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91. 发明授权

US4920179A Sulfonomaleation of organic molecules and polymers 失效
标题翻译：有机分子和聚合物的硫代化
公开(公告)号：US4920179A
公开(公告)日：1990-04-24
申请号：US174380
申请日：1988-03-28
申请人： Warren A. Thaler , Stanley J. Brois , Henry K. Hall
发明人： Warren A. Thaler , Stanley J. Brois , Henry K. Hall
IPC分类号： C08F8/34 , C08F8/46
CPC分类号： C08F8/34 , C08F8/32 , C08F2810/20
摘要： A sulfone adduct which comprises the reaction product of: ##STR1## and an unsaturated hydrocarbon polymer wherein X is an alkyl group selected from the group consisting of C.sub.n H.sub.2n +1, wherein n=1 to 18; X is an aryl group selected from the group consisting of C.sub.m H.sub.m-1 wherein m=6 and C.sub.m H.sub.m-2 Z wherein m=6 and Z is selected from the group consisting of OR', R", COOR'", NO.sub.2, Cl, Br, F and I where R', R" and R'" having about 1 to about 18 carbon atoms; wherein said unsaturated hydrocarbon polymer is selected from the group consisting of ethylene propylene terpolymers, ethylene diene copolymers, propylene diene copolymers, polyisoprene, butyl rubber, polybutadiene and styrenebutadiene, and styrene-isoprene random and block copolymers, polypropylenes and polyisobutylenes.
摘要翻译：一种砜加合物，其包含以下反应产物：＆lt; IMAGE＆gt;和不饱和烃聚合物，其中X为选自C n H 2n + 1，其中n = 1-18的烷基; X是选自CmHm-1，其中m = 6和CmHm-2Z的芳基，其中m = 6，Z选自OR'，R“，COOR”，NO 2，Cl ，Br，F和I，其中R'，R“和R”'具有约1至约18个碳原子; 其中所述不饱和烃聚合物选自乙烯丙烯三元共聚物，乙烯二烯共聚物，丙烯二烯共聚物，聚异戊二烯，丁基橡胶，聚丁二烯和苯乙烯丁二烯，以及苯乙烯 - 异戊二烯无规和嵌段共聚物，聚丙烯和聚异丁烯。

92. 依法登记的发明

USH751H Method of inhibiting acid corrosion of ferrous metals 失效
标题翻译：阻止金属腐蚀的方法
公开(公告)号：USH751H
公开(公告)日：1990-03-06
申请号：US204839
申请日：1988-06-10
申请人： Daniel S. Sullivan , Stanley J. Brois , Robert C. Portnoy
发明人： Daniel S. Sullivan , Stanley J. Brois , Robert C. Portnoy
IPC分类号： C09K8/54 , C09K8/74 , C23F11/04 , E21B43/27
CPC分类号： C23F11/04 , C09K8/54 , C09K8/74
摘要： A method for inhibiting acid corrosion of metal well equipment which comprises introducing into an aqueous acid solution an inhibiting amount of a quaternary compound prepared by reacting a tertiary aromatic heterocyclic amine with a (halo-substituted-aryl) alkyl halide, and contacting the well equipment with the inhibited aqueous acid solution.

93. 发明授权

US4737303A Sulfomaleation of organic molecules and polymers 失效
标题翻译：有机分子和聚合物的磺化
公开(公告)号：US4737303A
公开(公告)日：1988-04-12
申请号：US911761
申请日：1986-09-26
申请人： Warren A. Thaler , Stanley J. Brois , Francis N. Ferrara
发明人： Warren A. Thaler , Stanley J. Brois , Francis N. Ferrara
IPC分类号： C08F8/34 , C08F8/46
CPC分类号： C08F8/34 , C08F8/32 , C08F2810/20
摘要： A covalently bonded reaction product of:(a) a sulfomaleic anhydride adduct with an unsaturated hydrocarbon polymer; and(b) a polar molecule containing at least one primary or secondary amino group.
摘要翻译：共价键合的反应产物：（a）磺基马来酸酐加合物与不饱和烃聚合物; 和（b）含有至少一个伯或仲氨基的极性分子。

