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11. 发明授权

US4751011A Hydrocarbon soluble complexes based on metal salts of polyolefinic dicarboxylic acids 失效
标题翻译：基于聚烯烃二羧酸金属盐的烃溶性络合物
公开(公告)号：US4751011A
公开(公告)日：1988-06-14
申请号：US941095
申请日：1986-12-12
申请人： Robert D. Lundberg , Alan A. Schetelich , Antonio Gutierrez , Robert R. Phillips
发明人： Robert D. Lundberg , Alan A. Schetelich , Antonio Gutierrez , Robert R. Phillips
IPC分类号： C10M157/00 , C08F255/00 , C08L23/26 , C08L33/04 , C08L35/02 , C10M157/04 , C10M161/00 , C10M167/00 , C10N10/02 , C10N10/04 , C10N20/02 , C10N20/04 , C10N30/02 , C10N40/00 , C10N40/25 , F02B1/04 , C10M123/00
CPC分类号： C10M167/00 , C10M161/00 , C10M2205/00 , C10M2205/02 , C10M2207/027 , C10M2207/028 , C10M2207/09 , C10M2207/123 , C10M2207/125 , C10M2207/126 , C10M2207/129 , C10M2207/144 , C10M2207/146 , C10M2207/16 , C10M2207/22 , C10M2207/26 , C10M2207/262 , C10M2207/288 , C10M2209/02 , C10M2209/086 , C10M2215/04 , C10M2215/042 , C10M2215/08 , C10M2215/082 , C10M2215/086 , C10M2215/22 , C10M2215/221 , C10M2215/224 , C10M2215/225 , C10M2215/226 , C10M2215/26 , C10M2215/28 , C10M2215/30 , C10M2217/028 , C10M2217/046 , C10M2217/06 , C10M2219/044 , C10M2219/046 , C10M2219/068 , C10M2219/089 , C10M2223/045 , C10N2210/00 , C10N2210/01 , C10N2210/02 , C10N2210/03 , C10N2240/10 , C10N2240/101 , C10N2240/102 , C10N2240/103 , C10N2240/104 , C10N2240/106 , C10N2270/02 , F02B1/04
摘要： This invention relates to oil soluble additives particularly useful in lubricating oil compositions, and to concentrates or lubricating compositions containing these additives. The additives are various metal salts of mono- or dicarboxylic acids, anhydrides, esters, etc., which have been substituted with a high molecular weight hydrocarbon group, and derivatives thereof. The high molecular weight hydrocarbon group has a number average-molecular weight (M.sub.n) of greater than about 900. The metal salt additives are especially useful in combination with certain grafted ethylene-olefin copolymers or copolymers of 4-vinyl pyridine and esters of aliphatic mono-, di- or polycarboxylic acids as viscosifying agents.
摘要翻译：本发明涉及特别可用于润滑油组合物的油溶性添加剂，以及含有这些添加剂的浓缩物或润滑组合物。添加剂是已被高分子量烃基取代的单酸或二羧酸，酸酐，酯等的各种金属盐及其衍生物。高分子量烃基的数均分子量（Mn）大于约900.金属盐添加剂特别适用于某些接枝的乙烯 - 烯烃共聚物或4-乙烯基吡啶与脂族单体的酯的共聚物 - 二元或多元羧酸作为增粘剂。

12. 发明授权

US4692268A Method for controlling viscosity of organic liquids and compositions 失效
标题翻译：控制有机液体和组合物粘度的方法
公开(公告)号：US4692268A
公开(公告)日：1987-09-08
申请号：US814403
申请日：1985-12-30
申请人： Robert D. Lundberg , Robert R. Phillips , L. Sherwood Minckler , David Y. Chung
发明人： Robert D. Lundberg , Robert R. Phillips , L. Sherwood Minckler , David Y. Chung
IPC分类号： C08F8/30 , C08F8/44 , C10M157/06 , C10M159/18 , C10M149/00 , C10M155/00
CPC分类号： C10M159/18 , C08F8/30 , C08F8/44 , C10M157/06 , C10M2205/00 , C10M2205/02 , C10M2217/02 , C10M2217/024 , C10M2217/028 , C10M2217/06 , C10M2221/00 , C10M2221/041
摘要： A method for controlling the viscosity of organic liquids, said organic liquid having a solubility parameter of from about 6 to about 10.5, which comprises incorporating in said organic liquid a minor amount of a polymer complex, said complex being formed from the interaction of polymer A, containing neutralized sulfonate groups and polymer B, containing basic nitrogen groups, both functional groups being presented at a level of from about 4 to 500 meq. per 100 g. of polymer, wherein the polymeric backbone of polymer A and polymer B are the same.
摘要翻译：一种用于控制有机液体的粘度的方法，所述有机液体的溶解度参数为约6至约10.5，其包括在所述有机液体中引入少量的聚合物配合物，所述复合物由聚合物A的相互作用形成，含有中和的磺酸盐基团和含有碱性氮基团的聚合物B，两个官能团的存在量为约4至500meq。每100克的聚合物，其中聚合物A和聚合物B的聚合物主链相同。

