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91. 发明授权

US5319030A One-step process for the preparation of alkenyl succinic anhydride 失效
标题翻译：用于制备烯基琥珀酸酐的一步法
公开(公告)号：US5319030A
公开(公告)日：1994-06-07
申请号：US919342
申请日：1992-07-23
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C08F8/46 , C08F10/00 , C08F210/16 , C08F255/02 , C08F255/10 , C10M145/16
CPC分类号： C08F255/02 , C08F255/10
摘要： A process for the preparation of an alkenyl-substituted succinic anhydride wherein the alkenyl substituent has a number average molecular weight of from about 500 to 5000 and the average number of succinic groups per alkenyl group is greater than 1.2 which comprises reacting a polyolefin having an alkylvinylidene isomer content of less than about 10 percent and a number average molecular weight of about 500 to 5000 with maleic anhydride in the presence of a free radical initiator at a temperature in the range of about 80.degree. C. to 220.degree. C. for a period of less than 20 hours, wherein the molar ratio of maleic anhydride to polyolefin is about 1.0:1 to 9:1, and wherein the half-life of the decomposition of the free radical initiator is about 5 minutes to 10 hours at the reaction temperature.
摘要翻译：一种烯基取代的琥珀酸酐的制备方法，其中链烯基取代基的数均分子量为约500至5000，每个烯基的琥珀酸基平均数大于1.2，其包括使具有烷基亚乙烯基异构体含量小于约10％，数均分子量为约500至5000的马来酸酐在自由基引发剂存在下，在约80℃至220℃的温度下进行一段时间小于20小时，其中马来酸酐与聚烯烃的摩尔比为约1.0:1至9:1，并且其中自由基引发剂的分解的半衰期在反应温度下为约5分钟至10小时。

92. 发明授权

US4734212A Lubricating oil compositions containing bis-mannich base deposit inhibitors and a process for their preparation 失效
标题翻译：含有双甘露醇碱沉积抑制剂的润滑油组合物及其制备方法
公开(公告)号：US4734212A
公开(公告)日：1988-03-29
申请号：US846768
申请日：1986-03-31
申请人： James J. Harrison
发明人： James J. Harrison
IPC分类号： C10M133/08 , C10M159/16 , C10N10/02 , C10N10/04 , C10N30/04 , C10N40/25 , C10M129/26 , C10M133/04
CPC分类号： C10M133/08 , C10M2215/042 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106 , C10N2270/02
摘要： Disclosed are Bis-Mannich base deposit inhibitors; lubricating oil compositions containing these inhibitors and a process for preparing these inhibitors.
摘要翻译：披露了双曼尼希碱沉积物抑制剂; 含有这些抑制剂的润滑油组合物和制备这些抑制剂的方法。

93. 发明授权

US4697040A Isomerization of vinylidene olefins 失效
标题翻译：亚乙烯基烯烃的异构化
公开(公告)号：US4697040A
公开(公告)日：1987-09-29
申请号：US1930
申请日：1987-01-08
申请人： Roger C. Williamson , James J. Harrison
发明人： Roger C. Williamson , James J. Harrison
IPC分类号： C07C5/25 , C07C5/27
CPC分类号： C07C5/2518
摘要： A process for isomerization of vinylidene olefins at least in part to tri-substituted ethylene compound which process comprises contacting an olefinic feedstock, containing mostly vinyl olefins and minor amounts of vinylidene olefins, with a catalyst comprising LZ-Y52 zeolite so as to isomerize the vinylidene olefins to the tri-substituted ethylene compounds without losing substantial amounts of the vinyl olefins to side products. A process is preferably applied to a feedstock such as octene-1 containing 2-ethyl-hexane-1 and the 2-ethyl-hexene-1 is isomerized to 3-methyl-heptene-2 and 3-methyl-heptene-3 while retaining all or most all of the octene-1.
摘要翻译：至少部分地将亚乙烯基烯烃异构化为三取代的乙烯化合物的方法，该方法包括使含有大部分乙烯基烯烃和少量亚乙烯基烯烃的烯烃原料与包含LZ-Y52沸石的催化剂接触，以使亚乙烯基烯烃转化成三取代的乙烯化合物，而不会将大量的乙烯基烯烃丢失到副产物中。一种方法优选应用于含有2-乙基 - 己烷-1的辛烯-1的原料，2-乙基 - 己烯-1异构化为3-甲基 - 庚烯-2和3-甲基 - 庚烯-3，同时保留全部或大部分的辛烯-1。