94. 发明授权

US4491524A Lubricating additive for drilling muds 失效
标题翻译：钻井泥浆润滑添加剂
公开(公告)号：US4491524A
公开(公告)日：1985-01-01
申请号：US559340
申请日：1983-12-08
申请人： Antonio Gutierrez , Darrell W. Brownawell , Thad O. Walker , Stanley J. Brois
发明人： Antonio Gutierrez , Darrell W. Brownawell , Thad O. Walker , Stanley J. Brois
IPC分类号： C09K8/22 , C09K7/00 , C09K3/00 , E21B3/00
CPC分类号： C09K8/22 , C09K2208/02
摘要： Aqueous drilling fluids containing a minor amount of an additive composition featuring oxazolines of C.sub.1 -C.sub.30 alkylthioglycolic acid. Such fluids are especially useful where reduced torque drilling fluids are needed. Another embodiment of this invention relates to a method of drilling utilizing the above-described fluids.
摘要翻译：含有少量具有C1-C30烷硫基乙醇酸恶唑啉的添加剂组合物的水溶液钻井液。这种流体在需要减少扭矩钻井液的情况下尤其有用。本发明的另一个实施例涉及利用上述流体的钻井方法。

95. 发明授权

US4417062A Thio-bis-(alkyl lactone acid esters) and thio-bis-(hydrocarbyl diacid esters) are useful additives for lubricating compositions 失效
公开(公告)号：US4417062A
公开(公告)日：1983-11-22
申请号：US173299
申请日：1980-07-25
申请人： Stanley J. Brois , Antonio Gutierrez
发明人： Stanley J. Brois , Antonio Gutierrez
IPC分类号： C07D307/33 , C08F8/34 , C10L1/24 , F02B3/06 , C07D307/32
CPC分类号： C08F8/34 , C10L1/2493 , C10M1/08 , C10M2205/00 , C10M2205/022 , C10M2205/026 , C10M2205/14 , C10M2207/024 , C10M2209/084 , C10M2209/086 , C10M2209/112 , C10M2215/065 , C10M2215/22 , C10M2215/221 , C10M2215/225 , C10M2215/226 , C10M2215/30 , C10M2219/085 , C10M2219/087 , C10M2219/088 , C10M2219/089 , C10M2219/09 , C10M2219/10 , C10M2219/102 , C10M2219/104 , C10M2219/106 , C10M2223/041 , C10M2223/045 , C10M2223/047 , C10M2229/02 , C10M2229/05 , C10N2210/03 , C10N2240/08 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106 , C10N2270/02 , F02B3/06
摘要： Thio-bis-(hydrocarbyl substituted diacid materials), such as thio-bis-(polyalkyl lactone acid) and/or their precursors, the adducts of sulfur chloride and unsaturated diacid materials, e.g., 4,8-bis-polyalkyl-4,8-dichloro-5-thiaundecane-1,2,10,11-tetracarboxylic acid bis-anhydride and their dehydrochlorinated analogs, when esterified with an alcohol, preferably a polyol, such as pentaerythritol, polypentaerythritol or a polyalkylene glycol with or without acid catalysts and/or metal template reagents yield thio-bis-(alkyl lactone acid esters) and thio-bis-(hydrocarbyl diacid esters) which can be characterized in part, as macrocyclic and/or macrocyclic-like structures, are useful as stable additives in lubricating compositions, e.g. as varnish inhibiting dispersants for lubricating oils and fuels.

