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    • 1. 发明公开
    • 방사선이용 나노은입자/유기고분자 복합체의 제조방법 및그 나노은입자/유기고분자 복합체
    • 使用放射性和银纳米颗粒/有机聚合物复合材料的银纳米颗粒/有机聚合物的制备方法
    • KR1020040023159A
    • 2004-03-18
    • KR1020020054807
    • 2002-09-11
    • 최성호이상진이광필
    • 최성호이광필
    • C08K13/04B82Y30/00
    • PURPOSE: A method for preparing silver nanoparticles/organic polymer by using radioactive rays and a silver nanoparticle/organic polymer composite prepared by the method are provided, to obtain a useful silver nanoparticle/organic polymer composite by improving the dispersion of a silver nanoparticle in a polymer. CONSTITUTION: The method comprises the steps of fixing an organic compound having a hydrogen bond on the surface of a silver nanoparticle to prepare a functional silver nanoparticle; and dispersing uniformly the functional silver nanoparticle in an organic polymer whose main chain is hydrophilic to prepare a silver nanoparticle/organic polymer composite. Also the method comprises the steps of mixing a silver salt with a vinyl monomer; and irradiating radioactive rays to the mixture to prepare a silver nanoparticle/organic polymer composite.
    • 目的:提供通过使用放射线制备银纳米颗粒/有机聚合物的方法和通过该方法制备的银纳米颗粒/有机聚合物复合材料,以通过改进银纳米颗粒/有机聚合物的分散性获得有用的银纳米颗粒/有机聚合物复合材料 聚合物。 方案:该方法包括将具有氢键的有机化合物固定在银纳米颗粒的表面上以制备功能性银纳米颗粒的步骤; 并将功能性银纳米粒子均匀分散在主链为亲水性的有机聚合物中,制备银纳米颗粒/有机聚合物复合材料。 该方法还包括将银盐与乙烯基单体混合的步骤; 并向该混合物照射放射线以制备银纳米颗粒/有机聚合物复合物。
    • 2. 发明公开
    • 방사선 그래프트를 이용한 고분자 형광체의 제조방법 및그 고분자 형광체
    • 使用放射性聚酰胺聚合反应生产聚合物磷酸酯及其聚合物磷酸酯
    • KR1020010007762A
    • 2001-02-05
    • KR1020000049939
    • 2000-08-26
    • 이광필최성호
    • 이광필최성호
    • C08F2/54
    • C08F2/46C08F2/54C08F220/18
    • PURPOSE: A process of preparing a polymer phosphor by irradiating radioactive rays (electron beam or gamma ray) to polymer material to introduce a vinyl based monomer and bonding a rare earth ion to the functional group of the vinyl based monomer is provided, which can produce a phosphor at low cost in a simple manner at ordinary temperature. The process also has the advantage of having no complicated manufacturing and inspection processes and installing conveniently. CONSTITUTION: The process for the production of a polymer phosphor comprises the steps of generating radicals by irradiating radioactive rays to a vinyl based monomer having a functional group; introducing acrylic acid having carbonic acid by reacting a mixture solvent of water/methanol to a reaction sample at 30 to 70deg.C; dipping the washed grafted polymer in a caustic soda solution at ordinary temperature for 1 to 5 hr to substitute sodium for a carboxyl group and settling in a rare earth element aqueous solution when the reaction is completed; and washing with distilled water and drying.
    • 目的:提供通过向聚合物材料照射放射线(电子束或γ射线)以引入乙烯基类单体并将稀土离子粘合到乙烯基类单体的官能团上来制备聚合物荧光体的方法,其可以产生 在常温下以简单的方式成本低的磷光体。 该方法的优点是没有复杂的制造和检验过程,安装方便。 构成:聚合物荧光体的制造方法包括以下步骤:通过向具有官能团的乙烯基类单体照射放射线而产生自由基; 在30〜70℃下,通过使水/甲醇的混合溶剂与反应试料反应,导入具有碳酸的丙烯酸; 将洗涤的接枝聚合物在苛性钠溶液中浸渍1至5小时,以替代钠为羧基,并在反应完成时沉降在稀土元素水溶液中; 并用蒸馏水洗涤并干燥。
    • 3. 发明公开
    • 전자폐기물로부터 나노미터 크기의 금을 회수하는 방법 및그 방법으로 회수된 나노미터 크기의 금
    • 从废弃电子部件回收纳米金颗粒的方法和方法回收的纳米金颗粒
    • KR1020040085274A
    • 2004-10-08
    • KR1020030019911
    • 2003-03-31
    • 이광필조성제최성호
    • 이광필최성호
    • C22B11/00B82Y40/00
    • PURPOSE: A method for recovering nano gold particles in a phase of aqueous solution and organic solvent by preparing a gold cyanide aqueous solution from waste electronic parts containing gold and reducing the gold cyanide aqueous solution into gold ions, and nano gold recovered by the method are provided. CONSTITUTION: The method comprises the steps of preparing a gold cyanide solution by dissolving the waste electronic parts into the solution after putting waste electronic parts containing gold into a cyanide solution; and recovering nano gold particles by mixing surfactant with the gold cyanide solution, thereby reducing gold ions, wherein the surfactant is hexadecyltrimethylammonium bromide, sodium dodecyl sulfide, polyvinylalcohol, sodium phosphate or polyvinylpyrrolidone.
