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11. 发明申请

US20090054557A1 CEMENT ADMIXTURE 审中-公开
公开(公告)号：US20090054557A1
公开(公告)日：2009-02-26
申请号：US11816983
申请日：2006-03-29
申请人： Hiroshi Yamazaki , Tsuyoshi Hirata , Akihiko Yamashita
发明人： Hiroshi Yamazaki , Tsuyoshi Hirata , Akihiko Yamashita
IPC分类号： C04B24/04
CPC分类号： C04B24/2605 , C04B40/0039 , C04B2103/302 , C04B2103/308 , C08F290/00 , C08F290/06 , C08L33/14 , C08L53/00 , C08L53/005 , C04B28/02 , C08L2666/04 , C08L2666/02 , C04B24/2647
摘要： The present invention aims at providing a cement admixture having superior water-reducing performance, along with no decrease in slump and slump flow caused by decrease in fluidity of a cement composition over time. A cement admixture is to be provided, which cement admixture comprises two or more members of polycarboxylic acid-based polymers, wherein said cement admixture comprises at least one polycarboxylic acid-based polymer (A) having a constitutional unit represented by the following formula (1): wherein R1 and R2 independently represent a hydrogen atom, an alkyl group with carbon atoms of 1 to 30, an alkenyl group with carbon atoms of 1 to 30, an aryl group with carbon atoms of 6 to 12; A represents an alkylene group with carbon atoms of 1 to 30 or an arylene group with carbon atoms of 6 to 12; a is 0 or 1; OR3 represents an oxyalkylene group with carbon atoms of 2 to 18, wherein each OR3 may be the same or different each other, provided that when OR3 is in a mixed form of two or more members, each OR3 may be added in a block or random form; R4 represents a hydrogen atom or a hydrocarbon group with carbon atoms of 1 to 30; and m represents an average mole number of oxyalkylene groups added and is in the range of 1 to 300; and at least one polycarboxylic acid-based polymer (B) having a constitutional unit represented by the following formula (2): wherein R5 and R6 independently represent a hydrogen atom, a methyl group; x is an integer in the range of 0 to 2 and y is 0 or 1, provided that x and y are not 0 at the same time; OR7 represents an oxyalkylene group with carbon atoms of 2 to 18, wherein each OR7 may be the same or different each other, provided that when OR7 is in a mixed form of two or more members, each OR7 may be added in a block or random form; R8 represents a hydrogen atom or a hydrocarbon group with carbon atoms of 1 to 30; and n represents an average mole number of oxyalkylene groups added and is in the range of 1 to 300; and the weight ratio of said polycarboxylic acid-based polymer (A) and said polycarboxylic acid-based polymer (B) [weight ratio of (A)/(B)] is in the range of 1/99 to 99/1.

12. 发明申请

US20070254976A1 Method For Production Of Cement Dispersant And Polycarboxylic Acid Type Polymer For Cement Dispersant 审中-公开
标题翻译：水泥分散剂和聚羧酸类聚合物水泥分散剂生产方法
公开(公告)号：US20070254976A1
公开(公告)日：2007-11-01
申请号：US11631694
申请日：2005-07-11
申请人： Tsuyoshi Hirata , Hirokatsu Kawakami
发明人： Tsuyoshi Hirata , Hirokatsu Kawakami
IPC分类号： C08F220/06 , C04B24/26
CPC分类号： C04B24/2647 , C04B2103/408 , C08F216/14 , C08F220/06
摘要： The efficiency of production of the polycarboxylic acid type cement dispersant is exalted. Photo-polymerization is adopted in the production of the polycarboxylic acid type cement dispersant by polymerizing at least one kind of monomer represented by the chemical formula 1 and at least one kind of monomer represented by the chemical formula 2. A polymer composition having a small solvent content is obtained by causing the polymerization reaction to proceed under the condition of containing the monomers at a high concentration. Specifically, this invention is directed toward a method for producing a powdered polycarboxylic acid type cement dispersant, which method comprises a step of polymerizing the monomers under the condition of containing the monomers at a concentration of 50-100 mass % based on the total mss of the monomers and the solvent, a step of cooling the formed polymer thereby solidifying the polymer, and a step of pulverizing the solidified polymer.
摘要翻译：提高了多元羧酸型水泥分散剂的生产效率。通过聚合由化学式1表示的至少一种单体和由化学式2表示的至少一种单体，聚羧酸型水泥分散剂的制备中采用光聚合。具有小溶剂的聚合物组合物通过使聚合反应在含有高浓度单体的条件下进行，得到含量。具体地说，本发明涉及一种粉末状多元羧酸型水泥分散剂的制造方法，其特征在于，在单体浓度为50〜100质量％的条件下，以单体总量mss 单体和溶剂，冷却形成的聚合物从而使聚合物固化的步骤和粉碎固化的聚合物的步骤。

