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1. 发明专利

JP2013095703A Method for preparing chlorosulfonyl benzoyl chloride compound 有权
标题翻译：氯化苯甲酰氯化合物的制备方法
公开(公告)号：JP2013095703A
公开(公告)日：2013-05-20
申请号：JP2011240058
申请日：2011-11-01
申请人： Sumitomo Seika Chem Co Ltd , 住友精化株式会社
发明人： FUJITA KOJI , ASHIKAWA MASAYASU
IPC分类号： C07C303/02 , C07C309/89
摘要： PROBLEM TO BE SOLVED: To provide a method for preparing a chlorosulfonyl benzoyl chloride compound useful as a synthetic intermediate for a pharmaceutical raw material etc.SOLUTION: The method for preparing the chlorosulfonyl benzoyl chloride compound represented by formula (2) (wherein R is a hydrogen atom, halogen atom, 1-4C alkyl group, 1-4C alkoxyl group, nitro group or carboxyl group; and Mand Mare each independently a hydrogen atom or alkali metal atom, provided that at least one thereof is an alkali metal atom) comprises chlorinating a metal salt of a sulfobenzoic acid compound, dissolving a metal chloride produced as a byproduct in acid water and subsequently removing the same through liquid separation.
摘要翻译：解决方案：制备用作药物原料等的合成中间体的氯磺酰苯甲酰氯化合物的方法。解决方案：由式（2）表示的氯磺酰基苯甲酰氯化合物的制备方法）（其中R是氢原子，卤素原子，1-4C烷基，1-4C烷氧基，硝基或羧基; M 1 和M 2 各自独立地为氢原子或碱金属原子，条件是其至少一个为碱金属原子）包括将磺基苯甲酸化合物的金属盐氯化，将作为在酸性水中的副产物，随后通过液体分离除去。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP3814696B2 失效
公开(公告)号：JP3814696B2
公开(公告)日：2006-08-30
申请号：JP9099395
申请日：1995-04-17
IPC分类号： C07C303/18 , C07C309/86 , C07C303/02 , C07C303/16 , C07C309/89 , C07C315/04 , C07C317/14 , C07C319/20 , C07C323/66 , C07D213/71 , C07D241/18 , C07D251/22 , C07D263/46 , C07D275/02 , C07D275/03 , C07D277/36

3. 发明专利

JP2003505366A 2-methoxy -4- (N-t- butylamino-carbonyl) novel process for the preparation of benzenesulfonyl chloride 有权
公开(公告)号：JP2003505366A
公开(公告)日：2003-02-12
申请号：JP2001511415
申请日：2000-07-13
申请人：サノフイ−サンテラボ
发明人：ゲンツイ，チヤバ , シモン，カールマーン , シヤーンターネー・チユトル，アンドレア , シユメルコーネー・エシエク，アーゴタ , スボボダ，ジエルジネー , ソモル，テイボルネー , チコーシユ，エーバ , ナジ，ラヨシユ , ハイデユー，フエーリクス , ヘーヤ，ゲルゲイ , ヘーヤ，ゲルゲイネー , ヘルメツ，イシユトバーン
IPC分类号： C07B61/00 , C07C303/06 , C07C303/22 , C07C303/44 , C07C309/60 , C07C309/89
CPC分类号： C07C303/32 , C07C303/06 , C07C303/22 , C07C309/60 , C07C309/89
摘要： (57)【要約】本発明は、ｍ−ヒドロキシ安息香酸をスルホン化し、生じたスルホン酸またはその塩のヒドロキシ基をメチル化し、カルボン酸基及びスルホン酸基を酸クロリド基に変換し、４−クロロスルホニル−３−メトキシベンゾイルクロリドをｔ−ブチルアミンと反応させることによる２−メトキシ−４−（Ｎ−ｔ−ブチルアミノカルボニル）ベンゼンスルホニルクロリドの製造方法に関し、その方法は一般式（ＩＩ）を有する３−メトキシ安息香酸を９６％硫酸を用いてスルホン化し、こうして生じた式（ＩＩＩ）を有する３−ヒドロキシ−４−スルホ安息香酸を一般式（ＩＶ）（式中、Ｚはアルカリ金属またはアンモニウム基である）を有するその塩の形態で分離し、一般式（ＩＶ）を有する化合物を相間移動触媒の存在下ｐＨ約１１．５でメチル化し、一般式（Ｖ）（式中、Ｚは前記と同義である）を有する３−メトキシ−４−スルホ安息香酸モノ塩を一般式ＶＩを有する酸クロリドに変換し、一般式（ＶＩ）を有する化合物を等モルもしくは少し過剰量で使用するｔ−ブチルアミンと酸結合剤の存在下、非プロトン性溶媒中低温で反応させることを特徴とする。