96. 发明授权

US4155910A Two phase process for the preparation of azole and azoline disulfides 失效
标题翻译：用于制备唑和二硫化吡啶的两相方法
公开(公告)号：US4155910A
公开(公告)日：1979-05-22
申请号：US771183
申请日：1977-02-23
申请人： Stanley J. Brois , Antonio Gutierrez
发明人： Stanley J. Brois , Antonio Gutierrez
IPC分类号： C07D235/28 , C07D277/78 , C07D285/08 , C07D285/12 , C07D285/125 , C10M135/32 , C10M135/36
CPC分类号： C07D285/08 , C07D235/28 , C07D277/78 , C07D285/125 , C10M135/32 , C10M135/36 , C10M2219/10 , C10M2219/102 , C10M2219/104 , C10M2219/106 , C10N2240/08 , C10N2240/102 , C10N2240/103 , C10N2240/105 , C10N2240/40 , C10N2250/10
摘要： Azole and azoline disulfides useful as corrosion inhibitors and antiwear agents are prepared by the halogen-induced coupling of a thiol reactant e.g., hydrocarbyl mercaptans, with a metal azole thiolate, e.g. the potassium salt of 3,5-bis-mercapto 1,2,4-thiadiazole or 2,5-bis-mercapto 1,3,4 thiadiazole in a 2-phase reaction medium comprising a mixture of a hydrocarbon and water.
摘要翻译：用作腐蚀抑制剂和抗磨剂的唑和二氮杂二硫化物通过卤素诱导的硫醇反应物例如烃基硫醇与金属唑硫醇盐的偶联来制备。 3,5-二巯基1,2,4-噻二唑的钾盐或2,5-双巯基1,3,4噻二唑在包含烃和水的混合物的2相反应介质中。

97. 发明授权

US4123373A Lactone polyol esters as oleaginous additives 失效
标题翻译：内酯多元醇酯作为含油添加剂
公开(公告)号：US4123373A
公开(公告)日：1978-10-31
申请号：US768265
申请日：1977-02-14
申请人： Stanley J. Brois , Antonio Gutierrez
发明人： Stanley J. Brois , Antonio Gutierrez
IPC分类号： C10M159/12 , C07D307/33 , C07D309/30 , C08F8/06 , C08F8/14 , C08F8/34 , C10L1/198 , C10L1/24 , C10M129/76 , C10M129/95 , C10M135/26 , C10M135/32 , C10N30/04 , C10N40/25 , C07D307/32 , C10M1/28
CPC分类号： C10M135/26 , C08F8/08 , C08F8/12 , C08F8/14 , C08F8/16 , C08F8/34 , C10L1/198 , C10L1/2475 , C10M129/76 , C08F2810/20 , C08F2810/50 , C10M2205/00 , C10M2205/022 , C10M2205/026 , C10M2205/14 , C10M2207/282 , C10M2207/287 , C10M2207/289 , C10M2207/30 , C10M2207/34 , C10M2209/084 , C10M2209/086 , C10M2209/103 , C10M2209/104 , C10M2209/105 , C10M2209/106 , C10M2209/11 , C10M2209/112 , C10M2209/12 , C10M2219/085 , C10M2219/09 , C10M2223/041 , C10M2223/045 , C10M2229/02 , C10M2229/05 , C10N2210/02 , C10N2240/08
摘要： Lactone polyol ester reaction products of hydrocarbon substituted lactone carboxylic acid, with polyols such as pentaerythritol and their derivatives are useful additives in oleaginous compositions, such as varnish-inhibiting dispersants for lubricating oils, and fuels.
摘要翻译：烃取代的内酯羧酸与多元醇如季戊四醇及其衍生物的内酯多元醇酯反应产物是油性组合物中的有用添加剂，例如用于润滑油的清漆抑制性分散剂和燃料。

