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91. 发明授权

US5347047A Preparation of acylaromatic compounds 失效
标题翻译：酰基芳族化合物的制备
公开(公告)号：US5347047A
公开(公告)日：1994-09-13
申请号：US158776
申请日：1993-12-01
申请人： Wolfgang Siegel , Irene Troetsch-Schaller
发明人： Wolfgang Siegel , Irene Troetsch-Schaller
IPC分类号： B01J23/745 , C07B61/00 , C07C45/45 , C07C45/47 , C07C49/76 , C07C49/784 , C07C49/813 , C07C49/84 , C07C51/373 , C07C59/76 , C07C45/00
CPC分类号： C07C51/373 , C07C45/47 , C07C49/784 , C07C49/813 , C07C49/84
摘要： Acylaromatic compounds are prepared from aromatic compounds and carboxylic acids by reacting the starting compounds with phosgene in the presence of an aliphatic phosphine oxide or of an N,N-dialkylformamide and of an Fe(II), Fe(III) or Zn(II) compound.
摘要翻译：芳族化合物由芳族化合物和羧酸通过在脂族氧化膦或N，N-二烷基甲酰胺和Fe（II），Fe（III）或Zn（II））存在下使起始化合物与光气反应制备，复合。

92. 发明授权

US4478517A Process and gravity feed mixer for mixing bulk materials in a container 失效
标题翻译：用于在容器中混合散装材料的工艺和重力进料混合器
公开(公告)号：US4478517A
公开(公告)日：1984-10-23
申请号：US408197
申请日：1982-08-13
申请人： Hans Hoppe , Helmut Bercx , Wolfgang Siegel
发明人： Hans Hoppe , Helmut Bercx , Wolfgang Siegel
IPC分类号： B01F5/24 , B01F13/02 , B65G65/36
CPC分类号： B01F5/243 , B01F13/0244 , B65G65/365
摘要： The gravity feed mixing of bulk materials is effected by removing partial quantities of the material at each of a plurality of vertically disposed levels, and passing the removed material through a series of funnels arranged vertically so that the material is admixed with the material passing from a higher level and fed to a lower level.
摘要翻译：散装材料的重力进料混合是通过在多个垂直设置的水平的每一个处去除部分量的材料并使被去除的材料通过垂直布置的一系列漏斗来实现的，使得材料与从更高水平，并进入较低水平。

93. 发明授权

US08921598B2 Method for producing urethanes composed of mono and di-functional aromatic amines 有权
标题翻译：用于制备由单官能和二官能芳族胺组成的聚氨酯的方法
公开(公告)号：US08921598B2
公开(公告)日：2014-12-30
申请号：US12918617
申请日：2009-03-18
申请人： Andreas Leitner , Robert Baumann , Wolfgang Siegel
发明人： Andreas Leitner , Robert Baumann , Wolfgang Siegel
IPC分类号： C07C231/02 , C07C269/04 , C07C271/28
CPC分类号： C07C269/04 , C07C271/28
摘要： The object of the invention is to provide a process for preparing urethanes by reacting aromatic amines with a dialkyl carbonate, wherein the alkyl radical of the organic dialkyl carbonate comprises from 2 to 18 carbon atoms, and the reaction is carried out in the presence of a base.
摘要翻译：本发明的目的是提供一种通过使芳族胺与碳酸二烷基酯反应制备氨基甲酸酯的方法，其中有机碳酸二烷基酯的烷基包含2至18个碳原子，反应在基础。

