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91. 发明授权

US08940658B2 Catalyst for producing unsaturated carboxylic acid and a process for producing unsaturated carboxylic acid using the catalyst 有权
标题翻译：用于制备不饱和羧酸的催化剂和使用该催化剂生产不饱和羧酸的方法
公开(公告)号：US08940658B2
公开(公告)日：2015-01-27
申请号：US13990513
申请日：2011-09-26
申请人： Toshiya Nishiguchi
发明人： Toshiya Nishiguchi
IPC分类号： B01J27/228 , B01J35/06 , B01J23/00 , B01J23/28 , B01J23/887 , B01J23/888 , B01J35/02 , B01J37/02 , C07C51/235 , C07C51/25
CPC分类号： B01J27/228 , B01J23/002 , B01J23/28 , B01J23/8877 , B01J23/8885 , B01J35/023 , B01J35/06 , B01J37/0221 , B01J2523/00 , C07C51/235 , C07C51/252 , B01J2523/17 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/68 , B01J2523/69 , B01J2523/845 , C07C57/04
摘要： Provided is a catalyst for producing unsaturated carboxylic acid, which excels in mechanical strength and attrition loss and is capable of producing the object product at a high yield. This catalyst is formed of a catalytically active component comprising molybdenum and vanadium as the essential ingredients and inorganic fibers, which are supported on an inert carrier, said catalyst being characterized in that said inorganic fibers comprise at least an inorganic fiber having an average diameter less than 1.0 μm and another inorganic fiber having an average diameter ranging from 1.5 to 7 μm.
摘要翻译：提供了用于制备不饱和羧酸的催化剂，其机械强度和磨损损失优异，并且能够以高产率生产目标产物。该催化剂由负载在惰性载体上的以钼和钒为主要成分的催化活性组分和无机纤维形成，所述催化剂的特征在于，所述无机纤维至少包含平均直径小于 1.0μm的平均直径为1.5〜7μm的无机纤维。

92. 发明授权

US08926930B2 Alkali metal salt of fluorosulfonyl imide, and production method therefor 有权
公开(公告)号：US08926930B2
公开(公告)日：2015-01-06
申请号：US13700364
申请日：2011-05-27
申请人： Yuichi Sato , Shimpei Sato , Yasunori Okumura
发明人： Yuichi Sato , Shimpei Sato , Yasunori Okumura
IPC分类号： H01G9/02 , H01M10/0568 , H01M10/052 , H01G9/035 , C01B21/086 , C01B21/093 , B01D3/34 , B01D1/22
摘要： The present invention provides an alkali metal salt of fluorosulfonyl imide having favorable heat resistance and a reduced content of specific impurities and a water content, and provides a method for producing an alkali metal salt of fluorosulfonyl imide, which is capable of easily removing a solvent from a reaction solution. An alkali metal salt of fluorosulfonyl imide of the present invention is represented by the following general formula (I) and has a mass loss rate of 2% or less when the alkali metal salt of fluorosulfonyl imide is kept at 100° C. for 8 hours under an air current. A method for producing an alkali metal salt of fluorosulfonyl imide of the present invention comprises a step of concentrating a solution of the alkali metal salt of fluorosulfonyl imide by bubbling a gas into a reaction solution containing the alkali metal salt of fluorosulfonyl imide, and/or concentrating a solution of the alkali metal salt of fluorosulfonyl imide by thin layer distillation.