98. 发明授权

US4116876A Borated oxazolines as varnish inhibiting dispersants in lubricating oils 失效
标题翻译：硼酸恶唑啉作为润滑油中的清漆抑制分散剂
公开(公告)号：US4116876A
公开(公告)日：1978-09-26
申请号：US763545
申请日：1977-01-28
申请人： Stanley J. Brois , Antonio Gutierrez , Esther D. Winans
发明人： Stanley J. Brois , Antonio Gutierrez , Esther D. Winans
IPC分类号： C08F8/00 , B01F17/32 , C07F5/04 , C08F8/42 , C10L1/30 , C10M133/58 , C10M135/32 , C10M1/10 , C10M1/50
CPC分类号： C10L1/303 , C07F5/04 , C08F8/42 , C10M133/58 , C10M135/32 , C10M2205/00 , C10M2205/022 , C10M2205/026 , C10M2205/14 , C10M2207/024 , C10M2207/32 , C10M2209/084 , C10M2209/086 , C10M2209/112 , C10M2211/02 , C10M2215/065 , C10M2219/087 , C10M2219/088 , C10M2219/089 , C10M2223/041 , C10M2223/045 , C10M2227/062 , C10M2229/02 , C10M2229/05 , C10N2210/02
摘要： Borated derivatives of: (a) hydrocarbyl substituted mono- and bis-oxazolines obtained as a reaction product of hydrocarbyl substituted dicarboxylic acid, ester, or anhydride, for example, polyisobutenylsuccinic anhydride with from 1 to 2 molar equivalents of a 2,2-disubstituted-2-amino-1-alkanols, such as tris-(hydroxymethylamino)methane (THAM); and, (b) lactone oxazolines obtained as a reaction product of hydrocarbyl substituted lactone carboxylic acids, for example, polybutyl lactone carboxylic acid, with 2,2-disubstituted-2-amino-1-alkanols, such as tris-(hydroxymethyl)aminomethane (THAM), and their derivatives are useful additives in lubricating oils since both the sludge dispersant and/or varnish inhibiting properties of said oil are enhanced.
摘要翻译：硼酸衍生物：（a）作为烃基取代的二羧酸，酯或酸酐的反应产物获得的烃基取代的单 - 和双 - 恶唑啉，例如聚异丁烯基琥珀酸酐与1至2摩尔当量的2,2-二取代的 -2-氨基-1-链烷醇，例如三 - （羟甲基氨基）甲烷（THAM）; 和（b）作为烃基取代的内酯羧酸例如聚丁内酯羧酸与2,2-二取代-2-氨基-1-链烷醇如三 - （羟甲基）氨基甲烷的反应产物获得的内酯恶唑啉（THAM），其衍生物是润滑油中有用的添加剂，因为所述油的污泥分散剂和/或清漆抑制性能都得到增强。

99. 发明授权

US4062786A Lactone oxazolines as oleaginous additives 失效
标题翻译：内酯恶唑啉作为含油添加剂
公开(公告)号：US4062786A
公开(公告)日：1977-12-13
申请号：US726206
申请日：1976-09-24
申请人： Stanley J. Brois , Antonio Gutierrez
发明人： Stanley J. Brois , Antonio Gutierrez
IPC分类号： C07D413/06 , C07D307/32 , C07D307/33 , C07D307/60 , C07D309/30 , C07D413/14 , C10L1/233 , C10L1/24 , C10M133/44 , C10M133/48 , C10M133/58 , C10M135/22 , C10M135/32 , C10N30/04 , C10N30/12 , C10N40/04 , F02B3/06 , C10M1/32 , C07D263/10 , C08F8/32 , C10M3/26
CPC分类号： C07D307/33 , C07D307/32 , C07D307/60 , C07D309/30 , C10L1/233 , C10L1/2493 , C10M133/44 , C10M133/48 , C10M133/58 , C10M135/32 , C10M2205/00 , C10M2205/022 , C10M2205/026 , C10M2205/14 , C10M2207/024 , C10M2209/084 , C10M2209/086 , C10M2209/112 , C10M2215/065 , C10M2215/22 , C10M2215/221 , C10M2215/225 , C10M2215/226 , C10M2215/30 , C10M2219/085 , C10M2219/087 , C10M2219/088 , C10M2219/089 , C10M2219/09 , C10M2219/10 , C10M2219/102 , C10M2219/104 , C10M2219/106 , C10M2223/041 , C10M2223/045 , C10M2223/047 , C10M2229/02 , C10M2229/05 , C10N2210/03 , C10N2240/08 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106 , C10N2270/02 , F02B3/06
摘要： Lactone oxazoline reaction products of hydrocarbon substituted lactone carboxylic acids, for example, polybutyl lactone carboxylic acid, with 2,2-disubstituted-2-amino-1-alkanols, such as tris-(hydroxymethyl)aminomethane (THAM), and their derivatives are useful additives in oleaginous compositions, such as sludge dispersants for lubricating oil, or anti-rust agents for gasoline.
摘要翻译：烃取代的内酯羧酸（例如聚丁内酯羧酸）与2,2-二取代-2-氨基-1-链烷醇如三 - （羟甲基）氨基甲烷（THAM）及其衍生物的内酯恶唑啉反应产物是含油组合物中有用的添加剂，如润滑油污泥分散剂，或汽油防锈剂。

