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1. 发明授权

KR100328334B1 카르복시 알킬 키틴 및 키토산의 제조 방법 失效
标题翻译：羧甲基壳多糖和壳聚糖的制备方法
公开(公告)号：KR100328334B1
公开(公告)日：2002-03-13
申请号：KR1019990052024
申请日：1999-11-23
申请人： 김공수 , (주)켐바이오 , 조석형
发明人： 김공수 , 조석형
IPC分类号： C08B37/08
摘要： 유기용매/물의용매계에서키틴을알칼리모노클로로아세테이트, 모노클로로아세트산또는알킬모노클로로아세테이트로처리하고, 알카리용액을가함으로써제조하는것을특징으로하는알칼리카르복시알킬키틴및 키토산을제조하는방법에관한것이다.

2. 发明公开

KR1020000007056A 카르복시 알킬 키틴 및 키토산의 제조 방법 失效
标题翻译：羧甲基胆碱和酪蛋白的制备方法
公开(公告)号：KR1020000007056A
公开(公告)日：2000-02-07
申请号：KR1019990052024
申请日：1999-11-23
申请人： 김공수 , (주)켐바이오 , 조석형
发明人： 김공수 , 조석형
IPC分类号： C08B37/08
摘要： PURPOSE: A method for preparing carboxy alkyl chitin and chitosan by swelling in an esterifying reagent and adding alkali is provided which makes easy to produce an industrial production because of the high substitution degree of carboxyalkyl group and the solubility in pH area of weak acid and neutral. CONSTITUTION: 10-50 weight% of Chitin or chitosan based on a mixed solvent is dipped in the mixed solvent of organic solvent and water in a weight ratio of 95/5-50/50 and added with 1 to 0.5-15 mole of alkali monochloroacetate or monochloroacetic acid based on the equivalent of glucose acetamine or glucoseamine of chitin or chitosan and added with the same or 1 to 2 mole of solid or liquid phase(preferably liquid phase) alkali per an etherifying reagent and the etherifying reagent at below 40°C. The product can be used for a food, cosmetics, medical, drug, and agricultural material. The etherifying reagent is alkali monochloroacetate, low molecular alkyl monochloroacetate, propyl monochloroacetate, and isopropyl monochloroacetate.
摘要翻译：目的：提供羧基烷基甲壳素和壳聚糖通过在酯化试剂中溶胀并加入碱的方法，由于羧基烷基的取代度高，在弱酸和中性的pH范围内的溶解度，易于生产工业生产。构成：将基于混合溶剂的甲壳素或壳聚糖10-50重量％以95 / 5-50 / 50的重量比浸入有机溶剂和水的混合溶剂中，并加入1至0.5-15摩尔碱基于等效于甲壳质或壳聚糖的葡萄糖乙胺或葡萄糖胺的一氯乙酸酯或一氯乙酸，并且每个醚化试剂和醚化试剂在低于40℃下加入相同或1至2摩尔固体或液相（优选液相）碱 C。该产品可用于食品，化妆品，医疗，药物和农业材料。醚化试剂是一氯乙酸碱，一氯乙酸低分子烷基酯，一氯乙酸丙酯和一氯乙酸异丙酯。

3. 发明授权

KR100328335B1 4차 암모늄기가 질소-치환된 수용성 키토산 유도체의제조 방법 失效
标题翻译： 4 - 制备季铵基团N-取代的水溶性壳聚糖衍生物的方法
公开(公告)号：KR100328335B1
公开(公告)日：2002-03-13
申请号：KR1019990052023
申请日：1999-11-23
申请人： 김공수 , 조석형 , (주)켐바이오
发明人： 김공수 , 조석형
IPC分类号： C08B37/08
摘要： 유기용매/물의혼합용매계에서키토산에양이온성치환기를도입하여양이온성키토산유도체를제조하는방법에관한것이다. 본발명은글리시딜트리알킬암모늄염, 글리시딜아릴염등을유기용매/물의혼합용매계에서키토산과현탁상태로반응시키는것을특징으로한 양이온성 4차암모늄기가 N-치환된키토산유도체의 제조에관한것이다. 따라서치환도가높고반응생성물의회수가쉽기때문에제조방법이효율적이고경제적으로제조할수 있어서공업적생산이용이하다. 본발명에서제조한양이온성키토산유도체는화장품, 농업용, 섬유처리제, 이온교환수지, 정정기대전방지제, 응집제, 접착제, 잉크등에사용할수 있다.

