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1. 发明专利

JP2008163311A Thermosetting oxetane composition 审中-公开
标题翻译：热稳定性组合物
公开(公告)号：JP2008163311A
公开(公告)日：2008-07-17
申请号：JP2007281325
申请日：2007-10-30
申请人： Ube Ind Ltd , Yamaguchi Univ , 国立大学法人山口大学 , 宇部興産株式会社
发明人： YAMAMOTO TOSHIKI , WATANABE MASANORI
IPC分类号： C08G65/18
摘要： PROBLEM TO BE SOLVED: To provide a thermosetting oxetane composition excellent in rapid curability and its cured material excellent in mechanical properties.
SOLUTION: The thermosetting oxetane composition comprises (A) an oxetane compound, (B) a curing agent selected from the group consisting of an organic carboxylic acid, an organic carboxylic acid anhydride, and an organic carboxylate, and (C) a rare earth Lewis acid as a curing catalyst. Further a cured material is provided by curing the oxetane composition. The thermosetting oxetane composition cures sufficiently at a low temperature and in a short time with a high curing velocity, and the cured material is excellent in mechanical strength (e.g. tensile strength, elasticity, surface hardness, and bending strength), and durability (e.g. solvent resisitance and weather resisitance).
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供快速固化性优异的热固性氧杂环丁烷组合物及其机械性能优异的固化物。热固性氧杂环丁烷组合物包含（A）氧杂环丁烷化合物，（B）选自有机羧酸，有机羧酸酐和有机羧酸酯的固化剂，（C）稀土路易斯酸作为固化催化剂。此外，通过固化氧杂环丁烷组合物提供固化材料。热固性氧杂环丁烷组合物在低温和短时间内以高固化速度充分固化，并且固化材料具有优异的机械强度（例如拉伸强度，弹性，表面硬度和弯曲强度）和耐久性（例如溶剂抵抗和气候抵抗）。版权所有（C）2008，JPO＆INPIT

2. 发明专利

JP2013014535A Method of producing cyclohexanone 有权
标题翻译：生产环己酮的方法
公开(公告)号：JP2013014535A
公开(公告)日：2013-01-24
申请号：JP2011147917
申请日：2011-07-04
申请人： Yamaguchi Univ , 国立大学法人山口大学 , Ube Industries Ltd , 宇部興産株式会社
发明人： YAMAMOTO TOSHIKI , SUGIMOTO TSUNEMI
IPC分类号： C07C45/33 , C07B61/00 , C07C49/303
摘要： PROBLEM TO BE SOLVED: To provide a method of producing cyclohexanone, by which the cyclohexanone can be manufactured with high efficiency and good selectivity when cyclohexane is oxidized by using a cobalt catalyst.SOLUTION: The method of producing the cyclohexanone includes: bringing the cyclohexane into contact with oxygen or an oxygen-containing gas; and oxidizing a cobalt compound as a catalyst. The oxidation is conducted without a solvent.
摘要翻译：待解决的问题：提供一种环己酮的制备方法，当环己烷通过使用钴催化剂氧化时，可以高效率和高选择性制备环己酮。解决方案：制备环己酮的方法包括：使环己烷与氧或含氧气体接触; 氧化作为催化剂的钴化合物。无溶剂进行氧化。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2011173814A Method for producing amide compound 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：JP2011173814A
公开(公告)日：2011-09-08
申请号：JP2010037662
申请日：2010-02-23
申请人： Ube Industries Ltd , Yamaguchi Univ , 国立大学法人山口大学 , 宇部興産株式会社
发明人： YAMAMOTO TOSHIKI , HORI KENJI , SUMIMOTO MICHINORI , SUGIMOTO TSUNEMI
IPC分类号： C07D201/04 , C07B61/00 , C07D223/10
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an amide compound, which suppresses formation of a by-product and produces an amide compound in a high yield. SOLUTION: In the method for producing an amide compound by a Beckmann rearrangement reaction of an oxime compound, the Beckmann rearrangement reaction is carried out in the presence of a first catalyst of at least one or more of an acidic chloride, an acid anhydride and a Lewis acid and a second catalyst (except a compound specifically selected in the first catalyst) composed of a compound that has an interaction with the nitrogen atom of the oxime compound. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供抑制副产物形成并以高产率产生酰胺化合物的酰胺化合物的制备方法。解决方案：在通过肟化合物的贝克曼重排反应制备酰胺化合物的方法中，贝克曼重排反应在酸性氯化物，酸的至少一种或多种的第一催化剂的存在下进行酸酐和路易斯酸以及由与肟化合物的氮原子相互作用的化合物构成的第二催化剂（除了在第一催化剂中特别选择的化合物）。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2011190207A Method for producing amide compound 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：JP2011190207A
公开(公告)日：2011-09-29
申请号：JP2010056932
申请日：2010-03-15
申请人： Ube Industries Ltd , Yamaguchi Univ , 国立大学法人山口大学 , 宇部興産株式会社
发明人： YAMAMOTO TOSHIKI , SUGIMOTO TSUNEMI
IPC分类号： C07D201/04 , C07B61/00 , C07D225/02
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an amide compound which can produce the amide compound in a high yield by inhibiting the formation of by-products in the method for producing the amide compound by subjecting an oxime compound to the Beckmann rearrangement reaction. SOLUTION: The method for producing an amide compound by subjecting an oxime compound to the Beckmann rearrangement reaction comprises conducting the Beckmann rearrangement reaction in the presence of a triflate compound and trifluoromethanesulfonimide or cobalt borofluoride hexahydrate. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种制备酰胺化合物的方法，该酰胺化合物可以通过抑制酰胺化合物的制备方法中的副产物形成而以高产率生产酰胺化合物，方法是使肟化合物贝克曼重排反应。解决方案：通过使肟化合物进行贝克曼重排反应来制备酰胺化合物的方法包括在三氟甲磺酸酯化合物和三氟甲磺酰亚胺或六氟化硼钴的存在下进行贝克曼重排反应。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2011184332A Method for producing amide compound 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：JP2011184332A
公开(公告)日：2011-09-22
申请号：JP2010049548
申请日：2010-03-05
申请人： Ube Industries Ltd , Yamaguchi Univ , 国立大学法人山口大学 , 宇部興産株式会社
发明人： YAMAMOTO TOSHIKI , SUGIMOTO TSUNEMI
IPC分类号： C07D201/04 , C07B61/00 , C07D223/10
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an amide compound that permits the production of an amide compound simply in a high yield while suppressing formation of by-products. SOLUTION: The method for producing an amide compound comprises subjecting an oxime compound to a Beckmann rearrangement reaction, where a reaction product, obtained by a Beckmann rearrangement reaction in the presence of cyanuric chloride, and silica gel are mixed and agitated to be brought into contact with each other. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种制备酰胺化合物的方法，其允许简单地以高产率生产酰胺化合物，同时抑制副产物的形成。解决方案：酰胺化合物的制备方法包括使肟化合物进行贝克曼重排反应，其中将通过贝克曼重排反应在氰尿酰氯和硅胶存在下得到的反应产物混合并搅拌成互相接触。版权所有（C）2011，JPO＆INPIT

