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1. 发明公开

KR1020060118518A 관능화 플루오로단량체의 수성 유화중합 无效
标题翻译：功能性荧光体的水性乳液聚合
公开(公告)号：KR1020060118518A
公开(公告)日：2006-11-23
申请号：KR1020067010421
申请日：2004-10-08
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 탈러,아른 , 힌트저,클라우스 , 로카스,카이,에이치. , 메르즈,프랜즈 , 햄록,스티븐,제이.
IPC分类号： C08F214/18 , C08F214/00
CPC分类号： C08F214/18 , C08F214/184
摘要： A method is provided for aqueous emulsion co-polymerization of two or more fluoromonomers comprising the steps of: 1) forming an aqueous pre- emulsion by mixing a fluoromonomer according to formula I: F2 C=CF-R1-SO2X (I) wherein R1 is a branched or unbranched perfluoroalkyl, perfluoroalkoxy or perfluoroether group comprising 1-15 carbon atoms and 0-4 oxygen atoms and wherein X is F, Cl or Br, together with 0.001-0.9 molar equivalents of a base, in the absence of added emulsifier; and 2) reacting the pre-emulsion with one or more perfluorinated comonomers in the absence of added emulsifier so as to form a fluoropolymer latex comprising a fluoropolymer wherein more than 1 mol% of monomer units are derived from the fluoromonomer according to formula I. In another aspect, the present invention provides a fluoropolymer derived from the fluoropolymer latex made according to the method of the present invention which is free of added emulsifier. In another aspect, the present invention provides a polymer electrolyte membrane comprising the fluoropolymer made according to the method of the present invention which is free of added emulsifier.
摘要翻译：提供了一种用于两种或更多种含氟单体的水乳液共聚的方法，包括以下步骤：1）通过混合式I的氟单体形成水性预乳液：F2C = CF-R1-SO2X（Ⅰ）其中R1 是在不存在添加的乳化剂的情况下，包含1-15个碳原子和0-4个氧原子的支链或非支链全氟烷基，全氟烷氧基或全氟醚基团，其中X是F，Cl或Br，以及0.001-0.9摩尔当量的碱 ; 和2）在不存在加入的乳化剂的情况下使预乳液与一种或多种全氟化共聚单体反应，以便形成含氟聚合物的含氟聚合物胶乳，其中大于1mol％的单体单元衍生自根据式I的含氟单体。另一方面，本发明提供了衍生自根据本发明的方法制备的含氟聚合物胶乳的氟聚合物，其不含添加的乳化剂。另一方面，本发明提供了一种聚合物电解质膜，其包含根据本发明的方法制备的含氟聚合物，其不含添加的乳化剂。

2. 发明公开

KR1020060120172A 중합체 전해질 막 및 제조 방법 无效
标题翻译：聚合物电解质膜及其制备方法
公开(公告)号：KR1020060120172A
公开(公告)日：2006-11-24
申请号：KR1020067010422
申请日：2004-10-08
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 햄록,스티븐,제이. , 리바드,린다,엠. , 얀드라시츠,미카엘,에이. , 피어폰트,다니엘,엠.
IPC分类号： H01M8/10 , C08J5/22 , C08F214/18
CPC分类号： C08J5/225 , C08F14/18 , C08J2327/12 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M8/1044 , H01M8/1067 , H01M8/1081 , H01M8/109 , Y02P70/56
摘要： Polymer electrolyte membranes such as are used in fuel cells and methods of their manufacture. The polymer electrolyte membranes comprise polymers or blends of polymers having an equivalent weight of less than 1200 and a Tg of between 101 °C and 155 °C.
摘要翻译：用于燃料电池的聚合物电解质膜及其制造方法。聚合物电解质膜包含当量重量小于1200且Tg在101℃至155℃之间的聚合物或共聚物。

3. 发明公开

KR1020040045915A 방향족 이미드 및 방향족 메틸리딘트리스술포닐 화합물,및 그 제조 방법 无效
标题翻译：芳香族酰亚胺和芳香族脒三磺酰基化合物及其制造方法
公开(公告)号：KR1020040045915A
公开(公告)日：2004-06-02
申请号：KR1020047006061
申请日：2002-09-13
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 햄록,스티븐,제이.
IPC分类号： C07C311/48
CPC分类号： C07C303/36 , C07C311/48
摘要： 방향족 화합물 종을 화학식 (I)의 반응물과 반응시켜 방향족 이미드 및 방향족 메틸리딘트리스술포닐 화합물 종을 제조하는 방법이 제공된다.

