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101. 发明授权

US09172084B2 Method for producing porous granules from inorganic material and the use thereof 有权
标题翻译：从无机材料制造多孔颗粒的方法及其用途
公开(公告)号：US09172084B2
公开(公告)日：2015-10-27
申请号：US14006929
申请日：2012-03-14
申请人： Christian Neumann , Jörg Becker , Achim Hofmann
发明人： Christian Neumann , Jörg Becker , Achim Hofmann
IPC分类号： C04B38/00 , C03B37/00 , C04B14/00 , H01M4/1393 , C03B19/06 , C03B19/14 , C04B14/02 , C04B14/06 , C04B18/02 , C04B20/00 , C04B38/04 , C23C16/01 , C23C16/40 , C23C16/453 , H01M10/052
CPC分类号： H01M4/1393 , C03B19/06 , C03B19/14 , C04B14/022 , C04B14/06 , C04B18/023 , C04B20/008 , C04B38/0022 , C04B38/045 , C23C16/01 , C23C16/402 , C23C16/453 , H01M10/052 , Y02E60/122 , Y02P70/54
摘要： Build-up granulation and compaction granulation methods are generally known for producing granules from porous inorganic material. In order to allow a cost-efficient yet also reproducible production of porous granules having a more pronounced hierarchical pore structure, the invention relates to a method comprising the following steps: (a) supplying a feedstock flow to a reaction zone in which the feedstock is converted to material particles by means of pyrolysis or hydrolysis, (b) depositing the material particles on a deposition surface (1a) forming a soot layer (5), (c) thermally hardening the soot layer (5) to form a porous soot plate (5a), and (d) comminuting the soot plate (5a) to form porous granules (13).
摘要翻译：通常已知用于从多孔无机材料制备颗粒的堆积造粒和压实造粒方法。为了允许具有更加显着的等级孔结构的多孔颗粒的成本有效而又可重复的生产，本发明涉及一种包括以下步骤的方法：（a）将原料流供应到其中原料为通过热解或水解转化为材料颗粒，（b）将材料颗粒沉积在形成烟灰层（5）的沉积表面（1a）上，（c）将烟灰层（5）热硬化以形成多孔烟灰板（5a）和（d）粉碎烟灰板（5a）以形成多孔颗粒（13）。

102. 发明授权

US09139908B2 Gradient thin films 有权
标题翻译：梯度薄膜
公开(公告)号：US09139908B2
公开(公告)日：2015-09-22
申请号：US14104796
申请日：2013-12-12
申请人： The Boeing Company
发明人： Alpana Ranade , Marvi A. Matos
IPC分类号： C23C16/50
CPC分类号： C23C16/50 , C23C16/453 , C23C16/45523
摘要： An article comprising a thickness of a first film from a surface of the article, the first film having a gradient chemical composition within at least a portion of the thickness of the first film in a vertical and/or horizontal direction relative to the surface of the article, and methods and systems for producing same.
摘要翻译：一种从制品的表面形成第一膜的厚度的物品，所述第一膜在第一膜的至少一部分厚度的垂直和/或水平方向上相对于所述第一膜的表面具有梯度化学组成文章，生产方法和系统。

103. 发明申请

US20140263181A1 METHOD AND APPARATUS FOR GENERATING HIGHLY REPETITIVE PULSED PLASMAS 审中-公开
标题翻译：用于产生高度重复脉冲等离子体的方法和装置
公开(公告)号：US20140263181A1
公开(公告)日：2014-09-18
申请号：US13860393
申请日：2013-04-10
申请人： Jaeyoung Park
发明人： Jaeyoung Park
IPC分类号： H05H1/46 , C23F1/08 , C23C16/509
CPC分类号： H05H1/46 , C23C16/0245 , C23C16/452 , C23C16/453 , C23C16/45557 , C23C16/505 , C23C16/515 , H01J37/32082 , H01J37/321 , H01J37/3211 , H01J37/32146 , H01L21/3065 , H05H2001/4667 , H05H2001/4682
摘要： A pulsed radio frequency inductive plasma source and method are provided. The source may generate plasma at gas pressures from 1 torr to 2000 torr. By utilizing high power RF generation from fast solid state switches such as Insulated-Gate Bipolar Transistor (IGBT) combined with the resonance circuit, large inductive voltages can be applied to RF antennas to allow rapid gas breakdown from 1-100 μs. After initial breakdown, the same set of switches or an additional rf pulsed power systems are utilized to deliver large amount of rf power, between 10 kW to 10 MW, to the plasmas during the pulse duration of 10 μs-10 ms. In addition, several methods and apparatus for controlling the pulse power delivery, timing gas and materials supply, constructing reactor and substrate structure, and operating pumping system and plasma activated reactive materials delivery system will be disclosed. When combined with the pulsed plasma generation, these apparatuses and the methods can greatly improve the applicability and the efficacy of the industrial plasma processing.
摘要翻译：提供脉冲射频感应等离子体源和方法。源可以在1托至2000托的气体压力下产生等离子体。通过利用与谐振电路相结合的诸如绝缘栅双极晶体管（IGBT）的快速固态开关的高功率射频产生，可以对RF天线施加大的感应电压，以允许从1-100μs的快速气体击穿。在初始故障之后，在10μs-10 ms的脉冲持续时间期间，使用相同组的开关或附加的rf脉冲功率系统在10 kW至10 MW之间向等离子体提供大量的功率。此外，将公开用于控制脉冲功率输送，正时气体和材料供应，构建反应器和基底结构以及操作泵送系统和等离子体激活反应物质输送系统的几种方法和装置。当与脉冲等离子体产生相结合时，这些装置和方法可以大大提高工业等离子体处理的适用性和有效性。