93. 发明授权

US08921584B2 Composition containing intermediate for water-soluble monomer and process for production thereof, composition containing water-soluble monomer, intermediate for water-soluble monomer, and water-soluble monomer and process for production thereof 有权
标题翻译：含有水溶性单体的中间体的组合物及其制造方法，含有水溶性单体的组合物，水溶性单体的中间体和水溶性单体及其制造方法
公开(公告)号：US08921584B2
公开(公告)日：2014-12-30
申请号：US13512845
申请日：2010-12-03
申请人： Atsuro Yoneda , Makoto Saito , Aki Tsukajima , Daisuke Michitaka , Mitsuaki Makino
发明人： Atsuro Yoneda , Makoto Saito , Aki Tsukajima , Daisuke Michitaka , Mitsuaki Makino
IPC分类号： C07C43/188 , C07C43/178 , C11D3/37 , C08F216/14 , C07C217/28 , C08F216/12 , C08F290/06 , C07D303/24 , C07D303/22 , C07D303/20 , C02F1/28
CPC分类号： C07C43/178 , C02F1/285 , C07C43/188 , C07C217/28 , C07D303/20 , C07D303/22 , C07D303/24 , C08F216/125 , C08F216/1416 , C08F290/062 , C11D3/3746 , C11D3/3757
摘要： A composition is provided that contains an intermediate for a water-soluble monomer, wherein this intermediate is suitable for producing a water-soluble polyalkylene glycol-type monomer that has a polymerizable terminal double bond, and suitable for the production of water-soluble polymer, and moreover allows the high-yield production of water-soluble polymer. A process of producing this composition and a water-soluble monomer-containing composition obtained therefrom are also provided. A water-soluble monomer is also provided that can be used as a starting material for a water-soluble polymer that even at high hardnesses exhibits an excellent capacity to capture metal ions such as the calcium ion and magnesium ion, an excellent anti-gelation performance, an excellent anti-soil redeposition performance, a better anti-dye transfer performance than in the past, and also an excellent compatibility with surfactants. A production process is also provided that can produce such a water-soluble monomer at higher yields and higher selectivities (higher purities) than in the past. A composition containing an intermediate for a water-soluble monomer, that contains a compound (A) having a specified structure and that contains a specified amount of a compound (B) having a specified structure. Also, a water-soluble monomer having a specified structure is provided.
摘要翻译：提供了含有水溶性单体中间体的组合物，其中该中间体适用于生产具有可聚合端基双键的水溶性聚亚烷基二醇型单体，适用于生产水溶性聚合物，而且允许高产量生产水溶性聚合物。还提供了制备该组合物的方法和由其获得的含水溶性单体的组合物。还提供了可用作水溶性聚合物的起始材料的水溶性单体，即使在高硬度下也显示出优异的俘获金属离子的能力，例如钙离子和镁离子，优异的抗胶凝性能，优异的抗土壤再沉积性能，比过去更好的抗染料转移性能，以及与表面活性剂的优异相容性。还提供了一种生产方法，其可以以比过去更高的产率和更高的选择性（更高的纯度）生产这种水溶性单体。含有水溶性单体中间体的组合物，其含有具有规定结构且含有规定量的具有规定结构的化合物（B）的化合物（A）。另外，提供具有特定结构的水溶性单体。

94. 发明授权

US08916678B2 Polyalkylene glycol monomer, polyalkylene glycol polymer containing the same, and application thereof 有权
标题翻译：聚亚烷基二醇单体，含有它们的聚亚烷基二醇聚合物及其应用
公开(公告)号：US08916678B2
公开(公告)日：2014-12-23
申请号：US12088629
申请日：2006-09-26
申请人： Atsuro Yoneda , Akiko Hemmi
发明人： Atsuro Yoneda , Akiko Hemmi
IPC分类号： C08G65/04 , C08L51/08 , C11D3/37 , B01F17/00 , C08F290/06 , C04B24/26 , C11D3/00 , C04B24/16 , C08F283/06 , C04B24/32 , C08G65/26
CPC分类号： C08F283/065 , B01F17/0028 , C04B24/161 , C04B24/2605 , C04B24/32 , C08F290/06 , C08F290/062 , C08G65/2609 , C08L51/08 , C11D3/0036 , C11D3/3746 , C08L2666/02
摘要： To provide: a monomer having a polyalkylene glycol chain preferably used in various industrial applications such as detergent builder compositions for clothes and bodies, water-treatment agents, and pigment dispersants; and a polyalkylene glycol polymer using such a monomer as a raw material. A polyalkylene glycol monomer having a polymerizable double bond and a polyalkylene glycol chain, wherein the polyalkylene glycol monomer has a hydrophobic part in the polyalkylene glycol chain and/or at a terminal of the chain, and the polymerizable double bond is derived from allyl glycidyl ether, and a polyalkylene glycol monomer having a monomer unit derived from the above-mentioned polyalkylene glycol monomer, wherein the polyalkylene glycol polymer is a polyalkylene glycol polymer having a carboxylic acid group and/or a sulfonic acid group.
摘要翻译：提供：具有优选用于各种工业应用的聚亚烷基二醇链的单体，例如用于衣服和身体的洗涤剂助洗剂组合物，水处理剂和颜料分散剂; 和使用这种单体作为原料的聚亚烷基二醇聚合物。具有可聚合双键和聚亚烷基二醇链的聚亚烷基二醇单体，其中聚亚烷基二醇单体在聚亚烷基二醇链中和/或末端具有疏水部分，并且可聚合双键衍生自烯丙基缩水甘油醚和具有源自上述聚亚烷基二醇单体的单体单元的聚亚烷基二醇单体，其中聚亚烷基二醇聚合物是具有羧酸基和/或磺酸基的聚亚烷基二醇聚合物。