13. 发明授权

US4665115A Method for controlling viscosity of organic liquids and compositions 失效
标题翻译：控制有机液体和组合物粘度的方法
公开(公告)号：US4665115A
公开(公告)日：1987-05-12
申请号：US781029
申请日：1985-09-27
申请人： Robert D. Lundberg , Robert R. Phillips , Dennis G. Peiffer , Ilan Duvdevani
发明人： Robert D. Lundberg , Robert R. Phillips , Dennis G. Peiffer , Ilan Duvdevani
IPC分类号： C10M159/18 , C08K5/01 , C08L39/08
CPC分类号： C10M159/18 , C10M2205/00 , C10M2205/02 , C10M2217/02 , C10M2217/028 , C10M2217/06 , C10M2221/00 , C10M2221/041
摘要： A method for controlling the viscosity of organic liquids, said organic liquid having a solubility parameter of from about 6 to about 10.5, which comprises incorporating in said organic liquid a minor amount of a polymer complex, said complex being comprised of polymer A, containing neutralized sulfonate groups and polymer B, containing basic nitrogen groups, both functional groups being presented at a level of from about 4 to 500 meq. per 100 g. of polymer, wherein polymer B has the formula: ##STR1## wherein R.sub.1 is H or an alkyl group having about 1 to about 8 carbon atoms, R.sub.2 is an alkyl group having about 1 to about 18 carbon atoms, x is about 50.0 to 99.8 weight percent and x is about 0.2 to about 50.0 weight percent.
摘要翻译：一种用于控制有机液体的粘度的方法，所述有机液体的溶解度参数为约6至约10.5，其包括在所述有机液体中引入少量的聚合物配合物，所述复合物包含聚合物A，其包含中和的磺酸盐基团和含有碱性氮基团的聚合物B，两个官能团的存在量为约4至500meq。每100克的聚合物，其中聚合物B具有下式：其中R 1为H或具有约1至约8个碳原子的烷基，R 2为具有约1至约18个碳原子的烷基，x为约50.0至99.8 重量百分比，x为约0.2至约50.0重量％。

14. 发明授权

US4536547A Polymer complexes of a neutralized ionic polymer and a polycaprolactone polymer 失效
标题翻译：中和离子聚合物和聚己内酯聚合物的聚合物络合物
公开(公告)号：US4536547A
公开(公告)日：1985-08-20
申请号：US566347
申请日：1983-12-28
申请人： Robert D. Lundberg , Robert R. Phillips
发明人： Robert D. Lundberg , Robert R. Phillips
IPC分类号： C08L25/18 , C09J125/18 , C08L51/04 , C08L51/08 , C08L51/00
CPC分类号： C08L25/18 , C09J125/18
摘要： This invention relates to unique and novel polymer complexes between a metal neutralized sulfonated polymer and a tertiary amine terminated polylactone composition. The resulting polymer complexes have a variety of uses including those as diverse as adhesive agents, thermoplastic elastomers, additive uses wherein these materials can be utilized to compatibilize two different polymers which are normally incompatible. These polymer complexes can also be blended with fillers and/or oils when the sulfonated polymer is elastomeric. The materials display thermoplastic character.
摘要翻译：本发明涉及金属中和的磺化聚合物和叔胺封端的聚内酯组合物之间独特且新颖的聚合物络合物。所得聚合物复合物具有多种用途，包括粘合剂，热塑性弹性体，添加剂用途，其中这些材料可用于增容通常不相容的两种不同聚合物。当磺化聚合物是弹性体时，这些聚合物复合物也可与填料和/或油混合。材料显示热塑性。

