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1. 发明授权

KR100367042B1 보호된 안트라퀴논 유도체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译： 보호된안트라퀴논유도체와，이를이용한형광화상형성방보
公开(公告)号：KR100367042B1
公开(公告)日：2003-01-15
申请号：KR1019990046512
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 한동근 , 강종희
IPC分类号： C07C50/18
CPC分类号： Y02P20/55
摘要： PURPOSE: A method for forming a fine fluorescent image by using protected hydroxy group-containing anthraquinone derivatives or naphthacenequinone derivatives is provided. Thereby the obtained protected hydroxy group-containing compound can be applied to recording material and censor material because it can easily form a fine fluorescent image of micrometer units under the condition of a chemically amplified fine image forming process. CONSTITUTION: This method comprises the steps of: preparing a transparent solution by dissolving protected hydroxy group-containing anthraquinone derivatives of formula 1 or naphthacenequinone derivatives of formula 2 and a soluble polymer in an organic solvent; forming a thin film by coating the solution on a substrate; prebaking the thin film coated substrate; and removing a hydroxy protecting group of the anthraquinone derivatives or naphthacenequinone derivatives by treating under the condition of a chemically amplified fine image forming process.
摘要翻译：目的：提供一种通过使用被保护的含羟基蒽醌衍生物或并四苯醌衍生物来形成精细荧光图像的方法。因此，所获得的被保护的含羟基化合物可以应用于记录材料和传感材料，因为它可以在化学放大的精细图像形成过程的条件下容易地形成微米单位的精细荧光图像。构成：该方法包括以下步骤：通过将式1的受保护的含羟基蒽醌衍生物或式2的萘并萘醌衍生物和可溶性聚合物溶解在有机溶剂中制备透明溶液; 通过将溶液涂覆在基底上形成薄膜; 预烘烤薄膜涂覆的基材; 并通过在化学放大的精细图像形成过程的条件下处理除去蒽醌衍生物或萘并萘醌衍生物的羟基保护基。

2. 发明授权

KR100351074B1 치과수복용 광중합성 복합레진 조성물 失效
标题翻译：牙科修复用光聚合性复合树脂组合物
公开(公告)号：KR100351074B1
公开(公告)日：2002-09-05
申请号：KR1020000038132
申请日：2000-07-05
申请人： 한국과학기술연구원 , 주식회사 덴키스트
发明人： 한동근 , 안광덕 , 김종만 , 정진희
IPC分类号： A61K6/00
摘要： 본 발명은 종래 치과수복용 프리폴리머로 사용되고 있는 2,2-비스-(4-(2-히드록시-3-메타크릴로일옥시프로폭시)페닐)프로판 [이하, "Bis-GMA"라 명명함]에, 이 Bis-GMA 분자 중의 히드록시기의 수소 원자를 메타크릴레이트기로 치환한 멀티메타크릴레이트기 함유 다관능성 프리폴리머를 혼합한 프리폴리머 혼합물을 기재로 하고, 희석제, 무기 충전제, 광개시계 및 기타 첨가제를 포함하는 치과수복용 광중합성 복합레진 조성물에 관한 것이다. 다관능성 프리폴리머 혼합물을 기재로 하는 본 발명의 치과수복용 광중합성 복합레진 조성물은 기재로서 Bis-GMA 자체만을 포함하는 종래의 것보다 우수한 물리적, 기계적 특성과 생체 적합성을 나타낸다.

3. 发明授权

KR100341426B1 보호된 히드록시안트라퀴논 유도체 및 그의 공중합체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译：保护的羟基蒽醌衍生物及其共聚物和使用其形成荧光图像的过程
公开(公告)号：KR100341426B1
公开(公告)日：2002-06-21
申请号：KR1019990046511
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 한동근 , 강종희
IPC分类号： C07C50/16
CPC分类号： Y02P20/55
摘要： 본발명은미세형광화상형성용재료의전구물질로서유용한히드록시보호된 1,4-디히드록시안트라퀴논유도체및 그의공중합체와, 이공중합체를이용한미세형광화상형성방법에관한것이다. 본발명의히드록시보호된 1,4-디히드록시안트라퀴논공중합체는히드록시기의분자내수소결합을한시적으로차단한다음, 산, 열또는광 등에의해탈보호되어색 및형광의변화를일으키기때문에, 화학증폭성미세화상형성공정조건에서쉽게미크론미터단위의미세형광화상을형성할수 있어서, 색화상및 형광화상물질과같은기록용재료, 그리고센서재료로응용될수 있다.