95. 发明授权

US08877962B2 Manufacturing method for sulfonic acid group-containing ether compound 有权
公开(公告)号：US08877962B2
公开(公告)日：2014-11-04
申请号：US14304382
申请日：2014-06-13
申请人： Nippon Shokubai Co, Ltd
发明人： Masato Nakano , Akihiko Kanzaki , Takahiro Tsumori
IPC分类号： C07C309/00 , C07C309/20
CPC分类号： C07C309/20 , C07C303/02 , C07C309/09 , C08F216/1466
摘要： The present invention provides a method for efficiently producing a sulfonic acid group-containing ether compound having a high purity and a good polymerizability while preventing production of a byproduct, and provides a sulfonic acid group-containing ether compound containing fewer impurities and having a good radical (co)polymerizability.The present invention provides a method of producing a sulfonic acid group-containing ether compound by reacting a sulfurous acid compound with a compound represented by the formula (1): wherein R1 represents a single bond, a CH2 group, or a CH2CH2 group, and R2 represents H, or a CH3 group, the method comprising the steps of: adjusting pH of a reaction system to 5.5 or greater with use of an alkaline substance; and adding the compound represented by the formula (1) to a reaction vessel containing the sulfurous acid compound.

96. 发明授权

US08875415B2 Method for drying granular water-containing gel-like cross-linked polymer 有权
标题翻译：颗粒状含水凝胶状交联聚合物的干燥方法
公开(公告)号：US08875415B2
公开(公告)日：2014-11-04
申请号：US13583144
申请日：2011-03-07
申请人： Yoshio Irie
发明人： Yoshio Irie
IPC分类号： C08F6/06 , C08F6/00 , B01J2/26 , C08L33/02 , C08F22/02 , B01D1/24 , A61L15/22 , A61L15/60 , C08J3/12
CPC分类号： C08F6/008 , A61L15/22 , A61L15/60 , B01D1/24 , B01J2/26 , C08F22/02 , C08J3/12 , C08J2300/14 , C08L33/02 , C08L33/06
摘要： The present invention is to provide a drying method by which both cost reduction and superior physical properties can be attained in a step which comprises subjecting a water-containing gel-like crosslinked polymer obtained by polymerizing an aqueous monomer solution to fine granulation during or after the polymerization, and drying the resultant particulate water-containing gel-like crosslinked polymer with a through-circulation band dryer. The method has a feature in that the drying conditions over a period from a time of introducing the particulate water-containing gel-like crosslinked polymer into a drying zone of the through-circulation band dryer to a time of reaching a solid content concentration thereof to 80% by weight, satisfy that (1) a difference of temperature between a temperature of hot air blown to a particulate hydrogel layer and a temperature measured after the hot air passes through the particulate hydrogel layer is 20 to 70° C.
摘要翻译：本发明提供一种干燥方法，其可以在以下步骤中实现成本降低和物理性能优异的步骤：将含有单体溶液聚合得到的含水凝胶状交联聚合物在聚合，并用通过循环带式干燥器干燥得到的含颗粒状含水凝胶状交联聚合物。该方法的特征在于，在将含颗粒状含水凝胶状交联聚合物引入通循环带式干燥机的干燥区域到达固体成分浓度的时间的期间内的干燥条件为 80重量％，满足以下（1）吹送到颗粒状水凝胶层的热空气的温度与热空气通过颗粒状水凝胶层后测量的温度之间的温度差为20〜70℃。