94. 发明授权

US08415500B2 One-stage reductive amination 失效
标题翻译：一步还原胺化
公开(公告)号：US08415500B2
公开(公告)日：2013-04-09
申请号：US12808268
申请日：2008-12-10
申请人： Tobias Staeb , Thilo Hahn , Wolfgang Siegel
发明人： Tobias Staeb , Thilo Hahn , Wolfgang Siegel
IPC分类号： C07C211/27 , C07C209/62
CPC分类号： C07C209/26 , C07B2200/07 , C07C209/62 , C07C211/07 , C07C211/27
摘要： A process for preparing amines of the formula I, by reacting a carbonyl compound of the formula II with an amine of the formula III where R1 and R2 are different and are each an organic radical which has from 1 to 20 carbon atoms and may optionally also comprise heteroatoms, R3 is a C1-C6-alkyl group and R4 is an aryl group which may be partly or fully halogenated and/or may bear from one to three radicals from the group of cyano, nitro, C1-C6-alkyl, C1-C6-haloalkyl, hydroxyl, C1-C6-hydroxyalkyl, C1-C6-alkoxy, C1-C6-haloalkoxy, hydroxycarbonyl, C1-C6-alkoxycarbonyl, C1-C6-alkylamino, di(C1-C6-alkyl)amino, aryl and aryl(C1-C6-alkyl); and * represents the S or R configuration, and ** represents the S and/or R configuration; which comprises performing the reaction in the presence of a heterogeneous imination catalyst, of a hydrogenation catalyst and of hydrogen.
摘要翻译：一种制备式I的胺的方法，通过使式II的羰基化合物与式III的胺反应，其中R 1和R 2不同，并且各自是具有1至20个碳原子的有机基团，包括杂原子，R 3是C 1 -C 6烷基，R 4是可以部分或完全卤化的和/或可以从氰基，硝基，C 1 -C 6 - 烷基，C 1〜 C 1 -C 6 - 卤代烷基，羟基，C 1 -C 6羟基烷基，C 1 -C 6 - 烷氧基，C 1 -C 6 - 卤代烷氧基，羟基羰基，C 1 -C 6 - 烷氧基羰基，C 1 -C 6烷基氨基，和芳基（C 1 -C 6 - 烷基）; 和*表示S或R构型，**表示S和/或R构型; 其包括在非均相模拟催化剂，氢化催化剂和氢气存在下进行反应。

95. 发明申请

US20110171700A1 METHOD FOR PRODUCING L-PHENYLEPHRINE USING AN ALCOHOL DEHYDROGENASE OF AROMATOLEUM AROMATICUM EBN1 (AZOARCUS SP. EBN1) 有权
标题翻译：使用芳香木香酚EBN1（AZOARCUS SP.EBN1）的酒精脱氢酶生产L-苯丙胺的方法
公开(公告)号：US20110171700A1
公开(公告)日：2011-07-14
申请号：US13063630
申请日：2009-09-15
申请人： Michael Breuer , Andreas Pletsch , Bernhard Hauer , Wolfgang Siegel
发明人： Michael Breuer , Andreas Pletsch , Bernhard Hauer , Wolfgang Siegel
IPC分类号： C12P13/00 , C07C45/63 , C12P7/22
CPC分类号： C12P13/001 , C12P7/22
摘要： The present invention relates to a multi-stage process for producing substituted, optically active alcohols, comprising an enzyme-catalyzed synthesis step, in particular a synthesis step which is catalyzed by an alcohol dehydrogenase. The inventive method is particularly suitable for producing phenylephrine, i.e. 3-[(1R)-1-hydroxy-2-methylamino-ethyl]-phenol.
摘要翻译：本发明涉及一种制备取代的光学活性醇的多阶段方法，其包括酶催化的合成步骤，特别是由醇脱氢酶催化的合成步骤。本发明的方法特别适用于生产去氧肾上腺素，即3 - [（1R）-1-羟基-2-甲基氨基 - 乙基] - 苯酚。

96. 发明申请

US20110015424A1 METAL CARBAMATES FORMED FROM DIAMINOPHENYLMETHANE 失效
标题翻译：由二氨基苯甲醛形成的金属碳酸盐
公开(公告)号：US20110015424A1
公开(公告)日：2011-01-20
申请号：US12918931
申请日：2009-03-18
申请人： Andreas Leitner , Robert Baumann , Wolfgang Siegel
发明人： Andreas Leitner , Robert Baumann , Wolfgang Siegel
IPC分类号： C07C271/28 , C07C269/04
CPC分类号： C07C269/06 , C07C271/28
摘要： The invention provides metal carbamates of the general formula (I) where R1 and R2 are each an alkyl group.
摘要翻译：本发明提供通式（I）的金属氨基甲酸酯，其中R 1和R 2各自为烷基。