100. 发明授权

US4042523A Olefin-thionophosphine sulfide reaction products, their derivatives and use thereof as oil and fuel additives 失效
标题翻译：烯烃 - 硫代磷化氢反应产物，其衍生物和作为油和燃料添加剂的用途
公开(公告)号：US4042523A
公开(公告)日：1977-08-16
申请号：US622161
申请日：1975-10-14
申请人： Stanley J. Brois
发明人： Stanley J. Brois
IPC分类号： C07F9/32 , C07F9/38 , C07F9/40 , C07F9/6578 , C08F8/34 , C08F8/40 , C10L1/26 , C10M137/14 , C10M159/12 , C10M169/00 , C10M1/48
CPC分类号： C10M159/123 , C07F9/6578 , C08F8/40 , C10L1/2691 , C10M1/08 , C10M137/14 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/026 , C10M2207/282 , C10M2207/32 , C10M2207/34 , C10M2209/084 , C10M2209/086 , C10M2209/103 , C10M2209/104 , C10M2209/109 , C10M2209/111 , C10M2211/02 , C10M2215/065 , C10M2219/087 , C10M2219/088 , C10M2219/089 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/047 , C10M2223/06 , C10M2223/061 , C10M2223/063 , C10M2223/065 , C10M2223/12 , C10M2225/00 , C10M2225/02 , C10M2225/04 , C10M2225/041 , C10M2229/02 , C10M2229/05 , C10N2210/02 , C10N2270/02
摘要： Adducts are formed in a process which involves the reaction of an olefin, including olefin polymers, with a dimeric thionophosphine sulfide. Further derivatives may be formed by reacting the resulting olefin-thionophosphine sulfide adduct products with amines, e.g., alkylene polyamines, aziridines, phosphines or metal salts, e.g., zinc salts. Or, alkylene polyamine- or aziridine- treated olefin-thionophosphine sulfide reaction products may be further reacted with metal salts, e.g., zinc acetate. A representative material can be prepared by reacting polyisobutylene with an arylthionophosphine sulfide, and then further reacting the resulting cyclic bis(phosphinodithioic acid) anhydride product with an alkylene polyamine or aziridine, which in turn, may be further modified by reaction with zinc acetate.The oil soluble olefin-thionophosphine sulfide products, as well as its oil soluble derivatives outlined above, may be used as additives for lubricating oil, and petroleum fuels, e.g., gasoline or fuel oil.
摘要翻译：在包括烯烃聚合物的烯烃与二聚硫代膦硫化物反应的方法中形成加合物。另外的衍生物可以通过使所得到的烯烃 - 硫代膦硫化物加合产物与胺例如亚烷基多胺，氮丙啶，膦或金属盐例如锌盐反应形成。或者，亚烷基多胺或氮丙啶处理的烯烃 - 硫代膦化物反应产物可以与金属盐例如乙酸锌进一步反应。代表性材料可以通过使聚异丁烯与芳基硫羰基硫化膦反应制备，然后使所得的环状双（膦酸二硫酸）酸酐产物与亚烷基多胺或氮丙啶进一步反应，其又可以通过与乙酸锌反应进一步改性。

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