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    • 8. 发明专利
    • Autoclave device in high pressure acid leaching step
    • 高压酸浸洗步骤中的自动装置
    • JP2014025143A
    • 2014-02-06
    • JP2012260294
    • 2012-11-28
    • Sumitomo Metal Mining Co Ltd住友金属鉱山株式会社
    • MATSUBARA SATOSHINAKAI OSAMUKYODA YOJISAKAMOTO TAKASHIMAKI KOICHIROISHIKAWA HARUO
    • C22B3/04B01D11/02B01F7/16B01F15/02B01J3/00B01J3/02B01J3/04C22B3/44C22B23/00
    • C22B23/043B01D11/0234B01D11/0257B01D11/0284B01F7/22B01F13/1022B01F15/00863B01J19/006B01J19/0066B01J19/18B01J19/1862B01J2219/00768B01J2219/182B01J2219/1943C22B3/02C22B3/04C22B3/08Y02P10/234
    • PROBLEM TO BE SOLVED: To promote the mixing of raw material slurry and sulfuric acid and to reduce the control value of free sulfuric acid concentration after the exhaust of the mixture.SOLUTION: Regarding an autoclave device 100 in a high pressure acid leaching step in which heated and pressurized raw material slurry and sulfuric acid are stirred with stirring machines 30A to G provided at the respective partition chambers 20A to G in an autoclave body 110 divided to two or more with partitions 10A to F, and, while successively transferring the slurry from the partition chamber on the upstream side to the partition chamber on the downstream side, leaching is progressed, the respective partitions of the autoclave device 100 are provided with liquid passing ports 52A to F for transferring slurry freely openable/closable by liquid passing port doors for slurry transferring, respectively. In the liquid passing ports 52A to F, the height from the lowest part of the autoclave to the center of gravity of the liquid passing port door is 0.1 to 0.3 times the diameter of the autoclave, and they are installed in the position in which the distance from the central line of each partition to the center of gravity of the liquid passing port door is 0.05 to 0.25 times the diameter of the autoclave, and have a shape of not reaching the edge parts of the partition.
    • 要解决的问题:促进原料浆和硫酸的混合,并降低混合物排气后游离硫酸浓度的控制值。解决方案:关于高压酸浸提步骤中的高压釜装置100,其中 将加热加压的原料浆料和硫酸与设置在各分隔室20A〜G的搅拌机30A〜G一起分别分为两层以上的隔板10A〜F的高压釜体110中, 在下游侧的分隔室的上游侧的分隔室进行浸出,高压灭菌装置100的各隔壁设置有液体通过口52A〜F,用于将液体通过口门自由开闭的浆料输送 浆料转移。 在液体通过口52A至F中,从高压釜的最低部分到液体通过口门的重心的高度是高压釜直径的0.1至0.3倍,并且它们被安装在 从每个隔板的中心线到液体通过口门的重心的距离是高压釜直径的0.05至0.25倍,并且具有未到达隔板的边缘部分的形状。