    • 目的:通过从含有金的废电子部件制备金氰化物水溶液并将金氰化物水溶液还原为金离子,并通过该方法回收的纳米金,在水溶液和有机溶剂相中回收纳米金颗粒的方法是 提供。 方案:该方法包括在将含有金的废电子部件放入氰化物溶液中之后,将废电子部件溶解在溶液中制备氰化金溶液的步骤; 并通过将表面活性剂与氰化氰溶液混合来回收纳米金颗粒,由此还原金离子,其中表面活性剂是十六烷基三甲基溴化铵,十二烷基硫酸钠,聚乙烯醇,磷酸钠或聚乙烯吡咯烷酮。
    • 4. 发明公开
    • 발광형 평판표시소자용 고분자 칼라필터 필름제조방법
    • 用于制造用于LUMINOUS型平板显示装置的高聚物彩色滤光片的方法
    • KR1020020063414A
    • 2002-08-03
    • KR1020010004067
    • 2001-01-29
    • 손상호최성호김동국이광필
    • 손상호김동국최성호이광필
    • H05B33/00
    • H05B33/10H05B33/20
    • PURPOSE: A method for fabricating a high polymer color filter film for luminous type flat display device is provided to optimize color purity of a fluorescent substance by forming an anti-scratch layer and a diffusion barrier on a surface of a high polymer film. CONSTITUTION: A very small amount of Nd(NO3)3·6H2O and Pr(NO3)3·6H2O is mixed with a metallic silicate or a metallic hydrate such as Si(OC2H5)4), Al(NO3)3· 9H2O, and Al2O3·3SiO2. An aqueous solution is formed by melting the mixture in ethyl alcohol. A high polymer film(12) is reacted with 3-aminopropyltrialkoxysilane within an organic solvent such as toluene in order to improve a surface of the high polymer film(12) such as polyester, poly-carbonate, and polyethylene terephthalate. A hydrolysis is performed to form -Si(OH)n on the surface of the high polymer film(12). A silica layer(-((Si,Al,RE)Ox)n-OH,RE=Nd3+ or Pr3+) is formed on the surface of the high polymer film(12) by performing hydrolysis.
    • 目的:提供一种用于制造发光型平板显示装置的高分子彩色滤光片的方法,通过在高分子膜的表面上形成防刮伤层和扩散阻挡层来优化荧光物质的色纯度。 构成:将非常少量的Nd(NO 3)3·6H 2 O和Pr(NO 3)3·6H 2 O与金属硅酸盐或金属水合物如Si(OC2H5)4),Al(NO3)3·9H2O和 氧化铝·3SiO2。 通过将混合物在乙醇中熔融而形成水溶液。 为了改善聚酯,聚碳酸酯和聚对苯二甲酸乙二醇酯等高分子聚合物膜(12)的表面,高分子膜(12)与有机溶剂如甲苯中的3-氨基丙基三烷氧基硅烷反应。 进行水解以在高分子膜(12)的表面上形成-Si(OH)n。 通过进行水解,在高分子膜(12)的表面上形成二氧化硅层( - ((Si,Al,RE)Ox)n-OH,RE = Nd3 +或Pr3 +)。
    • 5. 发明授权
    • 발광형 평판표시소자용 고분자 칼라필터 필름제조방법
    • 발광형평판시시자용고분자칼라필터필름제조방발광
    • KR100397076B1
    • 2003-09-06
    • KR1020010004067
    • 2001-01-29
    • 손상호최성호김동국이광필
    • 손상호김동국최성호이광필
    • H05B33/00
    • PURPOSE: A method for fabricating a high polymer color filter film for luminous type flat display device is provided to optimize color purity of a fluorescent substance by forming an anti-scratch layer and a diffusion barrier on a surface of a high polymer film. CONSTITUTION: A very small amount of Nd(NO3)3·6H2O and Pr(NO3)3·6H2O is mixed with a metallic silicate or a metallic hydrate such as Si(OC2H5)4), Al(NO3)3· 9H2O, and Al2O3·3SiO2. An aqueous solution is formed by melting the mixture in ethyl alcohol. A high polymer film(12) is reacted with 3-aminopropyltrialkoxysilane within an organic solvent such as toluene in order to improve a surface of the high polymer film(12) such as polyester, poly-carbonate, and polyethylene terephthalate. A hydrolysis is performed to form -Si(OH)n on the surface of the high polymer film(12). A silica layer(-((Si,Al,RE)Ox)n-OH,RE=Nd3+ or Pr3+) is formed on the surface of the high polymer film(12) by performing hydrolysis.