4. 发明公开

KR1020000007055A 4차 암모늄기가 질소-치환된 수용성 키토산 유도체의제조 방법 失效
标题翻译：季铵组的制备方法 N-取代的可溶性CHITOSAN衍生物
公开(公告)号：KR1020000007055A
公开(公告)日：2000-02-07
申请号：KR1019990052023
申请日：1999-11-23
申请人： 김공수 , 조석형 , (주)켐바이오
发明人： 김공수 , 조석형
IPC分类号： C08B37/08
摘要： PURPOSE: A process for preparing water soluble chitosan derivatives by introducing cationic substituent to chitosan is provided which makes easy to produce an industrial production because of its high substitution degree and easy recovery of reaction product. CONSTITUTION: Chitosan is dispersed in mixed liquid of organic solvent and water and reacted with an ether reagent of glycidyl trialkyl ammonium salt and glycidyl aryl salt or an ether reagent of 3-chloro-2-hydroxy propyl trialkyl ammonium salt, 3-chloro-2-hydroxy propyl aryl ammonium salt, 3-chloro propyl trialkyl ammonium salt, and 3-chloro propyl aryl ammonium salt to give title compound(1). In formula X = Cl, Br, I, SO2, SO3H, NO3, PO4, CH3COOH; Z = Cl, Br and I; R1,R2,R3 = alkyl, aryl, alkylaryl, cycloalkyl, alkoxyalkyl, alkoxyaryl alkoxyalkyl, and alkoxyaryl. The product can be used for cosmetics, an agriculture, a fiber processing agent, an ion exchanger, an antistatic agent, a coagulant, an adhesive, and ink.
摘要翻译：目的：提供通过将阳离子取代基引入壳聚糖制备水溶性壳聚糖衍生物的方法，由于其取代度高，反应产物容易回收，易于生产工业生产。构成：将壳聚糖分散在有机溶剂和水的混合液中，与缩水甘油基三烷基铵盐和缩水甘油基芳基盐的醚试剂或3-氯-2-羟基丙基三烷基铵盐的醚试剂，3-氯-2 - 羟丙基芳基铵盐，3-氯丙基三烷基铵盐和3-氯丙基芳基铵盐，得到标题化合物（1）。式X = Cl，Br，I，SO2，SO3H，NO3，PO4，CH3COOH; Z = Cl，Br和I; R1，R2，R3 =烷基，芳基，烷基芳基，环烷基，烷氧基烷基，烷氧基芳基烷氧基烷基和烷氧基芳基。该产品可用于化妆品，农业，纤维加工剂，离子交换剂，抗静电剂，凝结剂，粘合剂和油墨。

5. 发明公开

KR1019990023496A 광을 이용하여 저분자 키틴, 키토산 및 키틴, 키토산 올리고당을 제조하는 방법 无效
标题翻译：用低分子量甲壳素，壳聚糖和甲壳素以及壳聚糖低聚糖生产光
公开(公告)号：KR1019990023496A
公开(公告)日：1999-03-25
申请号：KR1019980032474
申请日：1998-08-11
申请人： (주)켐바이오 , 조석형 , 김공수
发明人： 김공수 , 조석형 , 한영성
IPC分类号： C08B37/08
摘要： 광을 이용하여 저분자 키틴, 키토산 및 키틴, 키토산 올리고당을 제조하는 방법이 개시되어 있다. 본 발명에 따르면, 1중량부의 키토산을 5∼200중량부의 증류수에 분산시키고 산을 키토산의 아민기의 약 0.5∼10배 몰로 가하여 5∼50℃에서 교반하여 팽윤시킨다. 이 팽윤된 용액을 감마선(γ-선), 자외선(UV) 또는 전자선, 바람직하게는 자외선(UV)으로 조사하여 저분자 키토산과 키토산 올리고당을 제조한다. 그리고, 저분자 키틴 및 키틴 올리고당은 저분자 키토산 및 키토산 올리고당을 아세틸화하여 제조한다. 이렇게 제조한 저분자 키틴, 키토산 및 키틴, 키토산 올리고당은 농업분야에 있어서 식물의 성장 촉진제, 토양개량제, 성장조정제로 유용하고, 식품, 화장품 의약, 시약 등의 분야에서 광범위하게 이용된다.