4. 发明专利

JP2000507916A 失效
公开(公告)号：JP2000507916A
公开(公告)日：2000-06-27
申请号：JP51703097
申请日：1996-10-21
IPC分类号： C07D251/16 , A01N47/36 , A01P13/00 , A01P21/00 , C07C309/89 , C07C311/39 , C07D239/42 , C07D239/46 , C07D239/47 , C07D239/52 , C07D251/42 , C07D251/44 , C07D251/46 , C07D521/00 , F21S4/00 , F21V31/00 , H01R33/06

5. 发明专利

JPH11269141A FLUOROBENZOIC ACID CONTAINING SULFUR AND ITS PRODUCTION 失效
公开(公告)号：JPH11269141A
公开(公告)日：1999-10-05
申请号：JP6989098
申请日：1998-03-19
申请人： SUMITOMO SEIKA CHEMICALS
发明人： SAKAMOTO JUNICHI , KANDA NAOAKI , ITSUDA HIROSHI
IPC分类号： C07C311/16 , C07C303/16 , C07C303/38 , C07C309/89 , C07C319/14 , C07C319/20 , C07C323/62
摘要： PROBLEM TO BE SOLVED: To obtain a new 3-fluoro-4-aminosulfonylbenzoic acid and its synthetic intermediate and a new fluorobenzoic acid containing sulfur, and to provide a method for producing them. SOLUTION: The 3-fluoro-4-aminosulfonylbenzoic acid is obtained by reacting (3-fluoro-4-methylthio) benzoic acid with a chlorinating agent to form (3-fluoro-4- chloromethylthio) benzoic acid expressed by the formula [(n) is 1-3 integer], then hydrolyzing (3-fluoro-4-chloromethylthio)benzoic acid to form 3-fluoro-4- mercaptobenzoic acid, oxidizing 3-fluoro-4-mercaptobenzoic acid by a chlorinating agent in the presence of water to form 3-fluoro-4-chlorosulfonylbenzoic acid and then aminating the 3-fluoro-4-chlorosulfonylbenzoic acid.

6. 发明专利

JP2799246B2 失效
公开(公告)号：JP2799246B2
公开(公告)日：1998-09-17
申请号：JP50511891
申请日：1991-02-26
IPC分类号： A01N47/36 , C07C205/58 , C07C205/59 , C07C255/41 , C07C309/89 , C07C323/62 , C07D239/42 , C07D239/46 , C07D239/47 , C07D239/52 , C07D521/00 , C07F7/10

7. 发明专利

JPH09500623A 失效
公开(公告)号：JPH09500623A
公开(公告)日：1997-01-21
申请号：JP50326194
申请日：1994-06-28
IPC分类号： C07D239/42 , A01N47/36 , A01N47/46 , A01P13/02 , C07C309/89 , C07C311/39 , C07C311/65 , C07D239/46 , C07D239/47 , C07D239/48 , C07D239/52 , C07D251/16 , C07D251/22 , C07D251/44 , C07D251/46 , C07D251/48 , C07D251/52 , C07D521/00
摘要： Acylated aminophenylureas, preparation and use as herbicides and plant growth regulators The compounds of the formula I or their salts (I) in which G is a radical G1, G2 or G3 (G1) (G2) (G3) R1 is H or alkyl, R2 is COOH, CSOH or a derivative of the carboxyl or thiocarboxyl group, of 1 to 20 carbon atoms, or acyl of the type CO-R DEG of 1-12 carbon atoms, or an imino, hydrazone or oxime derivative of the group CO-R DEG , and R DEG , R3a, R4a, R3b, R4b, W, X, Y and Z are as defined in claim 1, are suitable as selective herbicides and plant growth regulators in crops. The preparation is carried out in analogy to known processes (see claim 5) by way of intermediates, some of which are new, from the group consisting of benzene-sulfonamides (II), benzenesulfonyl isocyanates (IV) and benzesulfonyl chlorides (VI) and heterocyclically substituted carbamates (III), amines (V) and/or (thio)-isocyanates (XIX).