15. 发明授权

US3974240A Thermoplastic elastomer compositions 失效
标题翻译：热塑性弹性体组合物
公开(公告)号：US3974240A
公开(公告)日：1976-08-10
申请号：US524502
申请日：1974-11-18
申请人： Jan Bock , Robert D. Lundberg , Robert R. Phillips , Henry S. Makowski
发明人： Jan Bock , Robert D. Lundberg , Robert R. Phillips , Henry S. Makowski
IPC分类号： C08L23/32 , C08L23/16 , C08L23/06 , C08L23/12
CPC分类号： C08L23/32
摘要： This invention relates to processable ionic elastomer compositions having improved compression set properties, especially at elevated temperatures. In this invention an intractable ionic elastomer, for example, a sulfonated elastomer is blended with from 10 to 70 parts per hundred of a crystalline polyolefin to yield novel compositions having the above properties. Preferably the ionic elastomer is a sulfonated ethylene propylene terpolymer having from about 0.2 to 20 mole percent sulfonate groups, at least 95% of which are combined with counterions selected from the group consisting of Groups IA, IIA, IB, and IIB of the Periodic Table of Elements, aluminum, antimony, lead, and mixtures thereof. The sulfonated polymer is combined with said counterions by neutralization of a polysulfonic acid precurser with a basic material in which the desired counterion is present as the cation thereof. The anion of said basic material is preferably selected from the group consisting of oxide, hydroxide, and lower alkanoates, for example, acetate, formate, and propionate.
摘要翻译：本发明涉及具有改进的压缩变形特性的可加工的离子弹性体组合物，特别是在高温下。在本发明中，难溶性离子弹性体，例如磺化弹性体与每100份结晶聚烯烃共混10至70份，得到具有上述性能的新型组合物。优选地，离子弹性体是具有约0.2至20摩尔％磺酸盐基团的磺化乙烯丙烯三元共聚物，其至少95％与选自元素周期表IA，IIA，IB和IIB族的抗衡离子组合元素，铝，锑，铅及其混合物。将磺化聚合物与所述抗衡离子组合，通过用其中存在所需抗衡离子作为其阳离子的碱性材料中和多磺酸前体。所述碱性物质的阴离子优选选自氧化物，氢氧化物和低级链烷酸酯，例如乙酸盐，甲酸盐和丙酸盐。

16. 发明授权

US4904722A Method for controlling viscosity of organic liquids and compositions thereof 失效
标题翻译：用于控制有机液体粘度的方法及其组合物
公开(公告)号：US4904722A
公开(公告)日：1990-02-27
申请号：US788963
申请日：1985-10-18
申请人： Robert D. Lundberg , Robert R. Phillips , Dennis G. Peiffer , Ilan Duvdevani
发明人： Robert D. Lundberg , Robert R. Phillips , Dennis G. Peiffer , Ilan Duvdevani
IPC分类号： C08J3/24 , C08L23/32 , C08L57/06
CPC分类号： C08L23/32 , C08J3/246 , C08L57/06
摘要： A method for controlling the viscosity of organic liquids, said organic liquid having a solubility parameter of less than 9.5, a viscosity, as measured at 25.degree. C., of less than 200 centipoises and said organic liquid is selected from the group consisting of mineral oils, synthetic oils, naphthanes, alkanes, cycloalkanes and aromatics and mixtures thereof, which comprises incorporating in said organic liquid about 0.01 to 20 grams of polymer complex per 100 ml. of said organic liquid, said polymer complex being formed "in situ" in said organic liquid or dissolved in said organic liquid, said complex being comprised of polymer A, containing about 4 meq. to 500 meq. of neutralized sulfonate groups, and polymer B, containing basic nitrogen groups, both functional groups being present at a level of from about 4 to 500 meq. per 100 g. of polymer, wherein polymer B has the formula: ##STR1## wherein x is about 50.0 to 99.8 weight percent and y is about 0.2 to about 50.0 weight percent, wherein said sulfonate groups of said polymer A being neutralized with basic compounds selected from the group consisting of transition elements, said polymer A having a polymeric backbone substantially soluble in said organic liquid and said polymer having a molecular weight of about 1,000 to 10,000,000.
摘要翻译：一种用于控制有机液体的粘度的方法，所述有机液体的溶解度参数小于9.5，在25℃下测得的小于200厘泊的粘度和所述有机液体选自矿物质油，合成油，萘烷，烷烃，环烷烃和芳族化合物及其混合物，其包括在每一100ml中在所述有机液体中加入约0.01至20克聚合物复合物。的所述有机液体，所述聚合物复合物在所述有机液体中“原位”形成或溶解在所述有机液体中，所述复合物由聚合物A组成，含有约4meq。至500毫克的中和磺酸盐基团和含有碱性氮基团的聚合物B，两个官能团的存在量为约4至500meq。每100克的聚合物，其中聚合物B具有下式：其中x为约50.0至99.8重量％，y为约0.2至约50.0重量％，其中所述聚合物A的所述磺酸盐基团用碱性化合物中和，所述碱性化合物选自由过渡元素组成，所述聚合物A具有基本上可溶于所述有机液体的聚合物骨架，所述聚合物的分子量为约1,000至10,000,000。