97. 发明授权

US08859809B2 Device and process for crystallizing (meth)acrylic acid 有权
标题翻译：用于结晶（甲基）丙烯酸的装置和方法
公开(公告)号：US08859809B2
公开(公告)日：2014-10-14
申请号：US13381449
申请日：2010-06-24
申请人： Kazuhiko Sakamoto , Koji Ueno , Yoshitake Ishii , Masatsugu Kitaura
发明人： Kazuhiko Sakamoto , Koji Ueno , Yoshitake Ishii , Masatsugu Kitaura
IPC分类号： C07C51/42 , B01D9/00 , C07C51/43
CPC分类号： B01D9/0013 , B01D9/0063 , C07C51/43 , C07C57/04
摘要： A crystallization device and a crystallization process are provided for obtaining (meth)acrylic acid with higher purity without causing leakage of a crude solution by preventing complete clogging in a crystallization tube from occurring. The device for crystallizing (meth)acrylic acid includes a crude (meth)acrylic acid solution supply part, a crystallization tube, a heat medium supply tube, a heat medium discharge tube, a storage part of a crude (meth)acrylic acid solution passed through the crystallization tube, a tube for circulating and supplying the crude (meth)acrylic acid solution to the supply part from the storage part, and a pump for circulating and supplying the crude (meth)acrylic acid solution to the supply part from the storage part, and also includes a pressure meter in the circulate-supply tube. The device is used for carrying out dynamic crystallization in a batch manner by circulating the crude (meth)acrylic acid solution to flow the crude solution downward along the inner wall of the crystallization tube in a coating film-like state.
摘要翻译：提供了一种结晶装置和结晶方法，用于获得高纯度的（甲基）丙烯酸，而不会通过防止结晶管中发生完全堵塞而导致粗溶液泄漏。用于结晶（甲基）丙烯酸的装置包括粗（甲基）丙烯酸溶液供应部分，结晶管，热介质供应管，热介质放电管，粗（甲基）丙烯酸溶液的储存部分通过通过结晶管，将来自储存部的粗（甲基）丙烯酸溶液循环供给到供给部的管，以及从储存部向供给部循环供给粗（甲基）丙烯酸溶液的泵并且还包括在循环供应管中的压力计。该装置用于以分批方式进行动态结晶，通过循环粗制（甲基）丙烯酸溶液使涂料膜状态沿着结晶管的内壁向下流动粗溶液。

98. 发明授权

US08859685B2 Polyacrylic acid (salt)-type water absorbent resin and method for producing of same 有权
标题翻译：聚丙烯酸（盐）型吸水性树脂及其制造方法
公开(公告)号：US08859685B2
公开(公告)日：2014-10-14
申请号：US13392214
申请日：2010-08-27
申请人： Kozo Nogi , Kunihiko Ishizaki , Kazumasa Konishi
发明人： Kozo Nogi , Kunihiko Ishizaki , Kazumasa Konishi
IPC分类号： C08F20/06 , C08J3/24 , C08F8/30 , C08F8/42 , A61L15/60 , C08F220/06 , C08F120/06 , A61L15/24
CPC分类号： A61L15/24 , A61L15/60 , C08F120/06 , C08F220/06 , C08J3/24 , C08J3/245 , C08J2300/14 , C08J2333/02 , C08L33/08 , C08F2222/1013
摘要： A process for producing a water absorbent resin is provided with which it is possible to efficiently and inexpensively obtain a surface-crosslinked water-absorbing resin having excellent material properties, while ensuring high productivity. In continuous production scaled up to a large scale (in particular, 1 t/hr or more), the physical properties are improved and stabilized (for example, a reduction in standard deviation of the physical properties) by a surface crosslinking treatment to further improve absorption against pressure (AAP) and saline flow conductivity (SFC). The process for producing a polyacrylic acid (salt)-type water absorbent resin includes a surface treatment step in which after addition of a surface-crosslinking agent, a crosslinking reaction is conducted in a transverse type continuous stirring apparatus having stirring means including a feeding inlet and a discharging outlet of a water absorbent resin and one or more rotary shafts having with a plurality of stirring discs, and heating means, at a stirring-power index of the device of 3-15 W·hr/kg. (Stirring-power index)=((power consumption of apparatus at the time surface treatment)−(power consumption at the time of idling))×average retention time)/(treatment amount per unit time×average retention time).
摘要翻译：提供一种生产吸水性树脂的方法，其可以有效且廉价地获得具有优异材料性能的表面交联吸水性树脂，同时确保高生产率。在大规模（特别是1t / hr以上）的连续生产中，物理性能通过表面交联处理得到改善和稳定（例如物理性能的标准偏差的降低），以进一步改善吸收抗压力（AAP）和盐水流动电导率（SFC）。制备聚丙烯酸（盐）型吸水性树脂的方法包括表面处理步骤，其中加入表面交联剂后，在具有搅拌装置的横向连续搅拌装置中进行交联反应，所述搅拌装置包括进料口以及具有多个搅拌盘的吸水性树脂的排出口和具有多个搅拌盘和加热装置的装置的搅拌功率指数为3-15W·hr / kg的一个或多个旋转轴。（搅拌功率指数）=（（表面处理时的设备的功率消耗） - （怠速时的功耗）×平均保持时间）/（每单位时间处理量×平均保持时间）。