13. 发明申请

US20060004149A1 Admixture composition for hydraulic material 审中-公开
标题翻译：液压材料的外加剂组合物
公开(公告)号：US20060004149A1
公开(公告)日：2006-01-05
申请号：US11168645
申请日：2005-06-27
申请人： Mari Masanaga , Tsuyoshi Hirata
发明人： Mari Masanaga , Tsuyoshi Hirata
IPC分类号： C08L71/02 , B28C5/00
CPC分类号： C04B24/2647 , C04B24/023 , C04B24/12 , C04B24/267 , C04B24/32 , C04B40/0039 , C04B2111/29 , C04B28/02 , C04B2103/302 , C04B2103/304
摘要： The present invention provids an admixture composition for hydraulic material that is capable of enabling minute air to be entrained into a hydraulic material composition and imparting an excellent the freeze/thaw durability to the hydraulic material. The object of the present invention is accomplished by an admixture composition for hydraulic material which contains component (A) and component (B) as essential components. The component (A) is a polyoxyalkylene polymer possessing a side chain containing a carboxyl group and the component (B) is a compound which is represented by the general formula (B-1) or (B-2). HO—(WO)p—H (B-1)
摘要翻译：本发明提供了一种水硬性材料的混合组合物，其能够使微小的空气被夹带在水硬性材料组合物中，并赋予水硬性材料优异的冷冻/解冻耐久性。本发明的目的是通过含有组分（A）和组分（B）作为必需组分的水硬性材料的混合物组合物来实现的。组分（A）是具有含羧基的侧链的聚氧化烯聚合物，组分（B）是由通式（B-1）或（B-2）表示的化合物。 <？in-line-formula description =“在线公式”end =“lead”？HO-（WO） -H（B-1）<βin-line-formula description =“内联公式”end =“tail”？>

14. 发明授权

US06919388B2 Cement admixture and cement composition 失效
标题翻译：水泥外加剂和水泥组成
公开(公告)号：US06919388B2
公开(公告)日：2005-07-19
申请号：US10110271
申请日：2001-06-27
申请人： Tomotaka Nishikawa , Hirokatsu Kawakami , Daisuke Imai , Hiromichi Tanaka , Tsuyoshi Hirata , Tsutomu Yuasa
发明人： Tomotaka Nishikawa , Hirokatsu Kawakami , Daisuke Imai , Hiromichi Tanaka , Tsuyoshi Hirata , Tsutomu Yuasa
IPC分类号： C04B24/32 , C04B24/12 , C04B24/26 , C04B24/28 , C04B28/00 , C04B103/32 , C04B103/48 , C04B103/50 , C04B111/00 , C08F220/20 , C08F290/06 , C08K5/06
CPC分类号： C04B24/2647 , C04B24/267 , C04B24/32 , C04B40/0028 , C04B40/0039 , C04B2103/408 , C04B2103/50 , C04B28/02
摘要： The admixtures for a cementitious composition of the invention, which have the above-mentioned constitutions, can suitably be used in cement pastes, mortar, concrete and like cement compositions and can stabilize the amount of air entrained with the lapse of time and thus facilitate the quality control of cement compositions and, further, can improve the workability of cement compositions owing to their excellent dispersing capacities. The cement compositions of the invention which comprise such admixture for a cementitious composition are excellent in water-reducing ability and workability and can give hardened products excellent in strength and durability and, further, can stably maintain the amount of air entrained without allowing increases in the amount of air even when the time of kneading is prolonged in the production.
摘要翻译：具有上述结构的本发明的水泥组合物的混合物可以适用于水泥浆，砂浆，混凝土和类似的水泥组合物，并且可以稳定随时间流入的空气量，从而有利于水泥组合物的质量控制，并且由于其优异的分散能力，可以改善水泥组合物的可加工性。包含这种水泥组合物的这种混合物的本发明的水泥组合物具有优异的降水能力和可加工性，并且可以得到强度和耐久性优异的硬化产品，并且还可以稳定地保持夹带的空气量，而不会增加即使在生产中延长捏合时间的情况下也可以使用空气量。