104. 发明申请

US20140227512A1 DEPOSITION OF SILICON OXIDE BY ATMOSPHERIC PRESSURE CHEMICAL VAPOR DEPOSITION 审中-公开
标题翻译：通过大气压力化学气相沉积沉积氧化硅
公开(公告)号：US20140227512A1
公开(公告)日：2014-08-14
申请号：US14346764
申请日：2012-09-13
申请人： Ryan C. Smith , Jeffery L. Stricker
发明人： Ryan C. Smith , Jeffery L. Stricker
IPC分类号： C23C16/40 , G02B1/10
CPC分类号： C23C16/402 , C03C17/245 , C03C2217/213 , C03C2217/23 , C03C2218/1525 , C07F7/0805 , C07F7/0838 , C07F7/12 , C07F7/1804 , C23C16/0209 , C23C16/401 , C23C16/403 , C23C16/405 , C23C16/407 , C23C16/453 , G02B1/10 , Y10T428/265
摘要： The invention provides methods for forming silicon oxide-containing layer(s) on a substrate, such as glass, by heating a substrate, vaporizing at least one precursor comprising a monoalkylsilane having an alkyl group with greater than two carbon atoms to form a vaporized precursor stream, and contacting a surface of the heated substrate with the vaporized precursor stream at about atmospheric pressure to deposit one or more layers comprising silicon oxide onto the surface of the substrate. The invention is particularly useful for applying an anti-iridescent coating to glass in an online float glass process.
摘要翻译：本发明提供了在诸如玻璃的基底上形成含氧化硅的层的方法，通过加热基底，汽化含有具有大于2个碳原子的烷基的单烷基硅烷的至少一种前体以形成汽化前体流并且使加热的基底的表面与蒸发的前体物流接近大气压力以将包含氧化硅的一个或多个层沉积到基底的表面上。本发明特别可用于在在线浮法玻璃工艺中将抗虹膜涂层应用于玻璃。

105. 发明授权

US08486488B2 Method and device for coating a polymer film with an oxide layer 有权
标题翻译：用氧化物层涂覆聚合物膜的方法和装置
公开(公告)号：US08486488B2
公开(公告)日：2013-07-16
申请号：US12092363
申请日：2006-11-02
申请人： Pierre Fayet , Torsten Olofsson , Hans-Jurgen Tiller , Thomas Richter
发明人： Pierre Fayet , Torsten Olofsson , Hans-Jurgen Tiller , Thomas Richter
IPC分类号： C23C16/00
CPC分类号： C23C16/453 , C23C16/401 , C23C16/54
摘要： A web of a polymer film (1) is coated with an oxide layer, in particular with an SiOx barrier layer, by transporting the web with the aid of a rotatable drum (12) through a plurality of flame bands, which are directed in a radial direction from above against the circumferential surface of the drum, which extend at a distance from each other across the width of the web being supported and transported on this circumferential surface, and which are fed with a gas mixture including a combustible gas, an oxidant, and a silicon containing compound. Therein the circumferential surface of the rotatable drum is cooled to a predetermined temperature and the web is transported through the area of the tip of the inner flame region. Polymer films with barrier layers produced in the named way have at small layer thicknesses of less than 10 nm very good barrier properties.
摘要翻译：聚合物膜（1）的网由氧化物层，特别是用SiO x阻挡层涂覆，借助可旋转的鼓（12）通过多个火焰带传送网径向方向从滚筒的圆周表面延伸，该圆周表面在该圆周表面上被支撑和输送的幅材的宽度上彼此间隔一定距离，并且被馈送有包括可燃气体，氧化剂，和含硅化合物。其中，可旋转滚筒的圆周表面被冷却到预定温度，并且幅材被输送通过内火焰区域的尖端区域。具有以指定方式制造的阻挡层的聚合物膜具有小于10nm的小层厚度非常好的阻隔性能。

