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1. 发明公开

KR1020090063242A 방사성 불소표지 유기화합물의 제조방법, 합성 장치 및 프로그램 无效
标题翻译：生产放射性荧光标记有机化合物的方法及相关合成装置及方案
公开(公告)号：KR1020090063242A
公开(公告)日：2009-06-17
申请号：KR1020097006970
申请日：2007-08-31
申请人： 니혼 메디피직스 가부시키가이샤
发明人： 히라노게이치 , 이토다쿠 , 이노센토
IPC分类号： C07H5/02 , C07B59/00 , C07B61/00
CPC分类号： C07B59/00 , C07B59/005 , C07H5/02
摘要： A process for producing a radioactive fluorine labeled compound, including the step (S10) of heating a mixture containing [18F] fluoride ions, a phase-transfer catalyst, potassium ions and water in a reactor vessel to thereby evaporate off the water from the mixture, wherein there is provided the step (S12) of, during the heating of the reactor vessel, measuring the temperature of an emission pipe for emission of the water evaporated off, and provided the step (S16) of completing the evaporation-off operation at time determined on the basis of temperature measurement results in the temperature measuring step (S12). Accordingly, in the process for producing a radioactive fluorine labeled organic compound, the content of water present in the mixture can be regulated so as to fall within an appropriate range, thereby realizing a stable yield.
摘要翻译：一种放射性氟标记化合物的制造方法，包括在反应容器中加热含有[18 F]氟离子，相转移催化剂，钾离子和水的混合物的步骤（S10），从而从混合物中蒸发掉水其中，提供了在反应堆加热期间测量用于排出蒸发的水的排放管的温度的步骤（S12），并且提供了完成蒸发关闭操作的步骤（S16）在温度测量步骤中基于温度测量结果确定的时间（S12）。因此，在放射性氟标记的有机化合物的制造方法中，可以将混合物中存在的水的含量调节到适当的范围内，从而实现稳定的产率。

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