15. 发明授权

US06911494B2 Cement admixture and cement composition 有权
标题翻译：水泥外加剂和水泥组成
公开(公告)号：US06911494B2
公开(公告)日：2005-06-28
申请号：US10253425
申请日：2002-09-25
申请人： Akihiko Yamashita , Hiromichi Tanaka , Tsuyoshi Hirata , Toru Uno , Yoshiyuki Onda
发明人： Akihiko Yamashita , Hiromichi Tanaka , Tsuyoshi Hirata , Toru Uno , Yoshiyuki Onda
IPC分类号： C04B24/26 , C04B24/32 , C08G65/26 , C08G65/332 , C08L71/02 , C08L31/02
CPC分类号： C04B24/2647 , C04B2103/308 , C04B2103/32 , C08G65/2609 , C08G65/3322 , C08L71/02 , C08L2205/05 , C08L2666/04
摘要： It is an object of the present invention to provide a cement admixture which can show not only a high dispersing ability and a slump loss preventing effect but also a viscosity reducing effect and can show these characteristics even in the high water reduction ratio range, and a cement composition in which this admixture is used.A cement admixture comprising, as three essential constituents, a copolymer (A), an unsaturated (poly)alkylene glycol ether monomer (a) and an unpolymerizable (poly)alkylene glycol (B) not containing an alkenyl group, wherein the content of the unsaturated (poly)alkylene glycol ether monomer (a) is 1 to 100% by mass relative to the copolymer (A) and the content of the unpolymerizable (poly)alkylene glycol (B) not containing an alkenyl group is 1 to 50% by mass relative to the copolymer (A), the copolymer (A) comprising, as essential constituent units, a constituent unit (I) derived from the unsaturated (poly)alkylene glycol ether monomer (a) and a constituent unit (II) derived from an unsaturated carboxylic acid monomer (b), with the constituent unit (I) and constituent unit (II) each accounting for not less than 1% by mass based on all the constituent units, and the unsaturated carboxylic acid monomer (b) being an unsaturated monocarboxylic acid monomer.
摘要翻译：本发明的目的是提供一种能够显示出高的分散能力和防止坍落度损失的作用的水泥混合物，而且还能够降低粘度，并且即使在高的减水率范围内也能够显示出这些特性，使用该混合物的水泥组合物。一种水泥外加剂，其包含不含烯基的共聚物（A），不饱和（聚）亚烷基二醇醚单体（a）和不可聚合（聚）亚烷基二醇（B）作为三种必需成分，其中，不饱和（聚）亚烷基二醇醚单体（a）相对于共聚物（A）为1〜100质量％，不含烯基的不可聚合（聚）亚烷基二醇（B）的含量为1〜50％相对于共聚物（A）的共聚物（A），作为必要构成单元的共聚物（A），由不饱和（聚）亚烷基二醇醚单体（a）得到的构成单元（I）和由不饱和羧酸单体（b）与构成单元（I）和构成单元（II）各自占所有构成单元不少于1质量％，不饱和羧酸单体（b）为不饱和一元羧酸单体。

16. 发明申请

US20050080298A1 Production processes for alkylene oxide addition product and its derivatives 有权
标题翻译：烯化氧加成产物及其衍生物的生产方法
公开(公告)号：US20050080298A1
公开(公告)日：2005-04-14
申请号：US10500554
申请日：2003-05-02
申请人： Toru Inaoka , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
发明人： Toru Inaoka , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
IPC分类号： C08F299/02 , C08G65/26 , C08G65/28 , C08G65/332 , C07C67/26 , C08G59/14
CPC分类号： C08G65/2609 , C08G65/2696 , C08G65/3322
摘要： The present invention provides: a production process for an alkylene oxide addition product, by which a high-molecular alkylene oxide addition product can be obtained with ordinary production facilities while the formation of by-products is suppressed; and production processes for derivatives from the alkylene oxide addition product. The present invention production process for an alkylene oxide addition product comprises the step of carrying out an addition reaction of an alkylene oxide to a hydroxyl-group-containing saturated compound in order to obtain the alkylene oxide addition product; with the production process being characterized by further comprising: the initial step of causing the alkylene oxide to add to the hydroxyl-group-containing saturated compound in an amount of not larger than 20 mols on average of the alkylene oxide per 1 mol of the hydroxyl-group-containing saturated compound to thereby obtain an alkylene oxide low-mol-addition product; and the molar-degree-of-polyaddition-adjusting step of causing the alkylene oxide to further add to the alkylene oxide low-mol-addition product as obtained in the initial step; wherein a portion of the entirety of the alkylene oxide low-mol-addition product as obtained in the initial step is used in the molar-degree-of-polyaddition-adjusting step.
摘要翻译：本发明提供：一种环氧烷加成物的制造方法，通过该方法可以获得具有普通生产设备的高分子量烯化氧加成产物，同时抑制副产物的形成; 以及来自烯化氧加成产物的衍生物的制备方法。本发明的烯化氧加成产物的制备方法包括进行烯化氧与含羟基的饱和化合物的加成反应以获得环氧烷烃加成产物的步骤; 其制备方法的特征还在于：使每1摩尔羟基的烯化氧的平均相对于含有羟基的饱和化合物不少于20摩尔的环氧烷加成的初始步骤含有饱和化合物，得到环氧烷低摩尔加成产物; 和加成摩尔加聚度调整步骤，使得氧化烯进一步添加到初始步骤中获得的环氧烷低摩尔加成产物; 其中在初始步骤中获得的全部烯化氧低摩尔加成产物的一部分用于加聚度加聚步骤。

