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1. 发明授权

US06436541B1 Conductive antireflective coatings and methods of producing same 有权
标题翻译：导电抗反射涂层及其制造方法
公开(公告)号：US06436541B1
公开(公告)日：2002-08-20
申请号：US09287305
申请日：1999-04-07
申请人： John F. Sopko , Michael O. Okoroafor , Huawen Li , George A. Neuman
发明人： John F. Sopko , Michael O. Okoroafor , Huawen Li , George A. Neuman
IPC分类号： B32B900
CPC分类号： G02B1/116 , G02B1/16 , Y10T428/24942 , Y10T428/24975 , Y10T428/265
摘要： This invention relates to a two layers or more anti-static film coating deposited on a substrate. Selected layers of the films may have anti-static and/or electromagnetic properties. In one embodiment, the film farthest from the substrate has an index of refraction lower than the underlying film. In another embodiment, the surface of the film is roughened to provide a graded index of refraction.
摘要翻译：本发明涉及沉积在基底上的两层或多层抗静电膜涂层。所选择的膜层可具有抗静电和/或电磁特性。在一个实施例中，距衬底最远的膜的折射率低于下面的膜。在另一个实施例中，膜的表面被粗糙化以提供渐变的折射率。

2. 发明授权

US5356718A Coating apparatus, method of coating glass, compounds and compositions for coating glasss and coated glass substrates 失效
标题翻译：涂布装置，玻璃涂覆方法，用于涂覆玻璃和涂覆的玻璃基板的化合物和组合物
公开(公告)号：US5356718A
公开(公告)日：1994-10-18
申请号：US17930
申请日：1993-02-16
申请人： Patricia R. Athey , Douglas S. Dauson , David E. Lecocq , George A. Neuman , John F. Sopko , Royann L. Stewart-Davis
发明人： Patricia R. Athey , Douglas S. Dauson , David E. Lecocq , George A. Neuman , John F. Sopko , Royann L. Stewart-Davis
IPC分类号： B32B9/00 , B32B17/06 , C03C17/00 , C03C17/23 , C03C17/245 , C03C17/30 , C03C17/34 , C07C7/04 , C23C16/40 , C23C16/44 , C23C16/453 , C23C16/455 , C23C16/54
CPC分类号： C03C17/245 , C03C17/002 , C03C17/2453 , C03C17/3417 , C23C16/401 , C23C16/4412 , C23C16/453 , C23C16/545 , C03C2217/211 , C03C2217/212 , C03C2217/213 , C03C2217/215 , C03C2217/216 , C03C2217/218 , C03C2217/219 , C03C2217/228 , C03C2217/23 , C03C2217/241 , C03C2217/244 , C03C2218/152
摘要： An apparatus for coating a glass ribbon has an exhaust on each side of a coating unit at different distances therefrom. With this arrangement, portions of the ribbon upstream and downstream of the coating unit are exposed to coating vapors from the coating unit for different periods of time. A coating mixture includes tin containing precursors and a silicon containing precursor. The silicon containing precursor has the structural formula ##STR1## where R.sub.1 is a group which does not have an oxygen available to form a peroxide, R.sub.2 is a functional group giving the silicon containing precursor the ability to be easily converted to silicon oxide coating, R.sub.3 is a bridging group to provide for multiple silicon atoms and R.sub.4 completes the bonding on the foundation silicon atom. An accelerant e.g. a phosphorus containing precursor may be used with the metal containing precursors to increase the deposition rate of the coating. The coating deposited on the glass has regions of continuously varying weight percent of silicon oxide and tin oxide as the distance from the glass-coating interface increases, with the surface of the coating farthest from the glass-coating interface being predominantly tin oxide. The regions within the coating provide the coating with different indices of refraction to eliminate iridescence resulting from increased thickness of the tin oxide at the outer coating surface and to provide the coated glass article with a neutral color. When phosphorus is used as the accelerant, the percent of crystallinity is reduced and approaches O, thereby reducing or eliminating the coating haze.
摘要翻译：用于涂覆玻璃带的设备在与其不同的距离处的涂布单元的每一侧上具有排气。通过这种布置，涂层单元的上游和下游的部分部分暴露于来自涂覆单元的涂覆蒸气不同的时间段。涂料混合物包括含锡前体和含硅前体。含硅前体具有结构式“IMAGE”，其中R1是不具有可用于形成过氧化物的氧的基团，R2是赋予含硅前体的能够容易地转化为氧化硅涂层的功能，R3 是提供多个硅原子的桥接基团，R4完成了在基础硅原子上的键合。加速剂例如可以将含磷前体与含金属的前体一起使用以增加涂层的沉积速率。随着玻璃 - 涂层界面的距离增加，沉积在玻璃上的涂层具有连续变化重量百分比的氧化硅和氧化锡的区域，其中最远离玻璃 - 涂层界面的涂层的表面主要是氧化锡。涂层中的区域为涂层提供不同的折射率，以消除由外涂层表面上的氧化锡厚度增加而产生的虹彩，并为涂覆的玻璃制品提供中性色。当磷用作促进剂时，结晶度的百分比降低并接近O，从而减少或消除涂层雾度。

