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    • 81. 发明公开
    • 불소 가스의 제조방법
    • 氟气的制备方法
    • KR1020100102336A
    • 2010-09-24
    • KR1020090020663
    • 2009-03-11
    • 이택홍(주)거봉한진
    • 이택홍
    • C01B7/20C01B7/00C25B1/24
    • C01B7/20C25B1/245
    • PURPOSE: A manufacturing method of fluorine gas is provided to safely and simply manufacture halogen gas and to manufacture halogen gas without electrolysis process facility. CONSTITUTION: A NaBF4 is melted at the temperature of 400°C. A sample of 200g is collected. At maximum, about 20A, 50V DC power is connected. A carbon rod or a metal rod is connected to as an electrode. Finally, the electrolysis process is executed and F2 gas is produced at the positive pole. The gas which is generated at the positive pole is collected by enabling F2 gas not to be leaked to the outside. A mantle(11) is installed in the lower part of a reactor(12) in order to melt raw materials by heating the reactor. Two electrodes are connected to a power supply part(16). The electrode receives power and the fluorine gas is generated when the electrolysis process starts.
    • 目的:提供氟气的制造方法,以安全和简单地制造卤素气体,并且在没有电解处理设备的情况下制造卤素气体。 构成:NaBF4在400℃的温度下熔化。 收集200g样品。 最多可连接约20A,50V直流电源。 碳棒或金属棒作为电极连接。 最后,执行电解过程,在正极产生F2气体。 通过使F2气体不会泄漏到外部来收集在正极产生的气体。 为了通过加热反应器来熔化原料,在反应器(12)的下部安装地幔(11)。 两个电极连接到电源部分(16)。 电极接收电力,并且在电解过程开始时产生氟气体。
    • 85. 发明公开
    • 기화되는 불산을 최소화한 고순도 삼불화질소 제조용전해조 및 이를 이용한 삼불화 질소의 제조방법
    • 用于制造氮化三氟乙烯的电解液以最小化蒸发氢气的量和使用其的制造方法
    • KR1020070057489A
    • 2007-06-07
    • KR1020050117004
    • 2005-12-02
    • 주식회사 효성
    • 이장원박용철
    • C25B1/24
    • C25B1/245C25B11/0415C25B15/08
    • An electrolyzer for producing high purity nitrogen trifluoride(NF3) at high efficiency and low cost, which has an electrolyzer top plate cooling pipe that removes hydrofluoric acid(HF) generated during the electrolysis for producing nitrogen trifluoride, and a method of producing nitrogen trifluoride using the electrolyzer are provided. In an electrolyzer for producing nitrogen trifluoride(NF3) through molten salt electrolysis, the electrolyzer comprises an electrolyzer body(1), a fluorine resin coated bottom face(2), a fluorine resin coated separation plate(3), an electrolyte(4), a Ni anode(5), a Ni cathode(6), an anode connecting rod(7), a cathode connecting rod(8), a produced nitrogen trifluoride(NF3) outlet(9), a produced hydrogen(H2) outlet(10), an electrolyzer top plate(11), and a cooling pipe, wherein the cooling pipe includes an electrolyzer top plate cooling pipe(13). The electrolyzer top plate cooling pipe is a cooling system capable of controlling temperature of the electrolyzer top plate to 10 to 130 deg.C while proceeding the molten salt electrolysis. The electrolyzer further comprises an electrolyzer sidewall cooling pipe(12) in addition to the electrolyzer top plate cooling pipe to control temperature of the electrolyte to 100 to 130 deg.C during the molten salt electrolysis.
    • 一种高效低成本生产高纯度三氟化氮(NF3)的电解槽,具有去除在生产三氟化氮的电解过程中产生的氢氟酸(HF)的电解槽顶板冷却管,以及使用 提供电解器。 在通过熔盐电解生产三氟化氮(NF 3)的电解槽中,电解槽包括电解槽体(1),氟树脂涂层底面(2),氟树脂涂层分离板(3),电解质(4) ,Ni阳极(5),Ni阴极(6),阳极连接杆(7),阴极连接杆(8),制备的三氟化氮(NF3)出口(9),产生的氢气 (10),电解槽顶板(11)和冷却管,其中冷却管包括电解槽顶板冷却管(13)。 电解槽顶板冷却管是能够在进行熔盐电解的同时将电解槽顶板的温度控制在10〜130℃的冷却系统。 除了电解槽顶板冷却管之外,电解槽还包括电解槽侧壁冷却管(12),以在熔盐电解期间将电解液的温度控制在100〜130℃。