97. 发明申请

US20100274054A1 ONE-STAGE REDUCTIVE AMINATION 失效
标题翻译：一级减少化学
公开(公告)号：US20100274054A1
公开(公告)日：2010-10-28
申请号：US12808268
申请日：2008-12-10
申请人： Tobias Staeb , Thilo Hahn , Wolfgang Siegel
发明人： Tobias Staeb , Thilo Hahn , Wolfgang Siegel
IPC分类号： C07C211/27 , C07C209/62
CPC分类号： C07C209/26 , C07B2200/07 , C07C209/62 , C07C211/07 , C07C211/27
摘要： A process for preparing amines of the formula I, by reacting a carbonyl compound of the formula II with an amine of the formula III where R1 and R2 are different and are each an organic radical which has from 1 to 20 carbon atoms and may optionally also comprise heteroatoms, R3 is a C1-C6-alkyl group and R4 is an aryl group which may be partly or fully halogenated and/or may bear from one to three radicals from the group of cyano, nitro, C1-C6-alkyl, C1-C6-haloalkyl, hydroxyl, C1-C6-hydroxyalkyl, C1-C6-alkoxy, C1-C6-haloalkoxy, hydroxycarbonyl, C1-C6-alkoxycarbonyl, C1-C6-alkylamino, di(C1-C6-alkyl)amino, aryl and aryl(C1-C6-alkyl); and * represents the S or R configuration, and ** represents the S and/or R configuration; which comprises performing the reaction in the presence of a heterogeneous imination catalyst, of a hydrogenation catalyst and of hydrogen.
摘要翻译：一种制备式I的胺的方法，通过使式II的羰基化合物与式III的胺反应，其中R 1和R 2不同，并且各自是具有1至20个碳原子的有机基团，包括杂原子，R 3是C 1 -C 6烷基，R 4是可以部分或完全卤化的和/或可以从氰基，硝基，C 1 -C 6 - 烷基，C 1〜 C 1 -C 6 - 卤代烷基，羟基，C 1 -C 6羟基烷基，C 1 -C 6 - 烷氧基，C 1 -C 6 - 卤代烷氧基，羟基羰基，C 1 -C 6 - 烷氧基羰基，C 1 -C 6烷基氨基，和芳基（C 1 -C 6 - 烷基）; 和*表示S或R构型，**表示S和/或R构型; 其包括在非均相模拟催化剂，氢化催化剂和氢气存在下进行反应。

98. 发明授权

US07777068B2 Ni(0) -containing catalyst system 有权
标题翻译：含Ni（0）的催化剂体系
公开(公告)号：US07777068B2
公开(公告)日：2010-08-17
申请号：US11860972
申请日：2007-09-25
申请人： Michael Bartsch , Robert Baumann , Dagmar Pascale Kunsmann-Keitel , Gerd Haderlein , Tim Jungkamp , Marco Altmayer , Wolfgang Siegel
发明人： Michael Bartsch , Robert Baumann , Dagmar Pascale Kunsmann-Keitel , Gerd Haderlein , Tim Jungkamp , Marco Altmayer , Wolfgang Siegel
IPC分类号： C07C255/01
CPC分类号： B01J31/185 , B01J23/755 , B01J31/1865 , B01J31/1875 , B01J2231/323 , B01J2531/847 , C07C253/10 , C07C255/07 , C07C255/04
摘要： A system comprising a) Ni(0) b) from 4 to 10 mol per mol of Ni(0) in a) of a compound (I) of the formula P(X1R1)(X2R2)(X3R3) (I) where X1, X2, X3 are each, independently of one another, oxygen or a single bond, R1, R2, R3 are, independently of one another, identical or different organic radicals and c) from 1 to 4 mol per mol of Ni(0) in a) of a compound (II) of the formula where X11, X12, X13 X21, X22, X23 are each, independently of one another, oxygen or a single bond, R11, R12 are identical or different, individual or bridged organic radicals, R21, R22 are identical or different, individual or bridged organic radicals and Y is a bridging group is suitable as catalyst for preparing mixtures of monoolefinic C5 mononitriles having nonconjugated C═C and C═N bonds by hydrocyanation of a 1,3-butadiene-containing hydrocarbon mixture and for preparing a dinitrile by hydrocyanation of a mixture of monoolefinic C5 mononitriles having nonconjugated C═C and C═N bonds.
摘要翻译：一种系统，其包含a）式（I）化合物（I）的式（I）化合物（I）中的每摩尔Ni（0）的每摩尔Ni（0）的Ni（0）b）4至10摩尔（X 2 R 2）（X 3 R 3），X2，X3各自独立地为氧或单键，R 1，R 2，R 3彼此独立地为相同或不同的有机基团，c）每摩尔Ni（0）为1〜4摩尔，其中X 11，X 12，X 13 X 21，X 22，X 23各自独立地为氧或单键，R 11，R 12相同或不同，单个或桥接的有机基团 R21，R22相同或不同，单个或桥接的有机基团和Y是桥连基团，适合作为具有非共轭C = C和C = N键的单烯烃C5单腈混合物的催化剂，通过1,3-丁二烯的氢氰化的含烃混合物，并通过氢化氰化得到具有非共轭C = C和C = N键的单烯烃C5单腈混合物来制备二腈。