3. 发明授权

US06797388B1 Methods of making low haze coatings and the coatings and coated articles made thereby 有权
标题翻译：制造低雾涂层的方法以及由此制成的涂层和涂层制品
公开(公告)号：US06797388B1
公开(公告)日：2004-09-28
申请号：US09521845
申请日：2000-03-09
申请人： Janos Szanyi , John F. Sopko , George A. Neuman
发明人： Janos Szanyi , John F. Sopko , George A. Neuman
IPC分类号： B32B1706
CPC分类号： C03C17/366 , C03C17/3417 , C03C17/3681 , C03C2217/734 , C03C2217/94 , Y10T428/24975
摘要： A coating in accordance with the invention has a substantially crystalline first layer with a substantially crystalline second layer provided over the first layer. A breaker layer is provided between the first and second layers and is configured to prevent or at least reduce epitaxial growth of the second layer on the first layer. A color suppression layer may be provided below the first layer. The coating can be provided on a substrate to make a coated article. A method of coating a substrate includes depositing a substantially crystalline first layer over at least a portion of the substrate and depositing a breaker layer over the first layer. The breaker layer is configured to prevent or at least reduce epitaxial growth of a subsequently deposited layer on the first layer.
摘要翻译：根据本发明的涂层具有基本上结晶的第一层，其具有设置在第一层上的基本上结晶的第二层。断路器层设置在第一和第二层之间，并且被配置为防止或至少减小第一层上的第二层的外延生长。可以在第一层下方设置颜色抑制层。涂层可以提供在基底上以制成涂层制品。涂覆衬底的方法包括在衬底的至少一部分上沉积基本上结晶的第一层并在第一层上沉积破坏层。断路器层被配置为防止或至少减少第一层上随后沉积的层的外延生长。

4. 发明授权

US5863337A Apparatus for coating a moving glass substrate 失效
标题翻译：用于涂覆移动玻璃基板的装置
公开(公告)号：US5863337A
公开(公告)日：1999-01-26
申请号：US464113
申请日：1995-06-05
申请人： George A. Neuman , John F. Sopko , Douglas S. Dauson
发明人： George A. Neuman , John F. Sopko , Douglas S. Dauson
IPC分类号： C03C17/00 , C03C17/245 , C03C17/34 , C23C16/40 , C23C16/44 , C23C16/453 , C23C16/54 , C23C16/00
CPC分类号： C03C17/002 , C03C17/245 , C03C17/2453 , C03C17/3417 , C23C16/401 , C23C16/402 , C23C16/4412 , C23C16/453 , C23C16/545 , C03C2217/213 , C03C2217/23 , C03C2218/152
摘要： An apparatus for coating a moving substrate which provides means for directing a coating composition vapor toward a substrate surface and moving portions of the vapor in opposite directions. The apparatus of the present invention may have the exhaust means on either side of the vapor directing means spaced at different distances from the vapor directing means, or the exhaust means may be spaced equally from the vapor directing means, but at different distances from the substrate surface. In another embodiment, the apparatus comprises the means to alter the flow volume of the vapor directing means and the two exhaust means such that the flow volume of the first and second exhaust means are not equal, such as by the exhaust means having openings of unequal surface area, wherein the exhaust means may be spaced equally or unequally from the vapor directing means at the same or different distances from the substrate surface. In another embodiment, the apparatus further comprises a structural element bridging the space between the vapor directing means and the exhaust means, which may be spaced equally or unequally from the vapor directing means, and at the same or different distances from the substrate surface.
摘要翻译：一种用于涂覆移动衬底的装置，其提供用于将涂料组合物蒸气引向衬底表面并使蒸气沿相反方向移动的装置。本发明的装置可以在蒸汽引导装置的任一侧上具有与蒸汽引导装置不同距离间隔开的排气装置，或者排气装置可以与蒸气引导装置间隔开，但距衬底不同的距离表面。在另一个实施例中，该装置包括改变蒸汽导向装置和两个排气装置的流量的装置，使得第一和第二排气装置的流量不相等，例如具有不等的开口的排气装置表面积，其中所述排气装置可以与所述蒸气引导装置以相同或不同的距离与所述基板表面间隔开或不等间隔。在另一个实施例中，该装置还包括桥接蒸气引导装置和排气装置之间的空间的结构元件，其可以与蒸气引导装置相等或不相等地间隔开，并且距离衬底表面相同或不同。