17. 发明授权

US06794473B2 Acrylic acid (salt) polymer, its production process and uses 有权
标题翻译：丙烯酸（盐）聚合物，其生产工艺和用途
公开(公告)号：US06794473B2
公开(公告)日：2004-09-21
申请号：US10126587
申请日：2002-04-22
申请人： Shigeru Yamaguchi , Tsuyoshi Hirata , Shorbu Shioji
发明人： Shigeru Yamaguchi , Tsuyoshi Hirata , Shorbu Shioji
IPC分类号： C08F12400
CPC分类号： C08F20/06
摘要： The present invention provides: an acrylic acid (salt) polymer, which has a low molecular weight and a narrow molecular weight distribution and can display excellent dispersibility, or which has a high molecular weight and a high water solubility; a production process that enables easy production of this polymer; and an acrylic acid (salt) polymer composition comprising this polymer. The acrylic acid (salt) polymer is an acrylic acid (salt) polymer of which not less than 1 weight % of the entirety is accounted for by an acrylic acid (salt) polymer having a specific terminal structure. In addition, the production process for an acrylic acid (salt) polymer comprises the step of carrying out polymerization of a monomer component including an acrylic acid (salt), wherein an acrylic acid (salt) having a furfural content of 200 to 400 weight ppm is used as at least a portion of the acrylic acid (salt) in an amount of not smaller than 10 weight % of the entire monomer component.
摘要翻译：本发明提供：具有低分子量和窄分子量分布且可显示优异分散性或具有高分子量和高水溶性的丙烯酸（盐）聚合物; 能够容易地生产该聚合物的制造方法; 和包含该聚合物的丙烯酸（盐）聚合物组合物。丙烯酸（盐）聚合物是丙烯酸（盐）聚合物，其不小于整体的1重量％由具有特定末端结构的丙烯酸（盐）聚合物占据。此外，丙烯酸（盐）聚合物的制备方法包括进行包含丙烯酸（盐）的单体组分的聚合的步骤，其中糠醛含量为200-400重量ppm的丙烯酸（盐）用作至少一部分丙烯酸（盐），其量不小于整个单体成分的10重量％。

18. 发明授权

US06762325B2 Method for production of alkoxylated compound 失效
标题翻译：烷氧基化合物的制造方法
公开(公告)号：US06762325B2
公开(公告)日：2004-07-13
申请号：US10144491
申请日：2002-05-13
申请人： Toru Inaoka , Yasuhiko Sato , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
发明人： Toru Inaoka , Yasuhiko Sato , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
IPC分类号： C07C21300
CPC分类号： C04B24/267 , B01F7/18 , B01J19/006 , B01J19/0066 , B01J19/18 , B01J2219/00063 , B01J2219/00168 , B01J2219/00768 , B01J2219/00779 , C04B24/2647 , C04B2103/408 , C08G65/2609 , C08G65/2696 , C08G65/30
摘要： When the reaction solution formed during the addition of an alkylene oxide to an active hydrogen-containing compound has viscosity of not less than 10 mPa·s, this invention provides a method for stirring the reaction solution by the rotation of a vane or vanes continuously disposed in the vertical direction within an agitating reaction vessel in such a manner that the numerical value C represented by the following formula (1): C=A/(h2−h1) (1) (wherein A denotes the length (m) of the vane or the vanes newly immersed by the supply of alkylene oxide, h1 denotes the height (m) of the liquid level before the supply of alkylene oxide, and h2 denotes the height (m) of the liquid level after the supply of alkylene oxide) may be not less than 0.5. By employing the method of this invention, it is made possible to effect addition of an alkylene oxide to the active hydrogen-containing compound with high efficiency. Further, the use of this method allows repression of the content of a by-product which causes the degradation of the characteristic properties of the alkoxylated compound.
摘要翻译：当在含有活性氢的化合物中加入烯化氧时形成的反应溶液的粘度不低于10mPa.s，本发明提供一种通过连续设置的叶片或叶片的旋转来搅拌反应溶液的方法在搅拌反应容器内沿垂直方向以下式（1）表示的数值C :(其中A表示叶片或通过供给环氧烷而新浸入的叶片的长度（m） h1表示供给环氧烷前的液面的高度（m），h2表示供给环氧烷以后的液面高度（μm））可以为0.5以上。通过采用本发明的方法，可以高效率地向含活性氢的化合物中加入烯化氧。此外，使用该方法可抑制副产物的含量，这导致烷氧基化化合物的特征性质的降解。