106. 发明申请

US20100159240A1 CNT-INFUSED METAL FIBER MATERIALS AND PROCESS THEREFOR 有权
标题翻译： CNT-浸入式金属纤维材料及其工艺
公开(公告)号：US20100159240A1
公开(公告)日：2010-06-24
申请号：US12611073
申请日：2009-11-02
申请人： Tushar K. SHAH , Slade H. Gardner , Mark R. Alberding , Harry C. Malecki
发明人： Tushar K. SHAH , Slade H. Gardner , Mark R. Alberding , Harry C. Malecki
IPC分类号： B32B1/00 , B32B15/02 , B05D7/14 , B32B15/04
CPC分类号： C01B31/0226 , B05C3/125 , B05D1/18 , B05D7/20 , B05D7/544 , B22F3/002 , C01B32/16 , C22C47/04 , C23C16/02 , C23C16/0272 , C23C16/26 , C23C16/453 , C23C16/545 , Y10S977/742 , Y10S977/75 , Y10S977/752 , Y10S977/843 , Y10T428/292 , Y10T428/2924
摘要： A composition includes a carbon nanotube (CNT)-infused metal fiber material which includes a metal fiber material of spoolable dimensions, a barrier coating conformally disposed about the metal fiber material, and carbon nanotubes (CNTs) infused to the metal fiber material. A continuous CNT infusion process includes: (a) disposing a barrier coating and a carbon nanotube (CNT)-forming catalyst on a surface of a metal fiber material of spoolable dimensions; and (b) synthesizing carbon nanotubes on the metal fiber material, thereby forming a carbon nanotube-infused metal fiber material.
摘要翻译：组合物包括碳纳米管（CNT） - 金属纤维材料，其包括可卷绕尺寸的金属纤维材料，围绕金属纤维材料保形地设置的阻挡涂层，以及注入金属纤维材料的碳纳米管（CNT）。连续CNT输注方法包括：（a）在可卷绕的尺寸的金属纤维材料的表面上设置阻挡涂层和形成碳纳米管（CNT）的催化剂; 和（b）在金属纤维材料上合成碳纳米管，由此形成碳纳米管注入的金属纤维材料。

107. 发明授权

US07740901B2 Low temperature method of making a zinc oxide coated article and the coated article made thereby 有权
标题翻译：制造氧化锌涂层制品的低温方法和由此制成的涂覆制品
公开(公告)号：US07740901B2
公开(公告)日：2010-06-22
申请号：US11800065
申请日：2007-05-03
申请人： Michael B. Abrams , Roman Y. Korotkov , Gary S. Silverman , Ryan C. Smith , Jeffery L. Stricker
发明人： Michael B. Abrams , Roman Y. Korotkov , Gary S. Silverman , Ryan C. Smith , Jeffery L. Stricker
IPC分类号： B05D5/12
CPC分类号： C23C16/407 , C03C17/245 , C03C2217/216 , C03C2218/152 , C23C16/453
摘要： An atmospheric chemical vapor deposition method of making a zinc oxide coated glass article, made by directing one or more streams of gaseous reactants, specifically a zinc containing compound, and an oxygen containing compound, onto a surface of a transparent substrate material heated to a temperature of 400° C. or less.
摘要翻译：一种通过将一种或多种气态反应物流，特别是含锌化合物和含氧化合物引入到加热到温度的透明基底材料的表面上制备经氧化锌涂覆的玻璃制品的大气化学气相沉积方法 400℃以下。

108. 发明申请

US20090233105A1 Composite coatings comprising hollow and/or shell like metal oxide particles deposited via combustion deposition 审中-公开
标题翻译：复合涂层包括通过燃烧沉积沉积的中空和/或壳状金属氧化物颗粒
公开(公告)号：US20090233105A1
公开(公告)日：2009-09-17
申请号：US12149460
申请日：2008-05-01
申请人： Michael P. Remington, JR. , David D. McLean
发明人： Michael P. Remington, JR. , David D. McLean
IPC分类号： C23C16/06 , B32B17/06 , B32B15/04
CPC分类号： C23C16/453 , C03C17/002 , C03C17/007 , C03C17/25 , C03C23/006 , C03C2217/475 , C03C2218/112
摘要： Certain example embodiments relate to the combustion deposition depositing of coatings comprising metal oxide matrices loaded with hollow metal oxide particles. The hollow metal oxide particles may be produced by combusting an emulsion including an aqueous phase and an oil phase, and an optional surfactant. The aqueous and/or oil phase may include a first metal oxide precursor. A second metal oxide precursor may be combusted in addition to the emulsion to produce a dense binder layer, acting as a “glue” to hold the hollow particles together. The matrix and the hollow particles comprising the coating may be of or include the same metal or a different metal. In certain example embodiments, the microstructure of the final deposited coating may resemble the microstructure of coatings produced by wet chemical (e.g., sol gel) techniques.
摘要翻译：某些示例实施例涉及包含装载有中空金属氧化物颗粒的金属氧化物基体的涂层的燃烧沉积沉积。中空金属氧化物颗粒可以通过燃烧包含水相和油相的乳液和任选的表面活性剂来制备。水相和/或油相可以包括第一金属氧化物前体。除了乳液之外，第二金属氧化物前体可以燃烧以产生致密的粘合剂层，用作将胶体保持在一起的“胶”。包含该涂层的基质和中空颗粒可以是或包括相同的金属或不同的金属。在某些示例性实施例中，最终沉积的涂层的微结构可类似于通过湿化学（例如，溶胶凝胶）技术产生的涂层的微结构。