    • 目的:提供一种用于制造用于发光型平板显示装置的高分子滤色膜的方法,以通过在高分子膜的表面上形成抗划痕层和扩散阻挡层来优化荧光物质的色纯度。 构成:将非常少量的Nd(NO3)3·6H2O和Pr(NO3)3·6H2O与金属硅酸盐或金属水合物如Si(OC2H5)4),Al(NO3)3和Al ; middot; 9H2O和Al2O3< 3SiO2。 将该混合物在乙醇中熔化形成水溶液。 为了改善聚合物,聚碳酸酯,聚对苯二甲酸乙二醇酯等高分子膜(12)的表面,使高分子膜(12)与3-氨丙基三烷氧基硅烷在甲苯等有机溶剂中反应。 进行水解以在高分子膜(12)的表面上形成-Si(OH)n。 通过进行水解在高分子膜(12)的表面上形成二氧化硅层( - ((Si,Al,RE)Ox)n -OH,RE = Nd3 +或Pr3 +)。
    • 6. 发明授权
    • 방사선 그래프트를 이용한 고분자 형광체의 제조방법 및그 고분자 형광체
    • 방사선그래프트를이용한고분자형광체의제조방법법그고분자형광체
    • KR100371583B1
    • 2003-02-07
    • KR1020000049939
    • 2000-08-26
    • 이광필최성호
    • 이광필최성호
    • C08F2/54
    • PURPOSE: A process of preparing a polymer phosphor by irradiating radioactive rays (electron beam or gamma ray) to polymer material to introduce a vinyl based monomer and bonding a rare earth ion to the functional group of the vinyl based monomer is provided, which can produce a phosphor at low cost in a simple manner at ordinary temperature. The process also has the advantage of having no complicated manufacturing and inspection processes and installing conveniently. CONSTITUTION: The process for the production of a polymer phosphor comprises the steps of generating radicals by irradiating radioactive rays to a vinyl based monomer having a functional group; introducing acrylic acid having carbonic acid by reacting a mixture solvent of water/methanol to a reaction sample at 30 to 70deg.C; dipping the washed grafted polymer in a caustic soda solution at ordinary temperature for 1 to 5 hr to substitute sodium for a carboxyl group and settling in a rare earth element aqueous solution when the reaction is completed; and washing with distilled water and drying.
    • 目的:提供一种通过向聚合物材料照射放射线(电子束或γ射线)以引入乙烯基类单体并将稀土离子结合到乙烯基类单体的官能团来制备聚合物磷光体的方法,其可以产生 在常温下以简单的方式以低成本获得磷光体。 该过程还具有不需要复杂的制造和检验过程以及方便安装的优点。 构成:生产聚合物荧光体的方法包括以下步骤:通过向具有官能团的乙烯基单体照射放射线产生自由基; 通过在30至70℃下将水/甲醇的混合溶剂与反应样品反应而引入具有碳酸的丙烯酸; 将洗过的接枝聚合物在常温下在苛性钠溶液中浸渍1至5小时,以便用钠代替羧基并在反应完成时沉淀在稀土元素水溶液中; 并用蒸馏水洗涤并干燥。
    • 7. 发明公开
    • 대두 배아로부터 생리활성 물질인 이소플라본의 분리정제방법
    • 从大豆胚芽中分离和纯化异黄酮的方法
    • KR1020010016220A
    • 2001-03-05
    • KR1020000070109
    • 2000-11-17
    • 주식회사 바이오소이텍이광필
    • 최성호이광필
    • A61K36/48A61P35/00A61P39/06A61P3/06
    • C07D311/36A23L2/38A23L33/105A23V2002/00A23V2200/3262A23V2250/2116
    • PURPOSE: Methods for purifying and isolating isoflavone in a high yield are provided. Thereby, isoflavone, which is a physiologically active ingredient, is isolated and purified from the embryo of soy bean obtained when raw soy bean is processed. CONSTITUTION: A method for purifying and isolating isoflavone, which is a physiologically active ingredient from the embryo of soy bean is composed of the following steps: (a) removing fat from the embryo of soy bean; (b) extracting it with alkaline aqueous solution, to remove fiber and protein; (c) flowing the resultant extracted solution onto absorption resin column, to absorb isoflavone and saponin and then isolating these materials with a polar solution (d) drying them under reduced pressure in infrared ray furnace, to obtain a mixture of isoflavone and saponin; and (e) purification and isolation of isoflavone from the mixture using acetone.