19. 发明授权

US06376581B1 Cement dispersant, method for production thereof, and cement composition using the dispersant 有权
标题翻译：水泥分散剂，其制造方法和使用该分散剂的水泥组合物
公开(公告)号：US06376581B1
公开(公告)日：2002-04-23
申请号：US09702858
申请日：2000-11-01
申请人： Yoshio Tanaka , Akira Ohta , Tsuyoshi Hirata , Toru Uno , Tsutomu Yuasa , Hideyuki Tahara
发明人： Yoshio Tanaka , Akira Ohta , Tsuyoshi Hirata , Toru Uno , Tsutomu Yuasa , Hideyuki Tahara
IPC分类号： C08K300
CPC分类号： C04B24/2647 , C04B24/2641 , C04B2103/302 , C04B2103/308 , C04B2103/408 , C04B2111/00189 , C08F2/38 , C08F220/06 , C08F290/062 , C08F2220/286 , C08F220/00
摘要： A cement dispersant having excellent ability to prevent slump loss and high water-reducing property which comprises a polycarboxylic acid type polymer having a specific molecular weight distribution, a method for the production thereof, and a cement composition using the dispersant are provided. The cement dispersant comprises as a main component thereof a polycarboxylic acid type polymer (A), having a weight average molecular weight in the range of 10,000 to 500,000 in terms of polyethylene glycol determined by gel permeation chromatography, and having a value determined by subtracting the peak top molecular weight from the weight average molecular weight in the range of 0 to 8,000.
摘要翻译：提供了具有优异的防止坍落度损失和高降水性能的水泥分散剂，其包含具有特定分子量分布的多元羧酸型聚合物，其制备方法和使用该分散剂的水泥组合物。水泥分散剂作为其主要成分，以聚乙二醇为基准，通过凝胶渗透色谱法测定重均分子量为10,000〜500,000的多元羧酸型聚合物（A），通过减去重均分子量在0至8,000范围内的峰顶分子量。

20. 发明授权

US4972025A Cement dispersant 失效
标题翻译：水泥分散剂
公开(公告)号：US4972025A
公开(公告)日：1990-11-20
申请号：US173200
申请日：1988-03-24
申请人： Tsuneo Tsubakimoto , Yoshinori Sano , Hideyuki Tahara , Tsuyoshi Hirata , Hiroshi Ito , Yasuhiro Mori
发明人： Tsuneo Tsubakimoto , Yoshinori Sano , Hideyuki Tahara , Tsuyoshi Hirata , Hiroshi Ito , Yasuhiro Mori
IPC分类号： B01F17/00 , B01F17/52 , C04B24/24 , C04B24/28
CPC分类号： C04B24/24 , B01F17/005 , C04B24/28
摘要： A cement dispersant containing a water-soluble polymer containing at least 10 mol % of structural units represented by the general formula I: ##STR1## wherein X is H or CH.sub.2 R.sup.1, R.sup.1 is H or COO--[--A).sub.m B).sub.n ]H, R is H, CH.sub.3, or COO--[--A).sub.m B).sub.n ]H (providing that R is H where X is CH.sub.2 R.sup.1), A is iminoalkylene having 2 to 4 carbon atoms, B is oxyalkylene having 2 to 4 carbon atoms, m is an average number in the range of 0.1 to 10, n is O or an average positive number not more than 100, --A).sub.m may be in a linear or branched configuration, wherein the sequence of A and B in the segment in parenthesis may be regular or random.
摘要翻译：包含含有至少10mol％由通式I表示的结构单元的水溶性聚合物的水泥分散剂：其中X为H或CH 2 R 1，R 1为H或COO - [ - A）m B） n] H，R是H，CH 3或COO - [ - A）mB）n] H（其中R是H，其中X是CH 2 R 1），A是具有2至4个碳原子的亚氨基亚烷基，B是氧亚烷基， 4个碳原子，m是0.1至10的平均数，n是0或不大于100的平均正数，-A）m可以是直链或支链构型，其中A和B的顺序在括号中的段可以是规则的或随机的。

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