5. 发明授权

US5464657A Method for coating a moving glass substrate 失效
标题翻译：涂覆移动玻璃基板的方法
公开(公告)号：US5464657A
公开(公告)日：1995-11-07
申请号：US264816
申请日：1994-06-23
申请人： Patricia R. Athey , Douglas S. Dauson , David E. Lecocq , George A. Neuman , John F. Sopko , Royann L. Stewart-Davis
发明人： Patricia R. Athey , Douglas S. Dauson , David E. Lecocq , George A. Neuman , John F. Sopko , Royann L. Stewart-Davis
IPC分类号： B32B9/00 , B32B17/06 , C03C17/00 , C03C17/23 , C03C17/245 , C03C17/30 , C03C17/34 , C07C7/04 , C23C16/40 , C23C16/44 , C23C16/453 , C23C16/455 , C23C16/54 , C23C16/00
CPC分类号： C03C17/245 , C03C17/002 , C03C17/2453 , C03C17/3417 , C23C16/401 , C23C16/4412 , C23C16/453 , C23C16/545 , C03C2217/211 , C03C2217/212 , C03C2217/213 , C03C2217/215 , C03C2217/216 , C03C2217/218 , C03C2217/219 , C03C2217/228 , C03C2217/23 , C03C2217/241 , C03C2217/244 , C03C2218/152
摘要： A method for coating a moving substrate provides a coating having a chemical composition which varies continuously from the interface with the substrate to the opposite surface of the coating. The method involves directing a vapor coating composition toward a substrate surface and moving portions of the vapor in opposite directions. A vapor coating mixture may include a tin-containing precursor and a silicon-containing precursor. An accelerant, e.g. a phosphorus-containing precursor, may be used with the metal-containing precursors to increase the deposition rate of the coating. The coating deposited on the substrate has regions of continuously varying weight percent of silicon oxide and tin oxide as the distance from the substrate-coating interface increases, with the surface of the coating farthest from the substrate-coating interface being predominantly tin oxide. The regions of varying composition provide the coating with varying indices of refraction to eliminate iridescence to provide a coated article, particularly a tin oxide coated glass article, with a neutral color.
摘要翻译：涂覆移动衬底的方法提供了具有从衬底到衬底的相对表面连续变化的化学组成的涂层。该方法包括将蒸气涂料组合物引向衬底表面，并使蒸汽的相反方向移动。蒸气涂覆混合物可以包括含锡前体和含硅前体。促进剂，例如。含磷前体可以与含金属的前体一起使用以增加涂层的沉积速率。沉积在基板上的涂层具有连续改变重量百分比的氧化硅和氧化锡的区域，这是随着与基板 - 涂层界面的距离增加，涂层表面离基材 - 涂层界面最远的地方主要是氧化锡。不同组成的区域为涂层提供了不同的折射率，以消除虹彩以提供具有中性色的涂层制品，特别是涂有氧化锡的玻璃制品。

6. 发明授权

US3970037A Coating composition vaporizer 失效
标题翻译：涂料组合物蒸发器
公开(公告)号：US3970037A
公开(公告)日：1976-07-20
申请号：US533609
申请日：1974-12-17
申请人： John F. Sopko
发明人： John F. Sopko
IPC分类号： C03C17/00 , C03C17/245 , C23C16/453 , C23C16/54 , C23C13/12
CPC分类号： C03C17/245 , C03C17/002 , C23C16/453 , C23C16/545 , C03C2217/21 , C03C2217/217 , C03C2217/219 , C03C2217/23 , C03C2218/152
摘要： A metal reactant, dissolved in a volatile solvent, is sprayed into converging reactive carrier gas streams, is vaporized and is carried past a heater for ultimate discharge against a heated substrate whereupon the metal reactant and a portion of the reactive gas streams react to form an adherent coating on the substrate.
摘要翻译：溶解在挥发性溶剂中的金属反应物被喷射到会聚的反应性载气流中，被蒸发并被运送通过加热器以最终排放到加热的基底上，于是金属反应物和一部分反应气流反应形成基材上的粘附涂层。