94. 发明授权

US4462836A Cement composition and method of cement casing in a well 失效
标题翻译：水泥套管在井中的水泥组成和方法
公开(公告)号：US4462836A
公开(公告)日：1984-07-31
申请号：US466550
申请日：1983-02-15
申请人： Wilford S. Baker , James J. Harrison
发明人： Wilford S. Baker , James J. Harrison
IPC分类号： C04B24/38 , C04B28/02 , C09K8/46 , C09K8/487 , C04B7/352 , C04B7/353
CPC分类号： C04B28/02 , C04B24/383 , C09K8/46 , C09K8/487 , C04B2103/46
摘要： A novel cement composition for the preparation of a novel aqueous slurry useful in cementing casing in the borehole of a well comprising (1) cement, (2) (a) a hydroxyethylcellulose ether or (2) (b) a mixture of a hydroxyethylcellulose ether and a hydroxypropylcellulose ether, (3) a polysaccharide produced as a result of microbial action and (4) a dispersant.
摘要翻译：一种新型的水泥组合物，用于制备用于井眼钻井中的固井套管的新型含水浆料，其包括（1）水泥，（2）（a）羟乙基纤维素醚或（2）（b）羟乙基纤维素醚和羟丙基纤维素醚，（3）作为微生物作用的结果产生的多糖和（4）分散剂。

95. 发明授权

US4293502A Nickel ylides 失效
标题翻译：镍叶立德
公开(公告)号：US4293502A
公开(公告)日：1981-10-06
申请号：US179079
申请日：1980-08-18
申请人： David L. Beach , James J. Harrison
发明人： David L. Beach , James J. Harrison
IPC分类号： C07C2/32 , B01J31/00 , B01J31/18 , B01J31/22 , C07B61/00 , C07C1/00 , C07C2/36 , C07C11/02 , C07C67/00 , C07F9/535 , C07F9/54 , C07F9/72 , C07F9/74 , C07F9/90 , C07F9/92 , C07F15/04 , C08F110/02
CPC分类号： C07F9/5407 , B01J31/2247 , C07C2/36 , C07F15/04 , C07F15/045 , C07F9/5352 , C07F9/5442 , C07F9/723 , C07F9/743 , C07F9/904 , C07F9/92 , C08F110/02 , B01J2231/20 , B01J2531/847 , B01J2540/32 , B01J31/1895
摘要： A new group of nickel ylides is provided that is highly active at relatively low operating temperatures and pressures in the oligomerization of ethylene. The compounds can be defined by the following Formula I: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7 and R.sub.8 are either alike or different members selected from the group consisting of hydrogen, alkyl radicals having from about one to about 24 carbon atoms, preferably from about one to about 10 carbon atoms; aryl radicals having from about six to about 20 carbon atoms, preferably from about six to about 10 carbon atoms; alkenyl radicals having from about two to about 30 carbon atoms, preferably from about two to about 20 carbon atoms; cycloalkyl radicals having from about three to about 40 carbon atoms, preferably from about three to about 30 carbon atoms; aralkyl and alkaryl radicals having from about six to about 40 carbon atoms, preferably from about six to about 30 carbon atoms; a halogen radical selected from the group consisting of fluorine, chlorine, bromine and iodine, preferably chlorine; a hydroxyl group; an alkoxy or aryloxy group; and a hydrocarbyl group, such as defined above, carrying halogen, hydroxyl or alkoxy or aryloxy; provided that at least one, preferably from about one to about four, of each of R.sub.1 to R.sub.8 is a sulfonato group (--SO.sub.3.sup.-) or an alkyl, aryl, alkenyl, cycloalkyl, aralkyl or alkaryl group carrying a sulfonato group; M is sulfur or oxygen, preferably oxygen; E is phosphorus, arsenic, antimony or nitrogen, preferably phosphorus; and F is phosphorus, arsenic or antimony, preferably phosphorus.
摘要翻译：提供了一组新的镍内鎓盐，其在乙烯低聚中的相对低的操作温度和压力下具有高活性。化合物可以由下式I定义：其中R 1，R 2，R 3，R 4，R 5，R 6，R 7和R 8为相同或不同的选自氢，具有约一个至约24个碳原子，优选约1至约10个碳原子; 具有约6至约20个碳原子，优选约6至约10个碳原子的芳基; 具有约2至约30个碳原子，优选约2至约20个碳原子的烯基; 具有约3至约40个碳原子，优选约3至约30个碳原子的环烷基; 具有约6至约40个碳原子，优选约6至约30个碳原子的芳烷基和烷芳基; 选自氟，氯，溴和碘的卤素，优选氯; 羟基; 烷氧基或芳氧基; 和如上所定义的含有卤素，羟基或烷氧基或芳氧基的烃基; 条件是R 1至R 8中的至少一个，优选约1至约4个为磺酸基（-SO 3 - ）或带有磺酸基的烷基，芳基，烯基，环烷基，芳烷基或烷芳基; M是硫或氧，优选氧; E是磷，砷，锑或氮，优选磷; F是磷，砷或锑，优选磷。

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