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    • 6. 发明专利
    • Method for measuring surface area of porous material
    • 测量多孔材料表面面积的方法
    • JPS61118646A
    • 1986-06-05
    • JP24124684
    • 1984-11-14
    • Matsushita Electric Works Ltd
    • YOKOYAMA MASARU
    • G01N15/08
    • G01N15/0893
    • PURPOSE:To make it possible to simply measure the surface area of a specimen, by such a simple mechanism that an adsorbing amount is calculated from the difference between values before and after the pressurization of inert gas calculated by a formula (pressureXvolume/temp.) and the surface area of the specimen is calculated from said adsorbing amount. CONSTITUTION:A specimen 4 to be measured is inserted in the specimen container 3 within a manifold 5 and subjected to degassing treatment under heating and, thereafter, the specimen container 3 is immersed in liquid nitrogen 9. Next, the specimen container 3 is evacuated and inert gas is introduced into said container 3 (to set pressure P1). A piston 2 is moved to reduce the pressure P1 to pressure P2 and the volumetric increase amount at this time is set to DELTAV, the volume of the manifold 10 to Vd, temp. to T and the temp. of liquid nitrogen to TN2 to calculate a dead volume Vs from formula I. Subsequently, inert gas is introduced at relative pressure (x) of about 0.3 and the position of the piston 2 is adjusted so as to obtain 4-5 measured values in a relative pressure range of 0.05-0.3 and an adsorbing amount V is calculated from the difference between values before and after pressurization calculated by a formula (pressureXvolume/temp.) and a monomolecular adsorbing amount is calculated by formula II and the surface area S of the specimen is calculated from formula III.
    • 目的:为了简单地测定试样的表面积,可以通过简单的机理,根据由式(压力×体积/温度)计算的惰性气体加压前后的值之差计算吸附量, 并从所述吸附量计算样品的表面积。 构成:将被测定体4插入到歧管5内的检体容器3内,在加热下进行脱气处理,然后将检体容器3浸渍在氮气9中。接着,将检体容器3抽真空, 将惰性气体引入所述容器3(以设定压力P1)。 移动活塞2以将压力P1降低到压力P2,此时的体积增加量被设定为DELTAV,歧管10的容积为Vd, 到T和温度 的液氮计算出TN2的死体积Vs。随后,在约0.3的相对压力(x)下引入惰性气体,调整活塞2的位置,以获得4-5个测量值 相对压力范围为0.05-0.3,吸附量V由加压之前和之后的压差值(压力X /体积/温度)计算,并且单分子吸附量通过式II计算,并且表面积S 样品从公式III计算。
    • 10. 发明专利
    • Permeameter-porosimeter
    • 渗透仪,孔隙
    • JP2008203268A
    • 2008-09-04
    • JP2008071774
    • 2008-03-19
    • Borgwarner Incボーグワーナー・インコーポレーテッド
    • CHAVDAR BULENT
    • G01N15/08
    • G01N15/0826G01N15/0893
    • PROBLEM TO BE SOLVED: To provide a permeameter-porosimeter capable of measuring permeability in the vertical and lateral directions of porous materials S, R and RR.
      SOLUTION: The permeability measurement is made on compressed or uncompressed samples and is made at room temperature or at elevated temperature. A wide variety of fluid, gas or liquid is used as the penetrating test fluid depending on the application and the porosity of the porous sample. The penetrating test fluid is forcibly supplied to the sample under pressure. The load, the fluid displacement, and the time are recorded and used in the calculation of permeability, porosity, pore size distribution, average pore size and the number of pores per unit area.
      COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题:提供能够测量多孔材料S,R和RR的垂直和横向渗透率的渗透计孔度计。

      解决方案:渗透率测量是在压缩或未压缩样品上进行的,并在室温或高温下进行。 根据多孔样品的应用和孔隙率,使用各种各样的流体,气体或液体作为渗透测试流体。 将渗透性试液在压力下强制供给样品。 记录载荷,流体位移和时间,用于计算渗透率,孔隙率,孔径分布,平均孔径和每单位面积孔隙数。 版权所有(C)2008,JPO&INPIT