17. 发明授权

US4617337A Novel polymer compositions based on sulfonated ionomers and amine containing polymers 失效
标题翻译：基于磺化离聚物和含胺聚合物的新型聚合物组合物
公开(公告)号：US4617337A
公开(公告)日：1986-10-14
申请号：US673005
申请日：1984-11-19
申请人： Robert D. Lundberg , Dennis G. Peiffer , Robert R. Phillips
发明人： Robert D. Lundberg , Dennis G. Peiffer , Robert R. Phillips
IPC分类号： C08L23/32 , C08L51/06 , C08K5/05 , C08K5/01 , C08L39/04 , C08L91/00
CPC分类号： C08L23/32 , C08L51/06
摘要： A composition comprising interacting a blend of a neutralized sulfonated polymer containing from about 4 meq. of metal sulfonate per 100 g. of polymer up to 200 meq. per 100 g. of polymer, said sulfonate polymer being at least 95% neutralized, complexed with a second polymer containing basic nitrogen atoms incorporated, pyridine copolymerized or grafted thereon, said polymer containing basic nitrogen from about 4 meq. up to 500 meq. per 100 g. of polymer, wherein the molar ratio of metal sulfonate groups to that of basic nitrogen atoms varies from about 0.03 to about 30; wherein said polymer containing basic nitrogen groups have the formula: ##STR1## wherein R.sub.1 is an alkyl group having about 1 to about 8 carbon atoms, R.sub.2 is an alkyl group having about 1 to about 18 carbon atoms, x is about 50 to about 99.8 wt. %, and y is about 0.2 to about 50 wt. %.
摘要翻译：一种组合物，其包含使含有约4meq的中和磺化聚合物的共混物相互作用。的金属磺酸盐/ 100g。的聚合物高达200meq。每100克的聚合物，所述磺酸盐聚合物至少95％中和，与含有碱性氮原子的第二聚合物络合，其中共聚或接枝的吡啶，所述聚合物含有约4meq的碱性氮。高达500毫克每100克的聚合物，其中金属磺酸盐基团与碱式氮原子的摩尔比为约0.03至约30; 其中所述含有碱性氮基团的聚合物具有下式：其中R 1为具有约1至约8个碳原子的烷基，R 2为具有约1至约18个碳原子的烷基，x为约50至约99.8 重量％，y为约0.2至约50wt。％。

