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1. 发明公开

KR1020010053844A 폴리지방족방향족실세스퀴옥산 및 그의 제조 방법 有权
标题翻译：聚氨酯芳族硅酸酯及其制备方法
公开(公告)号：KR1020010053844A
公开(公告)日：2001-07-02
申请号：KR1019990054374
申请日：1999-12-02
申请人： 한국과학기술연구원
发明人： 황승상 , 홍순만 , 이응찬 , 홍승표
IPC分类号： C08G77/00
摘要： PURPOSE: Provided is poly aliphatic aromatic silsesquioxane, which is soluble in organic solvents and excellent in heat-resistance, combustion-resistance, and flexibility and can be used as a heatproof coating agent, an optical fiber protection coating agent, an adhesive, a release paper, a protection film of semiconductor, resist material, etc. CONSTITUTION: The high regular poly aliphatic aromatic silsesquioxane (formula 1) is produced by condensing 1,3-organodisiloxane (formula 2) solution in an organic solvent at a temperature of 50-350deg.C in the presence of a catalyst selected from the consisting of an alkali metal hydroxide, an amine, a quaternary ammonium salt, and a fluoride. In the formula, one of R1 and R2 is unsubstituted or substituted monovalent aliphatic hydrocarbon and the other is unsubstituted or substituted monovalent aromatic hydrocarbon, X is H, Cl, OH, NH2, or COOH, R is H, alkyl, acetate, or an alkali metal.
摘要翻译：目的：提供聚脂肪族芳香族倍半硅氧烷，其可溶于有机溶剂，耐热性，耐燃性和柔软性优异，可用作耐热涂层剂，光纤保护涂层剂，粘合剂，释放纸，半导体保护膜，抗蚀剂材料等。构成：高规则的聚脂肪族芳族倍半硅氧烷（式1）是通过在有机溶剂中在50℃的温度下将1,3-有机二硅氧烷（式2）在选自由碱金属氢氧化物，胺，季铵盐和氟化物组成的催化剂存在下进行。在该式中，R 1和R 2中的一个为未取代或取代的一价脂族烃，另一个为未取代或取代的一价芳族烃，X为H，Cl，OH，NH 2或COOH，R为H，烷基，乙酸酯或碱金属。

2. 发明授权

KR101218758B1 실세스퀴옥산 폴리머 및 이의 합성 방법 有权
标题翻译：倍半硅氧烷聚合物及其合成方法
公开(公告)号：KR101218758B1
公开(公告)日：2013-01-07
申请号：KR1020100035325
申请日：2010-04-16
申请人： 한국과학기술연구원
发明人： 황승상 , 백경열 , 홍순만 , 최승석 , 이응찬 , 이희승 , 곽순종 , 구종민
IPC分类号： C08G77/16 , C08G77/38 , C08G77/06
摘要： 본발명은개질된환형실록산의입체이성질체를모노머로하여축합중합된분자량이 1000 내지 1,000,000인실세스퀴옥산폴리머및 이의제조방법에관한것으로, 중합된고분자는기존의실록산폴리머와달리, 다양한유기용제에좋은용해도를보이면서도우수한가공성및 높은열 안정성높은모듈러스를보이며, 또한저유전물질로의활용도기대된다.

3. 发明公开

KR1020100131312A 폴리플루오로계실세스퀴옥산 및 그의 제조방법 无效
标题翻译：氟化多官能团及其制备方法
公开(公告)号：KR1020100131312A
公开(公告)日：2010-12-15
申请号：KR1020090050134
申请日：2009-06-05
申请人： 한국과학기술연구원
发明人： 황승상 , 홍순만 , 곽순종 , 백경열 , 구종민 , 최승석 , 마성원 , 이응찬
IPC分类号： C08G77/24 , C08G77/385 , C08G77/06 , C07F7/14
摘要： PURPOSE: Fluorinated polysilsesquioxane and a producing method thereof are provided to use the fluorinated polysilsesquioxane as an inter-layer insulating film with the low dielectric constant. CONSTITUTION: Fluorinated polysilsesquioxane has a fluorohydrocarbon side chain, and is marked with chemical formula 1. In the chemical formula 1, R1 and R2 are selected from the group consisting of a fluoro aromatic group, a fluoroalkyl group, an allyl group, a vinyl group, an epoxy group, a methacryl group, and an acryl group. The number average molecular weight of the fluorinated polysilsesquioxane is 1,000~100,000.
摘要翻译：目的：提供氟化聚倍半硅氧烷及其制备方法，以使用氟化聚倍半硅氧烷作为低介电常数的层间绝缘膜。构成：氟化聚倍半硅氧烷具有氟代烃侧链，并用化学式1表示。在化学式1中，R 1和R 2选自氟代芳族基团，氟代烷基基团，烯丙基基团，乙烯基基团，环氧基，甲基丙烯酰基和丙烯酰基。氟化聚倍半硅氧烷的数均分子量为1,000〜100,000。