6. 发明公开

KR1020030081228A 항균섬유 제조방법 无效
标题翻译：制造抗纤维纤维的方法
公开(公告)号：KR1020030081228A
公开(公告)日：2003-10-17
申请号：KR1020030062432
申请日：2003-09-06
申请人： (주)켐바이오 , 조석형
发明人： 조석형 , 박태호
IPC分类号： D06M15/03
摘要： PURPOSE: Provided is a method of manufacturing an antimicrobial fiber which involves excellent antimicrobial capacity, wash resistance and bodily safety, and economic production cost. CONSTITUTION: The method of manufacturing an antimicrobial fiber comprises the steps of: preparing an antimicrobial composition with 5-15 wt.% of quarternized chitosan, 3-10 wt.% of polybasic acid including citric acid, 1-5 wt.% of di,tri-glycidyl ether compound including ethyleneglycol diglycidyl ether, 1-5 wt.% of surface active agent and 65-90 wt.% of water; and dipping the target fiber into 2-3 wt.% of the antimicrobial composition at 30-50 deg.C for 5-30 minutes, and drying it.
摘要翻译：目的：提供一种抗微生物纤维的制造方法，其具有优异的抗菌能力，耐洗涤性和身体安全性以及经济生产成本。构成：制造抗微生物纤维的方法包括以下步骤：制备具有5-15重量％季铵化壳聚糖，3-10重量％多元酸（包括柠檬酸），1-5重量％二，包括乙二醇二缩水甘油醚的三缩水甘油醚化合物，1-5重量％的表面活性剂和65-90重量％的水; 并将目标纤维在30-50℃下浸渍2-3重量％的抗微生物组合物5-30分钟，并干燥。

7. 发明公开

KR1020000058441A 저분자 다당류 및 그의 올리고당의 제조방법 无效
标题翻译：生产低分子多糖和低聚糖的方法
公开(公告)号：KR1020000058441A
公开(公告)日：2000-10-05
申请号：KR1020000027953
申请日：2000-05-24
申请人： 조석형 , 김공수
发明人： 조석형 , 김공수
IPC分类号： C08B30/12
摘要： PURPOSE: An aqueous low molecular polysaccharide and oligosaccharide thereof are provided which can be used in medicines, food-additive, cosmetic, natural pesticide, and etc.. CONSTITUTION: The low molecular polysaccharide and oligosaccharide thereof are produced by a process comprising the steps of: dispersing the polysaccharide such as pectin, chitin, chitosan, alginic acid, cellulose, and etc. in solvent such as pure water, and acetic acid; and adding a mixture of ozone/oxygen to the dispersed solution, wherein an amount of the ozone is 0.01-10 mole (based on the glucose amine of 1 mole).
摘要翻译：目的：提供一种可用于药物，食品添加剂，化妆品，天然农药等的低分子量多糖及其寡糖。构成：低分子多糖及其寡糖通过包括以下步骤的方法制备：将诸如果胶，几丁质，壳聚糖，藻酸，纤维素等多糖分散在溶剂如纯水和乙酸中; 并向分散的溶液中加入臭氧/氧气的混合物，其中一定量的臭氧为0.01-10摩尔（基于1摩尔的葡萄糖胺）。

8. 发明公开

KR1020000012173A 저분자다당류및올리고당의제조방법 无效
标题翻译：制备低分子多糖和低聚糖的方法
公开(公告)号：KR1020000012173A
公开(公告)日：2000-03-06
申请号：KR1019990010444
申请日：1999-03-26
申请人： 김공수 , 조석형
发明人： 김공수 , 조석형
IPC分类号： C08B37/08
摘要： PURPOSE: Low molecular polysaccharide and oligosaccharide are prepared by ultrasonic irradiation of the polysaccharide in a solvent. CONSTITUTION: The polysaccharides such as chitin, chitosan, cellulose and its derivatives, starch and its derivatives, glycogen and its derivatives, heparin hyaluronic acid, alginic acid, gum or pectin are dissolved in the solvent selected from sulfonic acid and benzoic acid etc, followed by irradiation of light, ultrasonic, ultraviolet, gamma ray or electron beam to give polysaccharide and oligosaccharide. For an example, 1.5 g of chitosan is suspended in 100 g of ion exchange water, followed by addition of 0.6 g of acetic acid, and swelled at room temperature. Obtained solution is irradiated by high pressure mercury lamp having 190- 340 nm wave length to give low molecular polysaccharide and oligosaccaharide.
摘要翻译：目的：通过在溶剂中超声辐照多糖制备低分子多糖和寡糖。构成：将几丁质，壳聚糖，纤维素及其衍生物，淀粉及其衍生物，糖原及其衍生物，肝素透明质酸，藻酸，胶或果胶等多糖溶解于选自磺酸，苯甲酸等溶剂中，通过照射光，超声波，紫外线，γ射线或电子束，得到多糖和寡糖。例如，将1.5g壳聚糖悬浮在100g离子交换水中，然后加入0.6g乙酸，并在室温下膨胀。获得的溶液由具有190-340nm波长的高压汞灯照射，得到低分子多糖和寡糖。