4. 发明授权

KR100324644B1 α-아미노안트라센 유도체 및 그의 공중합체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译： - 氨基蒽衍生物及其共聚物及使用其形成荧光图像的方法
公开(公告)号：KR100324644B1
公开(公告)日：2002-02-27
申请号：KR1019990046513
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 한동근 , 강종희
IPC分类号： C07C15/28
摘要： 본발명은미세형광화상형성용재료의전구물질로서유용한, α-아미노안트라센유도체및 그의공중합체와, 이공중합체를이용한미세형광화상형성방법에관한것이다. 본발명의α-아미노안트라센함유공중합체는유기산또는무기산에의해형광이변하고, 광산발생제와혼합하여박막상태에서노광할경우쉽게미크론미터단위의미세형광화상을형성할수 있으며, 용액, 필름및 입자상태에서센서기능이우수하여기록용재료및 센서재료로응용될수 있다.

5. 发明授权

KR100321563B1 피리딜벤족사졸 유도체 및 그의 공중합체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译：吡啶基苯并恶唑衍生物及其共聚物及其使用荧光图像的方法
公开(公告)号：KR100321563B1
公开(公告)日：2002-01-23
申请号：KR1019990046514
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 박기홍 , 한동근
IPC分类号： C07D263/54
摘要： 본발명은미세형광화상형성용재료의전구물질로서유용한, 피리딜벤족사졸유도체및 그의공중합체와, 이공중합체를이용한미세형광화상형성방법에관한것이다. 본발명의피리딜벤족사졸함유공중합체는유기산또는무기산, 또는금속이온에의해형광이변하고, 광산발생제와혼합하여박막상태에서노광할경우쉽게미크론미터단위의미세형광화상을형성할수 있으며, 용액, 필름및 입자상태에서센서기능이우수하여기록용재료및 센서재료로응용될수 있다.

6. 发明公开

KR1020010038525A 보호된 안트라퀴논 유도체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译：具有保护性羟基的蒽醌和萘醌衍生物及其使用形成荧光图像的方法
公开(公告)号：KR1020010038525A
公开(公告)日：2001-05-15
申请号：KR1019990046512
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 한동근 , 강종희
IPC分类号： C07C50/18
CPC分类号： Y02P20/55
摘要： PURPOSE: A method for forming a fine fluorescent image by using protected hydroxy group-containing anthraquinone derivatives or naphthacenequinone derivatives is provided. Thereby the obtained protected hydroxy group-containing compound can be applied to recording material and censor material because it can easily form a fine fluorescent image of micrometer units under the condition of a chemically amplified fine image forming process. CONSTITUTION: This method comprises the steps of: preparing a transparent solution by dissolving protected hydroxy group-containing anthraquinone derivatives of formula 1 or naphthacenequinone derivatives of formula 2 and a soluble polymer in an organic solvent; forming a thin film by coating the solution on a substrate; prebaking the thin film coated substrate; and removing a hydroxy protecting group of the anthraquinone derivatives or naphthacenequinone derivatives by treating under the condition of a chemically amplified fine image forming process.
摘要翻译：目的：提供通过使用保护的含羟基蒽醌衍生物或并四苯醌衍生物形成精细荧光图像的方法。由此，可以在化学放大精细图像形成工序的条件下容易地形成微米单位的微细荧光图像，将得到的保护的含羟基化合物施加到记录材料和检查材料上。构成：该方法包括以下步骤：通过将保护的含羟基的式1的蒽醌衍生物或式2的并四苯醌衍生物和可溶性聚合物溶解在有机溶剂中来制备透明溶液; 通过将溶液涂布在基材上形成薄膜; 预烘烤薄膜涂布基材; 并通过在化学放大的精细成像方法的条件下处理除去蒽醌衍生物或萘并醌衍生物的羟基保护基。

7. 发明公开

KR1020020004331A 치과수복용 광중합성 복합레진 조성물 失效
标题翻译：用于牙科修复的光聚合复合树脂组合物
公开(公告)号：KR1020020004331A
公开(公告)日：2002-01-16
申请号：KR1020000038132
申请日：2000-07-05
申请人： 한국과학기술연구원 , 주식회사 덴키스트
发明人： 한동근 , 안광덕 , 김종만 , 정진희
IPC分类号： A61K6/00
CPC分类号： C08F2/46 , A61K6/083 , C08F222/1006 , C08F2222/1046 , Y10S522/908 , C08F2222/1033 , C08F2222/1013 , C08L33/00
摘要： PURPOSE: A photopolymerizable composite resin composition for dental restoration using a multifunctional prepolymer mixture as a base material is provided, which has increased biocompatibility as well as exhibiting better physical and mechanical properties as compared to conventional compositions based on only Bis-GMA itself. CONSTITUTION: This composite resin composition comprises 2 to 40% by weight of multifunctional prepolymer mixture of 2,2-bis-(4-(2-hydroxy-3-methacryloyloxypropoxy)phenyl)propane ("Bis-GMA") of formula 1 and tri-GMA of formula 2 in a ratio of 95:5 to 5:95, 1 to 20% by weight of a diluent, 40 to 95% by weight of an inorganic filler, a photoinitiation system, and other additives. The composition has almost no cytotoxicity and high strength and hardness.
摘要翻译：目的：提供一种使用多官能预聚物混合物作为基础材料的用于牙科修复的可光聚合复合树脂组合物，与仅基于Bis-GMA本身的常规组合物相比，其具有增加的生物相容性以及表现出更好的物理和机械性能。构成：该复合树脂组合物包含2至40重量％的式1的2,2-双 - （4-（2-羟基-3-甲基丙烯酰氧基丙氧基）苯基）丙烷（“Bis-GMA”）的多官能预聚物混合物和式2的三-GMA比例为95:5至5:95,1至20重量％的稀释剂，40至95重量％的无机填料，光引发体系和其它添加剂。该组合物几乎没有细胞毒性和高强度和硬度。