4. 发明授权

KR101597551B1 SiO2 박막 형성용 재료의 제조방법 및 이를 이용한 SiO2 박막의 형성방법 有权
标题翻译：用于形成SIO2薄膜的材料的制备方法和使用其形成SIO2薄膜的方法
公开(公告)号：KR101597551B1
公开(公告)日：2016-02-25
申请号：KR1020140131626
申请日：2014-09-30
申请人： 한국과학기술연구원
发明人： 황승상 , 홍순만 , 백경열 , 구종민 , 송선자 , 이응찬
IPC分类号： C09D183/02 , C03C17/30
CPC分类号： C09D183/02 , C03C17/30
摘要： 본발명은테트라알콕시실란을가수분해하여가수분해물을얻는단계; 및상기가수분해물과 3관능성실란을반응시켜하기화학식 1로표시되는전구체를포함하는도포용액을제조하는단계를포함하는 SiO박막형성용재료의제조방법을제공한다. [화학식 1] [(SiO)·HSiO)][OH](상기식에서, m+n=100, 30≤m
摘要翻译：本发明提供了一种用于生产SiO_2薄膜形成材料的方法，包括以下步骤：通过水解四烷氧基硅烷获得水解产物; 并且通过使水解产物与三官能硅烷反应，制备含有由化学式1表示的前体的涂布溶液。在化学式1中，m + n = 100,30 <= m <90，10 <= n <70，x + y = 2,0

5. 发明公开

KR1020100131347A 실세스퀴옥산 폴리머 및 이의 합성 방법 有权
标题翻译： SILSESQUIOXANE聚合物及其合成方法
公开(公告)号：KR1020100131347A
公开(公告)日：2010-12-15
申请号：KR1020100035325
申请日：2010-04-16
申请人： 한국과학기술연구원
发明人： 황승상 , 백경열 , 홍순만 , 최승석 , 이응찬 , 이희승 , 곽순종 , 구종민
IPC分类号： C08G77/16 , C08G77/38 , C08G77/06
摘要： PURPOSE: A silsesquioxane polymer and a synthesis method thereof are provided to secure the low dielectric, the high modulus, and the compatibility with an organic solvent of the polymer. CONSTITUTION: A silsesquioxane polymer is obtained by condense-polymerizing a modified cyclic siloxane stereoisomer, and has the weight average molecular weight of 1,000~1,000,000. The modified cyclic siloxane stereoisomer is a cyclic siloxane substituted with a hydroxyl group. A synthesis method of the silsesquioxane polymer comprises the following steps: modifying the cyclic siloxane with a stereoisomer; separating the stereoisomer capable of forming a polymer; and condense-polymerzing the polymer using the stereoisomer as a monomer.
摘要翻译：目的：提供倍半硅氧烷聚合物及其合成方法以确保低介电常数，高模量和与聚合物的有机溶剂的相容性。构成：通过将改性的环状硅氧烷立体异构体进行缩聚而获得倍半硅氧烷聚合物，其重均分子量为1,000〜1,000,000。改性环状硅氧烷立体异构体是用羟基取代的环状硅氧烷。倍半硅氧烷聚合物的合成方法包括以下步骤：用立体异构体改性环状硅氧烷; 分离能够形成聚合物的立体异构体; 并使用立体异构体作为单体使聚合物缩聚。

6. 发明授权

KR101972761B1 가교제용 실릴카보실록산 유도체와 이의 제조방법 有权
公开(公告)号：KR101972761B1
公开(公告)日：2019-04-29
申请号：KR1020170143189
申请日：2017-10-31
申请人： 한국과학기술연구원
发明人： 한준수 , 황승상 , 홍순만 , 구종민 , 백경열 , 조상호 , 최지희 , 김송이 , 이응찬
IPC分类号： C07F7/08 , B01J31/22

7. 发明授权

KR100371070B1 폴리지방족방향족실세스퀴옥산 및 그의 제조 방법 有权
标题翻译： 폴리지방족방향족실세스퀴옥산및그의제조방폴
公开(公告)号：KR100371070B1
公开(公告)日：2003-02-05
申请号：KR1019990054374
申请日：1999-12-02
申请人： 한국과학기술연구원
发明人： 황승상 , 홍순만 , 이응찬 , 홍승표
IPC分类号： C08G77/00
摘要： PURPOSE: Provided is poly aliphatic aromatic silsesquioxane, which is soluble in organic solvents and excellent in heat-resistance, combustion-resistance, and flexibility and can be used as a heatproof coating agent, an optical fiber protection coating agent, an adhesive, a release paper, a protection film of semiconductor, resist material, etc. CONSTITUTION: The high regular poly aliphatic aromatic silsesquioxane (formula 1) is produced by condensing 1,3-organodisiloxane (formula 2) solution in an organic solvent at a temperature of 50-350deg.C in the presence of a catalyst selected from the consisting of an alkali metal hydroxide, an amine, a quaternary ammonium salt, and a fluoride. In the formula, one of R1 and R2 is unsubstituted or substituted monovalent aliphatic hydrocarbon and the other is unsubstituted or substituted monovalent aromatic hydrocarbon, X is H, Cl, OH, NH2, or COOH, R is H, alkyl, acetate, or an alkali metal.
摘要翻译：用途：提供一种可溶于有机溶剂，具有优异的耐热性，耐燃性和柔韧性的聚脂族芳族倍半硅氧烷，可用作耐热涂层剂，光纤保护涂层剂，粘合剂，释放剂纸，半导体保护膜，抗蚀剂材料等。组成：通过在有机溶剂中将1,3-有机二硅氧烷（式2）溶液在50℃-50℃的温度下缩合来制备高规则性多脂族芳族倍半硅氧烷（式1）在选自碱金属氢氧化物，胺，季铵盐和氟化物的催化剂存在下进行。在该式中，R 1和R 2中的一个是未取代或取代的一价脂族烃，另一个是未取代或取代的一价芳烃，X是H，Cl，OH，NH 2或COOH，R是H，烷基，乙酸根或碱金属。

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