition to wood particles, and b) molding or compressing the wood particles treated with the binder to form a composite wood product. Suitable binder compositions comprise a polymethylene poly(phenyl isocyanate) and a solid resole resin.
摘要翻译：本发明涉及生产复合木制品的方法。该方法包括a）将粘合剂组合物施用于木材颗粒，以及b）模塑或压缩用粘合剂处理的木材颗粒以形成复合木制品。合适的粘合剂组合物包含多亚甲基聚（苯基异氰酸酯）和固体甲阶酚醛树脂。

16. 发明授权

US5635583A Catalytic composition and method for curing urea-formaldehyde resin 失效
标题翻译：催化组合物和固化脲醛树脂的方法
公开(公告)号：US5635583A
公开(公告)日：1997-06-03
申请号：US469824
申请日：1995-06-06
申请人： William K. Motter , Nick K. Daisy , William D. Detlefsen
发明人： William K. Motter , Nick K. Daisy , William D. Detlefsen
IPC分类号： C08G12/12 , C08L61/24 , C08L97/02 , C08G14/04 , C08G14/08 , C08G14/10
CPC分类号： C08L61/24 , C08G12/12 , C08L97/02
摘要： Disclosed is a binder composition for binding substrates such as wood furnish for particleboard manufacture. The binder comprises a mixture of a first aqueous solution, comprising a buffering salt catalyst and preferably an acid, with a second aqueous solution comprising urea and formaldehyde. Methods of using the buffering salts as catalyst for curing urea-formaldehyde resins are also disclosed.
摘要翻译：公开了用于粘合基质例如木材配料用于刨花板制造的粘合剂组合物。粘合剂包括含有缓冲盐催化剂和优选酸的第一水溶液与包含尿素和甲醛的第二水溶液的混合物。还公开了使用缓冲盐作为脲醛树脂固化催化剂的方法。

17. 发明授权

US5059488A Glutaraldehyde resin binding system for manufacture of wood products 失效
标题翻译：用于制造木制品的戊二醛树脂结合体系
公开(公告)号：US5059488A
公开(公告)日：1991-10-22
申请号：US573389
申请日：1990-08-24
申请人： William D. Detlefsen , David Wen-I-Shiau , Nicholas K. Daisy
发明人： William D. Detlefsen , David Wen-I-Shiau , Nicholas K. Daisy
IPC分类号： C08G12/04 , C08G12/12 , C08L61/26 , C09J161/24 , C09J161/26
CPC分类号： C09J161/26 , C08G12/046 , C08L61/26 , Y10T428/31949 , Y10T428/31957 , Y10T428/31989
摘要： This invention relates to ethyleneurea-glutaraldehyde resins, urea-ethyleneurea-glutaraldehyde resins, their synthesis, as well as their application as an adhesive for wood panel manufacture. Molar ratio of ethyleneurea to glutaraldehyde can range from 0.3 to 3.5. Urea incorporated into ethyleneurea-glutaraldehyde resin can be high as two times the moles of glutaraldehyde used in the formulation and can be introduced at any stage during the reaction course, simply post added, or any combination of the above.

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