18. 发明授权

US4483957A Antiplasticization of polymer complexes 失效
标题翻译：聚合物复合物的抗增塑
公开(公告)号：US4483957A
公开(公告)日：1984-11-20
申请号：US551106
申请日：1983-11-14
申请人： Robert D. Lundberg , Robert R. Phillips
发明人： Robert D. Lundberg , Robert R. Phillips
IPC分类号： B05D5/08 , C08L23/32 , C08L57/00 , C08L101/00 , C08K5/05
CPC分类号： B05D5/08 , C08L101/00 , C08L23/32 , C08L57/00
摘要： The instant invention relates to a process for increasing the viscosity of organic liquids by incorporating in said liquid a minor amount of polymer complex, and 1 to 1000 parts per million by volume of a cosolvent for the ionic groups of said polymer. The polymer complex comprises the reaction product of a metal neutralized sulfonated polymer and a styrene-ring pyridene copolymer, wherein the polymer complex is substantially soluble in said organic liquid, and pendant sulfonate groups which are substantially insoluble in said organic liquid. The cosolvent is selected because it will solubilize the pendant sulfonate groups and provide a reasonably homogeneous mixture of solvent, cosolvent and ionomeric polymer. The preferred compositions prepared by the method of the instant invention comprise an organic liquid having a solubility parameter of from 6 to 10.5 in combination with a polymer complex containing from 0.2 up to 10.0 mole % sulfonate groups which has been neutralized by a basic material selected from Groups IA and IIA, IB and IIB of the Periodic Table of Elements (and also lead, tin and antimony) and 1 to 1000 parts per million by volume of a nonvolatile alcohol or amine cosolvent.
摘要翻译：本发明涉及一种通过在所述液体中加入少量聚合物络合物来提高有机液体的粘度的方法，以及用于所述聚合物的离子基团的共溶剂的1至1000份（体积）。聚合物络合物包括金属中和的磺化聚合物和苯乙烯 - 环的亚
甲基共聚物的反应产物，其中聚合物络合物基本上可溶于所说的有机液体中，以及基本上不溶于所说有机液体的磺酸根基侧基。选择共溶剂是因为它将溶解磺酸根基团并提供合适的溶剂，共溶剂和离聚物聚合物的均匀混合物。通过本发明的方法制备的优选组合物包含溶解度参数为6至10.5的有机液体与含有0.2至10.0摩尔％磺酸盐基团的聚合物复合物组合，该组合物已经被选自以下的碱性物质中和：元素周期表IA和IIA，IB和IIB族元素（以及铅，锡和锑）和1至1000份/百万体积的不挥发性醇或胺助溶剂。

19. 发明授权

US4157992A Elastomeric blend compositions having improved weathering stability 失效
标题翻译：具有改善的风化稳定性的弹性共混组合物
公开(公告)号：US4157992A
公开(公告)日：1979-06-12
申请号：US855773
申请日：1977-11-29
申请人： Robert D. Lundberg , Robert R. Phillips
发明人： Robert D. Lundberg , Robert R. Phillips
IPC分类号： C08L23/32 , C08L91/00
CPC分类号： C08L23/32
摘要： The present invention relates to improved elastomeric blend compositions for injection molding and extrusion application having improved compression set, weathering stability and physical properties, wherein the improved elastomeric compositions include minimally a metal neutralized sulfonated EPDM terpolymer, a non-polar process oil, an inorganic filler, and a carbon black at critically selected concentration levels. These blend compositions can be readily processed due to their superior rheological properties on conventional plastic fabrication equipment, especially on low pressure injection molding equipment into elastomeric articles having excellent physical properties and desirable rubbery characteristics.
摘要翻译：本发明涉及用于注射成型和挤出应用的改进的弹性体共混组合物，其具有改进的压缩永久变形，耐候性稳定性和物理性能，其中改进的弹性体组合物包括金属中和的磺化EPDM三元共聚物，非极性加工油，无机填料，和一个选定浓度水平的炭黑。这些共混组合物由于其在常规塑料制造设备，特别是低压注塑设备上具有优异的物理性能和所需橡胶特性的弹性体制品中的优异的流变性能而可以容易地加工。

20. 发明授权

US4127546A Plasticization of neutralized sulfonated elastomers with rosin salts 失效
标题翻译：中和的磺化弹性体与松香盐的增塑
公开(公告)号：US4127546A
公开(公告)日：1978-11-28
申请号：US855755
申请日：1977-11-29
申请人： Robert D. Lundberg , Robert R. Phillips , Henry S. Makowski , Douglas Brenner
发明人： Robert D. Lundberg , Robert R. Phillips , Henry S. Makowski , Douglas Brenner
IPC分类号： C08L23/00 , C08L7/00 , C08L21/00 , C08L23/26 , C08L23/32 , C08L33/00 , C08L33/02 , C08L101/00 , C08L93/00
CPC分类号： C08L23/32 , Y10S260/31
摘要： This invention relates to an improved elastomeric composition of metal neutralized sulfonated polymers which are plasticized with a preferential plasticizer at a concentration level of at least 1 part by weight based on 100 parts by weight of the metal neutralized EPDM terpolymer, wherein the preferential plasticizer is a metal rosin salt. The resultant compositions have improved physical properties and can be processed on conventional plastic fabrication equipment.
摘要翻译：本发明涉及金属中和的磺化聚合物的改进的弹性体组合物，其基于100重量份的金属中和的三元共聚物三元共聚物，以优选的增塑剂增塑至少1重量份，其中，优选的增塑剂是金属松香盐。所得组合物具有改善的物理性能并且可以在常规塑料制造设备上加工。

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