109. 发明申请

US20090232983A1 SUBSTRATE TEMPERATURE CONTROL FOR COMBUSTION CHEMICAL VAPOR DEPOSITION 审中-公开
标题翻译：用于燃烧化学气相沉积的衬底温度控制
公开(公告)号：US20090232983A1
公开(公告)日：2009-09-17
申请号：US11720846
申请日：2005-12-07
申请人： Johannes A.M. Ammerlaan , Ralph T.H. Maessen
发明人： Johannes A.M. Ammerlaan , Ralph T.H. Maessen
IPC分类号： C23C16/453 , C23C16/52
CPC分类号： C23C16/463 , C23C16/453 , C23C16/4586 , H01L21/67248
摘要： Method for depositing film on flexible (plastic/metal) foil and/or temperature sensitive substrates (101) by combustion chemical vapor deposition (C-CVD). A substrate (101) is held in place by suction to provide physical and thermal contact between the substrate (101) and a substrate holder (102) and, simultaneously, the substrate holder (102) is cooled using a cooling fluid and the substrate (101). Heating of the substrate (101) during C-CVD is controlled and deterioration by heating is avoided. The foil or substrate (101) is suitable, in particular, for use in flat and flexible displays.
摘要翻译：通过燃烧化学气相沉积（C-CVD）在柔性（塑料/金属）箔和/或温度敏感基板（101）上沉积膜的方法。通过抽吸将衬底（101）保持在适当位置，以在衬底（101）和衬底保持器（102）之间提供物理和热接触，并且同时使用冷却流体和衬底（ 101）。控制C-CVD时的基板（101）的加热，避免加热劣化。箔或衬底（101）特别适用于平面和柔性显示器。

110. 发明申请

US20090220702A1 METHOD FOR PREPARING METAL OXIDE CRYSTALLINE NANOPARTICLE FILMS FOR DYE SENSITIZED SOLAR CELL PHOTOANODES 有权
标题翻译：用于制备用于染料敏化太阳能电池片的金属氧化物晶体纳米膜的方法
公开(公告)号：US20090220702A1
公开(公告)日：2009-09-03
申请号：US12396200
申请日：2009-03-02
申请人： Hai Wang , Denis J. Phares , Erik Tolmachoff
发明人： Hai Wang , Denis J. Phares , Erik Tolmachoff
IPC分类号： C23C4/06
CPC分类号： C23C16/453 , C23C16/405 , H01G9/2031 , H01L2251/306 , H01M14/005 , Y02E10/542 , Y02P70/521
摘要： A method for manufacturing a dye sensitized nanocrystal film having the steps of exposing a tin oxide layer on a surface of a substrate to a flame for a time sufficient to form a layer of mesoporous, crystalline titanium oxide on the fluorinated tin oxide layer followed by sintering the substrate at a temperature of from about 300 to about 500° C. The flame contains a fuel gas, such as ethylene and oxygen and titanium organometallic. The concentration of titanium organometallic is from about 10 to about 2000 ppm. During the flame exposure step, the substrate is rotated about a central axis at a speed of from about 100 to about 600 RPM, and the flame is kept at a constant distance from the surface of the substrate. The temperature of the substrate is maintained at a temperature of less than 200° C. via the rotation and jets of gas.
摘要翻译：一种用于制造染料敏化纳米晶体膜的方法，其具有以下步骤：将基底表面上的氧化锡层暴露于火焰上足以在氟化氧化锡层上形成介孔的结晶二氧化钛层，随后烧结该基材在约300至约500℃的温度下。火焰含有诸如乙烯和氧气和钛的燃料气体。钛有机金属的浓度为约10至约2000ppm。在火焰曝光步骤期间，基板以约100至约600RPM的速度围绕中心轴旋转，并且将火焰保持在离基板表面恒定的距离处。通过气体的旋转和喷射将基板的温度保持在小于200℃的温度。

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