8. 发明公开

KR1020010038527A 피리딜벤족사졸 유도체 및 그의 공중합체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译：吡啶并苯并噻唑衍生物及其共聚物及荧光成像方法
公开(公告)号：KR1020010038527A
公开(公告)日：2001-05-15
申请号：KR1019990046514
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 박기홍 , 한동근
IPC分类号： C07D263/54
摘要： PURPOSE: The pyridyl benzoxazole derivatives, their copolymers, and a fluorescence image making method are provided, thereby the pyridyl benzoxazole copolymers have good sensor properties in solution, film and particle status, so that they can be used as recording materials or sensor materials. CONSTITUTION: The pyridyl benzoxazole derivative is represented by formula (1), in which A and B are independently CH and N; R1 is alkyl or phenyl; R2 is O or NH, R3 is vinyl, acryl, allyl, alpha-methylvinyl or 4-vinylphenyl; m is an integer from 0 to 20. The pyridyl benzoxazole copolymer represented by formula (2) is produced by radical polymerization of comonomer selected from the group consisting of pyridyl benzoxazole derivatives, styrene, maleimide and methacrylate, in which A and B are independently CH and N; R1 is alkyl or phenyl; R2 is O or NH, m is an integer from 0 to 20; R4 is hydrogen or methyl; R5 is methyloxycarbonyl or phenyl; and x and y are integer from 10 to 5000. The fluorescence image making method comprises the steps of: dissolving pyridyl benzoxazole copolymer of formula (2) wherein A is CH and B is N, AIBN, organic acid or inorganic acid in an organic solvent; coating the solution on board and drying to form a thin layer; prebaking the thin layer; and exposing the thin layer to light using photomask and post-exposure baking it.
摘要翻译：目的：提供吡啶基苯并恶唑衍生物，其共聚物和荧光图像制备方法，因此吡啶基苯并恶唑共聚物在溶液，膜和颗粒状态下具有良好的传感器性质，因此可用作记录材料或传感器材料。构成：吡啶基苯并恶唑衍生物由式（1）表示，其中A和B独立地为CH和N; R1是烷基或苯基; R2是O或NH，R3是乙烯基，丙烯基，烯丙基，α-甲基乙烯基或4-乙烯基苯基; m是0至20的整数。由式（2）表示的吡啶基苯并恶唑共聚物是通过选自吡啶基苯并恶唑衍生物，苯乙烯，马来酰亚胺和甲基丙烯酸酯的共聚单体的自由基聚合制备的，其中A和B独立地为CH 和N; R1是烷基或苯基; R2是O或NH，m是0至20的整数; R4是氢或甲基; R5是甲氧基羰基或苯基; 荧光图像的制造方法包括以下步骤：将有机溶剂中A为CH且B为N的式（2）的吡啶基苯并恶唑共聚物，AIBN，有机酸或无机酸溶解 ; 将溶液涂布在板上并干燥以形成薄层; 预制薄层; 并使用光掩模将该薄层曝光并曝光后烘烤。