상기 식에서, Q는 C 또는 N이고; X는 각각 독립적으로 할로겐으로 구성된 군으로부터 선택되고 (통상적으로, F 또는 Cl임); R
1 은 각각 독립적으로 포화되거나 불포화될 수 있고, 직쇄, 분지형 또는 시클릭일 수 있고, 헤테로원자를 갖거나 갖지 않을 수 있고, 중합체성이거나 아닐 수 있고, 할로겐화되거나 되지 않을 수 있고, 플루오르화되거나 되지 않을 수 있으며, 치환되거나 비치환될 수 있는 지방족 및 방향족 기들로 구성된 군으로부터 선택되고; m은 0보다 크고, Q가 N일 때 m+n은 2이며; Q가 C일 때 m+n은 3이다. Ar은 방향족 중합체성 화합물로부터 유도될 수 있다. 또한, 화학식 (Ar-SO
2 )
m -QH-(-SO
2 -R
1 )
n 의 화합물이 제공되며, 여기서 R
1 은 술폰산, 카르복실산 및 포스폰산으로부터 선택된 강산성 기를 포함하며, Ar은 방향족 화합물로부터 유도된 것이다.

4. 发明公开

KR1020070091307A 연료전지 어셈블리용 멤브레인의 마이크로파 어닐링 无效
标题翻译：用于燃料电池组件的膜的微波退火
公开(公告)号：KR1020070091307A
公开(公告)日：2007-09-10
申请号：KR1020077014746
申请日：2005-12-16
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 햄록,스티븐,제이. , 얀드래시츠,마이클,에이. , 펄,아담,엠.
IPC分类号： H01M8/02
CPC分类号： H01M8/1086 , H01B1/122 , H01M8/1023 , H01M8/1025 , H01M8/103 , H01M8/1039 , H01M8/1081 , H01M2300/0082 , H01M2300/0094 , Y02P70/56
摘要： Methods of manufacturing a film involve providing a coating of an ion-containing polymer or ion-containing polymer precursor and annealing the coating to form a film using microwave radiation. Methods of manufacturing an ion-containing membrane for use in a membrane electrode assembly of a fuel cell involve coating a solution of an ion-containing polymer or ion-containing polymer precursor to form a cast membrane of the membrane electrode assembly, and annealing the cast membrane using microwave radiation. The cast membrane may comprise a PEM, for example, which may be incorporated in a fuel cell assembly.
摘要翻译：制造薄膜的方法包括提供含离子的聚合物或含离子的聚合物前体的涂层，并使用微波辐射退火涂层以形成薄膜。制造用于燃料电池的膜电极组件的含离子膜的方法包括涂覆含离子的聚合物或含离子的聚合物前体的溶液以形成膜电极组件的流延膜，并对铸件退火膜使用微波辐射。浇铸膜可以包括例如可并入燃料电池组件中的PEM。