8. 发明专利

JPH0820511A ANTI-AGING AGENT WHEREIN COMPOUND WITH SULFONIC ACID GROUP IS USED AND METHOD FOR USING IT 失效
公开(公告)号：JPH0820511A
公开(公告)日：1996-01-23
申请号：JP4761195
申请日：1995-03-07
申请人： OREAL
发明人： JIYAN POORU BOERU , JIYANNPIEERU ROOJIE , SERUJIYU FUORESUTEI
IPC分类号： C07D277/66 , A61K20060101 , A61K8/00 , A61K8/30 , A61K8/34 , A61K8/37 , A61K8/46 , A61K8/49 , A61K8/55 , A61K8/92 , A61K8/97 , A61K8/98 , A61K31/00 , A61K31/125 , A61K31/185 , A61K31/19 , A61K31/41 , A61K31/415 , A61K31/4184 , A61K31/42 , A61K31/423 , A61K31/425 , A61K31/428 , A61P17/00 , A61P43/00 , A61Q17/04 , A61Q19/00 , A61Q19/08 , C07C309/04 , C07C309/19 , C07C309/24 , C07C309/29 , C07C309/87 , C07C309/89 , C07D235/18 , C07D263/56 , A61K7/00 , A61K7/48
摘要： PURPOSE: To prevent an intrinsic or a physiological aging of a skin, especially preventing wrinkles and fine wrinkles without accompanying adverse effects such as irritation and redness by adding a specific compound having sulfonic acid to a cosmetic material or a dermatological composition and treating the skin. CONSTITUTION: This aging prevention agent resisting against an intrinsic aging of a skin is obtained by adding a compound having at least one sulfonic acid group which is at least partially non-neutralized to a cosmetic material or a dermatological composition. By using the aging prevention agent, wrinkles and fine wrinkles due to intrinsic aging can be prevented. Further, it is possible to remove dead cells from the skin. As the above compound, a compound of the formula: RSO3 H (R is an optionally substituted aliphatic or aromatic hydrocarbon), especially camphor-10-sulfonic acid, a compound of formula I [B is H or SO3 H; (p) is >=0 and =0 and

9. 发明专利

JPS6087245A 3-CHLORO-4-FLUOROBENZOIC ACID DERIVATIVE 失效
公开(公告)号：JPS6087245A
公开(公告)日：1985-05-16
申请号：JP19664483
申请日：1983-10-20
申请人： IHARA CHEMICAL IND CO
发明人： YOSHIDA YASUO , TANIZAWA NAOHITO , TAKAHASHI HAJIME , SUZUKI TOSHIHIRO
IPC分类号： C07C63/70 , C07C51/00 , C07C67/00 , C07C201/00 , C07C205/58 , C07C301/00 , C07C309/89
摘要： NEW MATERIAL:A 3-chloro-4-fluorobenzoic acid derivative of formula I (X is H or nitro; Y is Cl or chlorosulfonyl). EXAMPLE:3-Chloro-5-chlorosulfonyl-4-fluorobenzoic acid. USE:Having a repellent action on injurious aquatic organisms, and useful as an antistaining coating material, fish net antistaining agent, etc. by preparing the compound as an active constituent in the form of a coating material, solution, emulsion, etc. PREPARATION:For example, 3-chloro-4-fluorobenzoic acid of formula II is reacted with chlorosulfonic acid at 80-160 deg.C, preferably 130-160 deg.C to give the examplified compound in the compound formula I . The examplified compound is reacted with a halogen in the presence of a solvent, e.g. 1,2,4-trichlorobenzene, at the boiling point of the solvent or below, preferably 60-80 deg.C under irradiation with light or in the presence of a catalyst to afford a compound of formula III.

10. 发明专利

JPWO2015125892A1 蛋白質の標識化合物审中-公开
公开(公告)号：JPWO2015125892A1
公开(公告)日：2017-03-30
申请号：JP2016504177
申请日：2015-02-19
申请人：国立大学法人京都大学
发明人：格浜地 , 格浜地 , 和哉松尾 , 和哉松尾 , 真理恵増田 , 真理恵増田 , 雄貴西川 , 雄貴西川
IPC分类号： C07D213/82 , C07C309/77 , C07C309/89 , C07D213/89 , C07D233/60 , C07D241/08 , C07D401/12 , C07D401/14 , C07D475/04 , C07D493/10
CPC分类号： C07C309/77 , C07C309/89 , C07D213/82 , C07D213/89 , C07D239/86 , C07D239/94 , C07D311/16 , C07D311/82 , C07D401/12 , C07D405/12 , C07K1/13 , G01N21/6428 , G01N33/533 , G01N33/542
摘要：本発明は、一般式(I)[化1](式中、Zは[化2]を示す。Y1はN又はCR1を示し、Y2はN又はCR2を示し、Y3はN又はCR3を示し、Y4はN又はCR4を示し、これら式中のR1〜R4のいずれか1つは下記式-(L1)n1-Lg(式中、L1は2価の連結基を示し、n1は0又は1を示し、Lgは蛋白質に対するリガンドを示す)で表す基を示し、R1〜R4の他の3つの基は水素原子又は置換基を示し、R5〜R9のいずれか1つは下記式-(L2)n2-pr(式中、L2は2価の連結基を示し、n2は0又は1を示し、prはプローブを示す)で表す基を示し、R5〜R9の他の4つの基は水素原子又は置換基を示す。)で表される化合物又はその塩を提供する。

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