7. 发明授权

US4401695A Method of and apparatus for applying powder coating reactants 失效
标题翻译：粉末涂料反应物的应用方法和设备
公开(公告)号：US4401695A
公开(公告)日：1983-08-30
申请号：US383644
申请日：1982-06-01
申请人： John F. Sopko
发明人： John F. Sopko
IPC分类号： B05D1/12 , B05D7/00 , C03C17/00 , C03C17/23 , C23C20/08
CPC分类号： B05D1/12 , C03C17/002 , C03C17/23 , C03C2217/211 , C03C2217/229 , C03C2217/23 , C03C2218/17
摘要： A method is disclosed for depositing a coating from a gaseous stream of a powder coating reactant, wherein the carrier gas is supplied at a high volume rate (at least 100 cubic ft./min) and low pressure (not greater than one psi).
摘要翻译：公开了一种从粉末涂料反应物的气流中沉积涂层的方法，其中载气以高体积速率（至少100立方英尺/分钟）和低压（不大于1psi）供应。

8. 发明授权

US4259371A Method for improving the alkali durability of metal oxide films formed by pyrolysis 失效
标题翻译：提高通过热解形成的金属氧化物膜的耐碱性的方法
公开(公告)号：US4259371A
公开(公告)日：1981-03-31
申请号：US060318
申请日：1979-07-25
申请人： Dennis S. Postupack , John F. Sopko
发明人： Dennis S. Postupack , John F. Sopko
IPC分类号： C03C17/25 , C03C17/23 , B05D3/02
CPC分类号： C03C17/23 , C03C2217/229 , C03C2218/112
摘要： A method is disclosed for improving the uniformity and durability of a pyrolytically deposited metal oxide film on glass by cooling the coating solution and/or the atomizing air prior to the application of the coating composition to the hot glass surface.
摘要翻译：公开了一种通过在将涂料组合物施加到热玻璃表面之前冷却涂覆溶液和/或雾化空气来提高玻璃上热解沉积的金属氧化物膜的均匀性和耐久性的方法。

9. 发明授权

US08197940B2 Aqueous suspension for pyrolytic spray coating 有权
标题翻译：用于热解喷涂的水悬浮液
公开(公告)号：US08197940B2
公开(公告)日：2012-06-12
申请号：US12179669
申请日：2008-07-25
申请人： John F. Sopko , Patricia R. Athey
发明人： John F. Sopko , Patricia R. Athey
IPC分类号： B32B15/00
CPC分类号： C03C17/25 , C03C2217/217 , C03C2217/219 , C03C2217/23 , C03C2218/112
摘要： The durability of a transparent pyrolytic spray applied coating is improved by providing a spray solution of metal acetylacetonates having different particle size distribution. More particularly, the particle size distribution of each of the metal acetylacetonates is a function of its melting temperature, and optionally of its melting temperature and solubility.
摘要翻译：通过提供具有不同粒度分布的金属乙酰丙酮化物的喷雾溶液来改善透明热解喷涂涂层的耐久性。更具体地，每个金属乙酰丙酮化物的粒度分布是其熔融温度，以及任选其熔融温度和溶解度的函数。

10. 发明授权

US3951100A Chemical vapor deposition of coatings 失效
标题翻译：化学气相沉积涂层
公开(公告)号：US3951100A
公开(公告)日：1976-04-20
申请号：US507656
申请日：1974-09-18
申请人： John F. Sopko , Krishna Simhan
发明人： John F. Sopko , Krishna Simhan
IPC分类号： C03C17/00 , C03C17/245 , C23C16/40 , C23C16/453 , C23C16/54 , C23C13/08
CPC分类号： C23C16/545 , C03C17/00 , C03C17/002 , C03C17/245 , C23C16/40 , C23C16/453 , C03C2217/21 , C03C2217/217 , C03C2217/219 , C03C2217/23 , C03C2218/152
摘要： A metal oxide coating is applied to a hot glass surface by contacting the surface with a mixture of carrier air, vaporized solvent and a vaporized metal containing reactant. The mixture is directed against the glass through an elongated, converging slot-nozzle, the interior surfaces of which have an increasing radius of curvature towards the exit end, nozzle at a Reynolds number exceeding 2500 with the nozzle-to-glass spacing at least 1.25 times the characteristic dimension of the nozzle.
摘要翻译：通过使表面与载体空气，蒸发溶剂和含有气化金属的反应物的混合物接触，将金属氧化物涂层施加到热玻璃表面。混合物通过细长的会聚狭缝喷嘴引导抵靠玻璃，其内表面朝向出口端具有增加的曲率半径，雷诺数超过2500的喷嘴，喷嘴间距至少为1.25 倍于喷嘴的特征尺寸。

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