5. 发明公开

KR1020060122829A 미공질 ＰＶＤＦ 필름 및 제조 방법 无效
标题翻译：微波PVDF膜及其制造方法
公开(公告)号：KR1020060122829A
公开(公告)日：2006-11-30
申请号：KR1020067006952
申请日：2004-07-06
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 스미쓰,사만다,디. , 쉽맨,진,에이치. , 플로이드,로버트,엠. , 프리마이어,에이치.,토드 , 햄록,스티븐,제이. , 얀드라시츠,마이클,에이. , 왈튼,데이비드,지.,에스.
IPC分类号： C08J5/18 , C08J9/28 , C08J5/22 , B29C55/00
CPC分类号： H01M8/1044 , B01D67/0009 , B01D67/0011 , B01D67/0016 , B01D67/0027 , B01D69/141 , B01D71/34 , B01D2323/46 , B01D2325/022 , B01D2325/20 , B01D2325/24 , C08J5/2281 , C08J2327/16 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M8/106 , H01M8/1079 , H01M8/1083 , Y02E60/521 , Y02P70/56 , Y10T428/1352 , Y10T428/139 , Y10T428/249953 , Y10T428/249958 , Y10T428/249959 , Y10T428/249978 , Y10T428/249987 , Y10T428/3154
摘要： Shaped microporous articles are produced from polyvinylidene fluoride (PVDF) and nucleating agents using thermally induced phase separation (TIPS) processes. The shaped microporous article is oriented in at least one direction at a stretch ratio of at least approximately 1.1 to 1.0. The shaped article may also comprise a diluent, glyceryl triacetate. The shaped microporous article may also have the micropores filled with a sufficient quantity of ion conducting electrolyte to allow the membrane to function as an ion conductive membrane. The method of making a microporous article comprises the steps of melt blending polyvinylidene fluoride, nucleating agent and glyceryl triacetate; forming a shaped article of the mixture; cooling the shaped article to cause crystallization of the polyvinylidene fluoride and phase separation of the polyvinylidene fluoride and glyceryl triacetate; and stretching the shaped article in at least one direction at a stretch ratio of at least approximately 1.1 to 1.0.
摘要翻译：成型微孔制品由聚偏氟乙烯（PVDF）和使用热诱导相分离（TIPS）工艺的成核剂制备。成形的微孔制品以至少约1.1至1.0的拉伸比在至少一个方向上取向。成型制品还可以包含稀释剂，三乙酸甘油酯。成形的微孔制品也可以具有填充足量的离子导电电解质的微孔，以允许膜用作离子导电膜。制造微孔制品的方法包括熔融共混聚偏二氟乙烯，成核剂和三乙酸甘油酯的步骤; 形成混合物的成型制品; 冷却成型制品以引起聚偏二氟乙烯的结晶和聚偏二氟乙烯和甘油三乙酸酯的相分离; 并且以至少约1.1至1.0的拉伸比在至少一个方向上拉伸成形制品。

6. 发明公开

KR1020060100444A 방향족 술폰 가교를 갖는 중합체 전해질 无效
标题翻译：聚合物电解质与AROMATIC SULFONE CROSSLINKING
公开(公告)号：KR1020060100444A
公开(公告)日：2006-09-20
申请号：KR1020067009976
申请日：2004-11-19
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 징,나이용 , 얀드라시츠,마이클,에이. , 햄록,스티븐,제이.
IPC分类号： C08J5/22 , H01M8/10
CPC分类号： B01D67/0093 , B01D69/141 , B01D71/32 , B01D2323/30 , C08F214/18 , C08F214/26 , C08J5/2237 , C08J2327/18 , H01M8/1023 , H01M8/1039 , H01M8/106 , H01M8/1081 , H01M8/1088 , Y02P70/56
摘要： A method is provided for obtaining crosslinked polymers having pendent sulfonic acid groups by crosslinking through the sulfonic acid groups or their precursors with aromatic crosslinkers or aromatic pendent crosslinking groups to form aromatic sulfones. Such crosslinked polymers may be used to make polymer electrolyte membranes (PEM's) that may be used in electrolytic cells such as fuel cells.
摘要翻译：提供了一种通过使用芳族交联剂或芳香族侧链交联基团通过磺酸基团或其前体进行交联以形成芳族砜来获得具有侧链磺酸基团的交联聚合物的方法。这种交联聚合物可用于制备可用于诸如燃料电池的电解池中的聚合物电解质膜（PEM's）。

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