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1. 发明公开

KR1020000049546A 키토산 함유 구강청정제 및 그 제조방법 无效
标题翻译：含有谷氨酸盐的洗涤剂及其制备方法
公开(公告)号：KR1020000049546A
公开(公告)日：2000-08-05
申请号：KR1020000018318
申请日：2000-04-07
申请人： 주식회사 오스코텍 , 이현주 , 권오규 , 정동식 , 이성철 , 고선일 , 임성빈 , 유영목 , 신동령 , 김형건 , 김종여 , 김정근 , 김세원 , 임창준 , 한국유나이티드제약 주식회사
发明人： 김정근 , 길영식 , 안승호 , 신현종 , 배건우 , 조재민
IPC分类号： A61K8/98 , A61K8/73 , A61Q11/00
摘要： PURPOSE: A novel mouth wash composition comprises specific molecular weight of aqueous chitosan instead of chemical antibiotic agents in the conventional mouth wash. The novel mouth wash has an improved efficacy and stability and improves oral hygiene. CONSTITUTION: A novel mouth wash is characterized by adding 0.01-1% of chitosan having 3,000-13,000 Da of molecular weight to a surfactant, a stabilizing agent, a sweetening agent, a flavoring agent, a colorant and a solvent. A preparation method of the mouth wash is characterized by the following steps of: obtaining albumen only from eggs and then diluting the albumen with distilled water; adding the diluted albumen to chitosan solution; homogenizing by warming up in a double boiler at 90°C for 30 minutes; centrifuging at 12,000 rpm for 10 minutes followed by collecting supernatant; and adding the supernatant to the conventional mouth wash comprising the components mentioned above. The multi-functional mouth wash has not only an antibiotic activity but also protection activity, such as inhibiting noxious effect of organic acid and promoting separation or inhibiting bond of hydroxyaptite and Streptococcus mutans, and treatment activity such as promoting reforming of oral soft tissue and osteoconduction.
摘要翻译：目的：新型漱口水组合物包含特定分子量的水性壳聚糖代替常规漱口水中的化学抗生素。新颖的漱口水具有改进的功效和稳定性并改善口腔卫生。构成：新型漱口水的特征在于向表面活性剂，稳定剂，甜味剂，调味剂，着色剂和溶剂中加入0.01-1％具有3,000-13,000Da分子量的壳聚糖。漱口水的制备方法的特征在于以下步骤：仅从鸡蛋中获得白蛋白，然后用蒸馏水稀释白蛋白; 将稀释的蛋白加入壳聚糖溶液中; 通过在双层锅炉中在90℃下预热30分钟来均化; 以12,000rpm离心10分钟，然后收集上清液; 并将上清液加入到包含上述组分的常规漱口水中。多功能漱口水不仅具有抗菌活性，而且具有抑制有机酸的有害作用，促进羟基磷酸酯和变形链球菌分离抑制作用等保护作用，促进口腔软组织改造和骨传导等治疗活性。

2. 发明公开

KR1020000051845A 사과로부터 추출한 폴리페놀을 포함하는 항진균성 힐패드 失效
标题翻译：从应用中提取的含有聚苯乙烯的抗菌垫
公开(公告)号：KR1020000051845A
公开(公告)日：2000-08-16
申请号：KR1019990002541
申请日：1999-01-27
申请人： 한국유나이티드제약 주식회사
发明人： 배건우 , 김동관 , 장용남 , 박홍철 , 김윤경
IPC分类号： A61L9/04
CPC分类号： A61L9/013 , A43B7/149 , A61L9/04
摘要： PURPOSE: An antifungal heel-pad containing polyphenol, which is extracted from apples and has excellent antifungal activity, is provided. CONSTITUTION: Polyphenol extracted from apples has antioxidant property and prepared by the following steps of: obtaining fruit juice by washing malus pumila miller apples, breaking, and pressing; storing at 50°C for 24 hours and treating with pectinase GL; filtering, adsorbing to Sepabeads SP-850, and washing; erupting with 65% ethanol, concentrating eluent solution under reduced pressure, and filtering; adding dextrin BLD solution containing 60% of dextrin to concentrate, and spray-drying; separating the extract of apples by filtering particles mixed with 40% of the powder extract of apples and 60% of dextrin powder using magnet(12,000 gauss) and 30 mesh filter. The heel pad is based on silicon comprising 0.0001-10.0wt.% of the polyphenol
摘要翻译：目的：提供从苹果中提取并具有优异抗真菌活性的含有多酚的抗真菌脚跟垫。构成：从苹果提取的多酚具有抗氧化性能，并通过以下步骤制备：通过洗涤苹果苹果苹果获得果汁，破碎和压制; 在50℃保存24小时，用果胶酶GL处理; 过滤，吸附到Sepabeads SP-850，洗涤; 用65％乙醇喷出，减压浓缩洗脱液，过滤; 加入含有60％糊精的糊精BLD溶液浓缩，喷雾干燥; 通过使用磁体（12,000高斯）和30目过滤器过滤与40％的苹果粉末提取物和60％糊精粉末混合的颗粒分离苹果提取物。鞋跟垫基于含有0.0001-10.0重量％多酚的硅

3. 发明授权

KR100296737B1 아세클로페낙의 제조방법 有权
标题翻译：醋氯芬酸的过程
公开(公告)号：KR100296737B1
公开(公告)日：2001-07-04
申请号：KR1019990050584
申请日：1999-11-15
申请人： 한국유나이티드제약 주식회사
发明人： 안승호 , 배건우 , 백기현 , 장용남
IPC分类号： C07C229/58
摘要： 본발명은디클로페낙과알릴알코올을다양한산 촉매하에서에스테르화반응으로디클로페낙알릴에스테르를제조하고, 이것을오존과반응시켜아세클로페낙으로명명되는 2-[(2,6-디클로로페닐)아미노]페닐아세톡시아세트산을수득하는방법에관한것이다.