9. 发明公开

KR1020000000245A 방향성 고분자 미립자의 제조방법 无效
标题翻译：制备芳族聚合物颗粒的方法
公开(公告)号：KR1020000000245A
公开(公告)日：2000-01-15
申请号：KR1019990042995
申请日：1999-10-06
申请人： 김공수 , (주)이지켐 , 김태경 , 조석형
发明人： 김공수 , 조석형 , 김태경
IPC分类号： C08J3/12
摘要： PURPOSE: A process for manufacturing aromatic polymer granule is provided which gives a substance with a lasting fragrance. CONSTITUTION: 5-30 weight % of Aromatic compound, 5-40 weight % of monomer, 2-10 weight % of functional monomer, and 0-5 weight % of cross-link agent are dispersed in a dispersion medium by using a dispersing agent and polymerized by using an oxidation-reduction initiator or a thermal polymerization initiator at 0-80°C for 1-5 hr to give an acrylic aromatic polymer granule. 7.5-25 mole % of polyol, 15-60 mole % of diisocyanate, and 2.5-15 mole % of stabilizer to give a prepolymer, which is reacted with 5-30 weight % of aromatic compound based on the total weight of prepolymer to give a polyurethane aromatic granule. The granule is used for a sports wear, an underwear, hygienic goods, and sanitary goods.
摘要翻译：目的：提供一种制备芳香族聚合物颗粒的方法，其提供具有持久香味的物质。构成：通过使用分散剂将5-30重量％的芳香族化合物，5-40重量％的单体，2-10重量％的官能单体和0-5重量％的交联剂分散在分散介质中并通过使用氧化还原引发剂或热聚合引发剂在0-80℃下聚合1-5小时，得到丙烯酸芳族聚合物颗粒。 7.5-25摩尔％的多元醇，15-60摩尔％的二异氰酸酯和2.5-15摩尔％的稳定剂，得到预聚物，其与基于预聚物总重量的5-30重量％的芳族化合物反应，得到聚氨酯芳香颗粒。该颗粒用于运动服，内衣，卫生用品和卫生用品。

10. 发明公开

KR1020000063528A 저분자 키토산을 함유한 주류 및 음료 无效
标题翻译：含有低分子基因座的酒精饮料或饮料
公开(公告)号：KR1020000063528A
公开(公告)日：2000-11-06
申请号：KR1020000041551
申请日：2000-07-20
申请人： 조석형 , 김공수
发明人： 조석형 , 김공수
IPC分类号： A23L2/38
摘要： PURPOSE: Method for the preparation of alcoholic liquors and drinks containing low molecular chitosan is provided, which extends the preservation period and lowers one's blood pressure and blood sugar level is provided. CONSTITUTION: Alcoholic liquors and drinks containing chitosan are prepared by adding 0.0001-5.0 wt% of low molecular chitosan in the process of making liquors or drinks including dairy products or adding the chitosan after producing liquors or drinks. The chitosan is at least 85% deacetylated and has a molecular weight of 10,000-100,000.
摘要翻译：目的：提供含有低分子壳聚糖的酒精饮料的制备方法，延长保存期，降低血压，提供血糖水平。构成：含有壳聚糖的酒精和饮料通过在制造含有乳制品的液体或饮料或在生产酒或饮料之后加入壳聚糖的过程中加入0.0001-5.0重量％的低分子壳聚糖来制备。壳聚糖至少85％去乙酰化，分子量为10,000-100,000。

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