    • 目的:提供高产纯化和分离异黄酮的方法。 因此,当生大豆被加工时,从大豆的胚胎中分离和纯化作为生理活性成分的异黄酮。 构成:从大豆胚的生理活性成分中提取和分离异黄酮的方法由以下步骤组成:(a)从大豆胚中除去脂肪; (b)用碱性水溶液萃取,去除纤维和蛋白质; (c)将所得提取液流入吸收树脂柱,吸收异黄酮和皂苷,然后用极性溶液分离这些物质(d)在红外线炉中减压干燥,得到异黄酮和皂苷的混合物; 和(e)使用丙酮从混合物中纯化和分离异黄酮。
    • 10. 发明公开
    • 직액식 필기구
    • 直接液体类型书写工具
    • KR1020150107022A
    • 2015-09-23
    • KR1020140029298
    • 2014-03-13
    • 최성호
    • 최성호
    • B43K8/04B43K8/02
    • B43K8/04B43K3/00B43K8/03
    • 본 발명은 직액식 필기구에 관한 것으로서, 더욱 상세하게는 필심 측으로의 잉크 공급 및 필기구 내측으로의 공기 유입이 적절하고, 원활하게 이루어질 수 있도록 한 직액식 필기구에 관한 것이다.
      그 구성은, 내부 수용공간부를 갖는 몸체; 상기 수용공간부의 하부에 장착되고, 상방 개방된 내부 저장공간부를 갖는 잉크저장체; 상기 잉크저장체의 저장공간부에 삽입된 잉크흡수체; 상기 잉크저장체의 상단부에 장착되어 상기 저장공간부의 상측을 폐쇄하는 커버; 상기 몸체의 하단부에 장착되되, 하단부가 상기 몸체의 하방으로 노출되고, 상단부가 상기 잉크저장체의 저장공간부 측으로 진입하여 상기 잉크흡수체에 삽입되는 필심; 상기 잉크저장체의 내벽에 돌출 형성되되, 상기 잉크저장체의 바닥에서부터 상방 돌출 형성되어 상기 잉크흡수체의 외주면 전부 또는 일부와 접하게 되는 지지부; 상기 잉크저장체의 하면에서 상기 지지부를 관통하도록 형성된 공기유입로; 상기 잉크저장체 및 상기 지지부를 측방 관통하도록 형성되되, 상기 잉크저장체의 중심을 기준으로 방사상 배열되는 둘 이상의 관통공; 및 상기 수용공간부의 상부와 상기 각 관통공을 연결하도록 상기 잉크저장체의 외주면에 형성된 유통로;를 포함하여 이루어진 것을 특징으로 한다.
      이와 같은 구성으로 이루어진 본 발명의 직액식 필기구는 수용공간부의 상부에 저장되어 있던 잉크가 필기시 각 관통공 중 하측에 위치하게 되는 관통공을 통하여 저장공간부로 유입되고, 공기유입로를 통하여 저장공간부로 유입된 공기는 필기시 각 관통공 중 상측에 위치하게 되는 관통공을 통하여 수용공간부의 상부로 유입되는 구조를 갖게 됨으로써, 잉크흡수체로의 잉크 공급 및 수용공간부로의 공기 유입이 적절하고, 원활하게 이루어질 수 있는 효과가 있다.
    • 本发明涉及一种直接液体式书写工具,更具体地涉及一种书写工具,该书写工具具有储存在储存空间的上部的墨水,该储存空间通过位于每个通孔中的下侧的通孔 当书写时具有空气通过空气流入路径流入储存空间的结构的孔在书写时通过位于每个通孔上侧的通孔流入储存空间的上部,从而具有 适当和平稳的空气流入储存空间,并向墨水吸收器供墨。