4. 发明公开

KR1020000063125A 아세클로페낙의 제조방법 有权
标题翻译： ACECHLOPHENAC的制造方法
公开(公告)号：KR1020000063125A
公开(公告)日：2000-11-06
申请号：KR1019990050584
申请日：1999-11-15
申请人： 한국유나이티드제약 주식회사
发明人： 안승호 , 배건우 , 백기현 , 장용남
IPC分类号： C07C229/58
摘要： PURPOSE: A manufacturing method of acechlophenac(non-steroidal anti-inflammatory analgesics) of formula (1) within short time is provided, which is cost effective by using aryl alcohol, a simple apparatus, and common organic solvent. CONSTITUTION: A preparation method of acechlophenac comprises the steps of: dissolving 5g(17mmol) of 2-£(2,6-dichlorophenyl)amino|benzene acetate in 200ml of ethyl acetate, adding 0.5g of concentrated sulfuric acid, and shaking well; adding 4.9g(84mmol) of aryl alcohol, shaking by circulating, and reacting for 5hrs; cooling to room temperature, adding 200ml of water to wash organic layer; drying with magnesium sulfate, distilling under decompression to eliminate solvent; distillation-refining the residue under high-vacuumed state at 280°C to get dichlophenac aryl ester; reacting the dichlophenac aryl ester with ozone in a solvent at -10 to -90°C for 5 minutes-5 hrs to get 2-£(2,6-dichlorophenyl)amino|phenyl acetoxy acetate(acechlophenac).
摘要翻译：目的：提供在短时间内制备式（1）的乙酰胆碱（非甾体抗炎镇痛药）的方法，其通过使用芳醇，简单的装置和常见的有机溶剂是有成本效益的。构成：乙酰苯胺的制备方法包括以下步骤：将5g（17mmol）2-（2,6-二氯苯基）氨基苯乙酸乙酯溶于200ml乙酸乙酯中，加入0.5g浓硫酸，摇匀; 加入4.9g（84mmol）芳基醇，通过循环摇动，反应5小时; 冷却至室温，加入200ml水洗涤有机层; 用硫酸镁干燥，减压蒸馏除去溶剂; 在280℃下在高真空状态下蒸馏精制残渣，得到二氯苯乙烯芳基酯; 使二氯苯乙烯芳基酯与臭氧在-10至-90℃下反应5分钟-5小时，得到2-（2,6-二氯苯基）氨基|苯基乙酰氧基乙酸酯（乙烯基苯甲酸）。

5. 发明公开

KR1020000056792A 프로폴리스 추출물의 제조방법 无效
标题翻译：丙酸酯提取物的制备方法
公开(公告)号：KR1020000056792A
公开(公告)日：2000-09-15
申请号：KR1019990006424
申请日：1999-02-26
申请人： 한국유나이티드제약 주식회사
发明人： 신현종 , 배건우 , 김동관 , 장용남 , 박홍철
IPC分类号： B01D11/00 , A61K35/64
CPC分类号： B01D11/0492 , A61K35/644 , B01D11/0484
摘要： PURPOSE: A method for preparing the propolis extract is provided, not to change the color, perfume and taste of the propolis extract during the preparation process and not to generate the precipitate during the long-term distribution. CONSTITUTION: A method comprises the steps of extracting the raw proplis with 70% ethanol at the temperature of 44-46°C; adding a pH controlling agent to the extract to adjust the pH to be 6.0-7.0; adding protease, lipase, cellulase, amylase, glucoamylase, pectinase and lactase, and stirring the mixture for 10-15 hours; mixing the mixture with ethanol and filtering off the floating materials; and adding glycerin to the filtrate and stirring it. Preferably the pH controlling agent is citric acid. The ratio of glycerin to the propolis extract is 70-80 : 20-30 by weight.
摘要翻译：目的：提供制备蜂胶提取物的方法，不改变制备过程中蜂胶提取物的颜色，香气和味道，而不会在长期分配过程中产生沉淀。构成：一种方法包括在44-46℃的温度下用70％乙醇萃取原料的步骤; 向提取液中加入pH调节剂调节pH至6.0-7.0; 加入蛋白酶，脂肪酶，纤维素酶，淀粉酶，葡糖淀粉酶，果胶酶和乳糖酶，并搅拌混合物10-15小时; 将混合物与乙醇混合并过滤掉浮动材料; 并将甘油加入到滤液中并搅拌。优选地，pH控制剂是柠檬酸。甘油与蜂胶提取物的重量比为70-80:20-30。

6. 发明授权

KR100286691B1 사과로부터 추출한 폴리페놀을 포함하는 항진균성 힐패드 失效
标题翻译：含有从苹果提取的多酚的抗真菌脚垫
公开(公告)号：KR100286691B1
公开(公告)日：2001-04-16
申请号：KR1019990002541
申请日：1999-01-27
申请人： 한국유나이티드제약 주식회사
发明人： 배건우 , 김동관 , 장용남 , 박홍철 , 김윤경
IPC分类号： A61L9/04
摘要： 본발명은사과로부터추출한폴리페놀을포함하는항진균성힐패드에관한것이다.

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