99. 发明授权

US07767852B2 Method for the separation of acids from chemical reaction mixtures by means of ionic fluids 有权
标题翻译：通过离子液体从化学反应混合物中分离酸的方法
公开(公告)号：US07767852B2
公开(公告)日：2010-08-03
申请号：US10500145
申请日：2003-01-21
申请人： Martin Volland , Verena Seitz , Matthias Maase , Miguel Flores , Rainer Papp , Klemens Massonne , Veit Stegmann , Klaus Halbritter , Ralf Noe , Michael Bartsch , Wolfgang Siegel , Michael Becker , Oliver Huttenloch
发明人： Martin Volland , Verena Seitz , Matthias Maase , Miguel Flores , Rainer Papp , Klemens Massonne , Veit Stegmann , Klaus Halbritter , Ralf Noe , Michael Bartsch , Wolfgang Siegel , Michael Becker , Oliver Huttenloch
IPC分类号： C07F9/02
CPC分类号： C07C403/12 , C07C1/30 , C07C45/50 , C07C51/412 , C07C51/58 , C07C67/14 , C07C2531/02 , C07C2601/16 , C07D295/185 , C07D317/36 , C07F9/142 , C07F9/145 , C07F9/46 , C07F9/4841 , C07F9/52 , C07F9/572 , C07F9/5728 , C07F9/65038 , C07F9/65746 , C07F9/65848 , C07C47/02 , C07C13/23 , C07C69/78 , C07C69/24 , C07C69/14 , C07C53/10
摘要： Process for preparing aminodihalophosphines, diaminohalophosphines, triaminophosphines, phosphorous ester diamides, aminophosphines, diaminophosphines, phosphorous ester amide halides and aminophosphine halides with elimination of an acid in the presence of an auxiliary base, wherein the auxiliary base b) and the acid form a salt which is liquid at temperatures at which the desired product is not significantly decomposed during the process of separating off the liquid salt and c) the salt of the auxiliary base forms two immiscible liquid phases with the desired product or the solution of the desired product in a suitable solvent.
摘要翻译：在辅助碱存在下，除去酸以制备氨基二卤代膦，二氨基卤代膦，三氨基膦，亚磷酰胺，氨基膦，二氨基膦，磷酰胺卤化物和氨基膦卤化物的方法，其中辅助碱b）和酸形成盐在分离液体盐的过程中期望产物没有显着分解的温度下是液体的，c）辅助碱的盐与所需产物或所需产物的溶液形成两个不混溶的液相，溶剂。

100. 发明授权

US07695011B2 Airbag arrangement for a motor vehicle 失效
标题翻译：汽车安全气囊安排
公开(公告)号：US07695011B2
公开(公告)日：2010-04-13
申请号：US12155735
申请日：2008-06-09
申请人： Wolfgang Siegel
发明人： Wolfgang Siegel
IPC分类号： B60R21/26 , B60R21/213
CPC分类号： B60R21/231 , B60R21/217 , B60R2021/23123 , B60R2021/2617
摘要： An airbag can include a covering that surrounds an interior space that can be filled with gas, a gas-conducting pipe which is stretched longitudinally along a direction of extent, and a contact region of the covering that surrounds the inflow opening and encloses the gas-conducting pipe in a sealing manner along a circumferential direction of the gas-conducting pipe that encircles the direction of extent. A protective layer of the covering can be arranged, at least in some sections in the interior space of the covering, with respect to the gas-conducting pipe so that damage to the covering during filling of the interior space of the covering with hot gas can be prevented by the protective layer. At least one fastening region of the protective layer, via which the protective layer can be connected to the covering, can be connected to the contact region of the covering.
摘要翻译：安全气囊可以包括围绕可填充有气体的内部空间的覆盖物，沿着方向纵向拉伸的导气管和围绕流入开口的覆盖物的接触区域，沿导气管的圆周方向以密封方式导管，该导气管围绕该方向。覆盖物的保护层至少在覆盖物的内部空间的一些部分中相对于导气管布置，使得在用热气体填充覆盖物的内部空间期间对覆盖物的损坏可以被保护层防止。保护层的至少一个固定区域，保护层可以通过该紧固区域连接到覆盖物上，可以连接到覆盖物的接触区域。

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