99. 发明授权

US08846148B2 Composition for chemical vapor deposition film-formation and method for production of low dielectric constant film 有权
标题翻译：用于化学气相沉积膜形成的组合物和用于制备低介电常数膜的方法
公开(公告)号：US08846148B2
公开(公告)日：2014-09-30
申请号：US12084568
申请日：2006-11-15
申请人： Teruhiko Kumada , Hideharu Nobutoki , Naoki Yasuda , Tetsuya Yamamoto , Yasutaka Nakatani , Takuya Kamiyama
发明人： Teruhiko Kumada , Hideharu Nobutoki , Naoki Yasuda , Tetsuya Yamamoto , Yasutaka Nakatani , Takuya Kamiyama
IPC分类号： C23C16/00 , C07F5/02 , C23C16/30 , H01L21/314 , C23C16/34 , H01L21/318
CPC分类号： C23C16/342 , C07F5/02 , C23C16/30 , H01L21/314 , H01L21/318
摘要： A composition for chemical vapor deposition film-formation comprising a borazine compound represented by the Chemical Formula 1 satisfying at least one of a condition that content of each halogen atom in the composition is 100 ppb or less or a condition that content of each metal element in the composition is 100 ppb or less. In the Chemical Formula 1, R1 may be the same or different, and is hydrogen atom, alkyl group, alkenyl group or alkynyl group, and at least one thereof is hydrogen atom; R2 may be the same or different, and is hydrogen atom, alkyl group, alkenyl group or alkynyl group, and at least one thereof is alkyl group, alkenyl group or alkynyl group.
摘要翻译：一种用于化学气相沉积膜形成的组合物，其包含由化学式1表示的环硼氮烷化合物，其满足组合物中每个卤素原子的含量为100ppb以下的条件中的至少一种或每种金属元素的含量组合物为100ppb以下。在化学式1中，R 1可以相同或不同，为氢原子，烷基，链烯基或炔基，其中至少一个为氢原子; R2可以相同或不同，为氢原子，烷基，烯基或炔基，其中至少一个为烷基，烯基或炔基。

100. 发明授权

US08824047B2 Polarizing plate, optical film and image display 有权
标题翻译：偏光板，光学膜和图像显示
公开(公告)号：US08824047B2
公开(公告)日：2014-09-02
申请号：US12682607
申请日：2008-10-21
申请人： Naoki Tomoguchi , Youichirou Sugino , Nobuaki Iwamoto , Megumi Katou
发明人： Naoki Tomoguchi , Youichirou Sugino , Nobuaki Iwamoto , Megumi Katou
IPC分类号： G02B5/30 , G02F1/1335 , G02B1/10
CPC分类号： G02B5/3033 , G02B1/105 , G02B1/14 , Y10T428/25
摘要： A polarizing plate of the present invention includes a polyvinyl alcohol-based polarizer and transparent protective films provided on both sides of the polarizer with an adhesive layer interposed between the polarizer and each transparent protective film, wherein the transparent protective films each comprise a lactone ring structure-containing (meth)acrylic resin, each one of the transparent protective films has a thickness T1 (μm) of 10 to 35 μm, and the polarizer has a thickness T2 (μm) which satisfies that the ratio (T2/T1) of T2 to the thickness T1 of each one of the transparent protective films falls within the range of 0.8 to 1.8. The polarizing plate is designed to be thin and can satisfy durability.
摘要翻译：本发明的偏振片包括聚偏乙烯醇系偏振片和透明保护膜，该透明保护膜设置在偏振片的两面，夹着偏光板与透明保护膜之间的粘接层，透明保护膜各自包含内酯环结构（甲基）丙烯酸树脂，每个透明保护膜的厚度T1（μm）为10〜35μm，偏振片的厚度T2（μm）满足T2（T2）/ T2 每个透明保护膜的厚度T1落在0.8至1.8的范围内。偏振片设计薄，可以满足耐用性。

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