9. 发明公开

KR1020010038524A 보호된 히드록시안트라퀴논 유도체 및 그의 공중합체와, 이를 이용한 형광 화상 형성 방법 失效
标题翻译：保护的羟基四氢喹啉衍生物及其共聚物，使用它们形成荧光图像的方法
公开(公告)号：KR1020010038524A
公开(公告)日：2001-05-15
申请号：KR1019990046511
申请日：1999-10-26
申请人： 한국과학기술연구원
发明人： 안광덕 , 김종만 , 한동근 , 강종희
IPC分类号： C07C50/16
CPC分类号： Y02P20/55
摘要： PURPOSE: Provided are hydroxy protected 1,4-dihydroxyanthraquinone derivatives used as a precursor of material for forming fine fluorescent image, copolymers thereof applied to material for recording and a sensor, and a process for forming the fine fluorescent image by using the copolymers. CONSTITUTION: The hydroxy protected 1,4-dihydroxyanthraquinone derivatives are represented by the formula (1), and the copolymers thereof represented by the formula (2) are produced by radical polymerizing the hydroxy protected 1,4-dihydroxyanthraquinone derivatives and comonomers selected from the group consisting of styrene, maleimide, and methacrylate in the presence of a polymerization initiator. And the process for forming the fine fluorescent image comprises the steps of: dissolving the copolymers containing the hydroxy protected 1,4-dihydroxyanthraquinone and a photoacid generator in an organic solvent; spreading the solution on a substrate and drying to from a thin film; prebaking the thin film coated substrate; treating under the condition of chemical amplification to remove the hydroxy protecting group from the copolymers. In the formula, R1 is hydroxy protecting group, one of A and B is H, R2 is O or NH, R3 is vinyl, alpha-methyl vinyl, or 4-biphenyl, one of C and D is H and the other is represented by the formula (c) or (d), R4 is hydrogen or methyl, R5 is methyloxycarbonyl or phenyl, m is an integer of 0-20, x and y are independently an integer of 10-5000.
摘要翻译：目的：提供用作形成细荧光图像的材料的前体的羟基保护的1,4-二羟基蒽醌衍生物，其用于记录材料的共聚物和传感器，以及通过使用该共聚物形成微细荧光图像的方法。构成：羟基保护的1,4-二羟基蒽醌衍生物由式（1）表示，其由式（2）表示的共聚物通过自由基聚合羟基保护的1,4-二羟基蒽醌衍生物和选自以下的共聚单体制备：在聚合引发剂存在下由苯乙烯，马来酰亚胺和甲基丙烯酸酯组成的组。并且形成细荧光图像的方法包括以下步骤：将含有羟基保护的1,4-二羟基蒽醌和光致酸产生剂的共聚物溶解在有机溶剂中; 将溶液铺展在基材上并从薄膜干燥; 预烘烤薄膜涂布基材; 在化学扩增条件下处理以从共聚物中除去羟基保护基团。在该式中，R 1是羟基保护基，A和B之一是H，R 2是O或NH，R 3是乙烯基，α-甲基乙烯基或4-联苯基，C和D之一是H，另一个被表示通过式（c）或（d），R 4是氢或甲基，R 5是甲氧基羰基或苯基，m是0-20的整数，x和y独立地是10-5000的整数。

10. 发明公开

KR1020000019999A 순간자발중합성부타디엔유도체및그의제조방법 失效
标题翻译：现代自聚合双丁二烯衍生物及其方法
公开(公告)号：KR1020000019999A
公开(公告)日：2000-04-15
申请号：KR1019980038386
申请日：1998-09-17
申请人： 한국과학기술연구원
发明人： 안광덕 , 한동근 , 김종만
IPC分类号： C07C255/02 , C08F236/00
摘要： PURPOSE: High-reactivity butadiene derivatives which self-polymerize instant and method for producing the same are provided which can manufacture a polymer simply without any initiator, catalyst and polymerization apparatus. CONSTITUTION: High-reactivity butadiene derivatives which self-polymerize instant, a butadiene monomer of formula(1), a butadiene polymer of formula(2) and a butadiene copolymer of formula(3), and method for producing the same are described. In formula, R1, R2, R4 are same or different cyan, carboxylate(2-8C carboxylate in the formula(1), 1-8C carboxylate in the formula(2) and (3)), sulfon, formal acetyl, benzoyl, phosphonyl, amide, or phenyl, R3 is H, or methyl, 1-8C carboxylate, sulfon, formal, acetyl, benzoyl, phosphonyl, amide, or phenyl. The compound can be used for various functional polymer fields such as a new process, a new polymer product, a coating agent, a carbon fiber precursor, an instant adhesive or the like.
摘要翻译：目的：提供快速自聚合的高反应性丁二烯衍生物及其制备方法，其可以简单地制备聚合物，而无需任何引发剂，催化剂和聚合装置。本发明描述了即时自聚合的高反应性丁二烯衍生物，式（1）的丁二烯单体，式（2）的丁二烯聚合物和式（3）的丁二烯共聚物及其制备方法。在式中，R 1，R 2，R 4是相同或不同的青色羧酸酯（式（1）中的2-8C羧酸酯，式（2）和（3）中的1-8C羧酸酯），磺酰基，乙酰基，苯甲酰基，膦酰基，酰胺或苯基，R 3为H或甲基，1-8C羧酸酯，磺酰基，正式，乙酰基，苯甲酰基，膦酰基，酰胺基或苯基。该化合物可以用于各种功能性聚合物领域，例如新方法，新聚合物产品，涂布剂，碳纤维前体，速溶胶粘剂等。

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