6. 发明专利

JP2011178672A Method of producing amide compound 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：JP2011178672A
公开(公告)日：2011-09-15
申请号：JP2010041788
申请日：2010-02-26
申请人： Ube Industries Ltd , Yamaguchi Univ , 国立大学法人山口大学 , 宇部興産株式会社
发明人： YAMAMOTO TOSHIKI , SUGIMOTO TSUNEMI
IPC分类号： C07D233/10 , B01J31/26 , C07B61/00
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method of producing an amide compound capable of producing the same at a high yield by preventing the production of byproducts. SOLUTION: The method of producing an amide compound by subjecting an oxime compound to a Beckmann rearrangement reaction, is characterized by carrying out the Beckmann rearrangement reaction in the presence of one or more of a first catalyst selected from acid chlorides and Lewis acids, and one or more of a second catalyst selected from trifluoroalkylsulfonic acid anhydrides and zinc oxide. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种制备能够通过防止副产物生产而以高产率生产该酰胺化合物的方法。解决方案：通过使肟化合物进行贝克曼重排反应制备酰胺化合物的方法的特征在于在一种或多种选自酰氯和路易斯酸的第一催化剂存在下进行贝克曼重排反应以及一种或多种选自三氟烷基磺酸酐和氧化锌的第二种催化剂。版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2014136680A Method for producing cyclohexanone 有权
标题翻译：生产环己酮的方法
公开(公告)号：JP2014136680A
公开(公告)日：2014-07-28
申请号：JP2013004792
申请日：2013-01-15
申请人： Yamaguchi Univ , 国立大学法人山口大学
发明人： YAMAMOTO TOSHIKI
IPC分类号： C07C45/33 , C07B61/00 , C07C49/403
摘要： PROBLEM TO BE SOLVED: To provide a method for producing cyclohexanone efficiently and inexpensively, that improves conversion of cyclohexane and selectivity of cyclohexanone, suppresses byproduct formation, and uses various cobalt compounds as a catalyst, in oxidation of cyclohexane.SOLUTION: A method for producing cyclohexanone that subjects raw material cyclohexane to oxidation by bringing it into contact with oxygen or an oxygen-containing gas is characterized in that a mixture of cyclohexane subjected to oxidation conditions and a cobalt compound is added as a catalyst to raw material cyclohexane.
摘要翻译：要解决的问题：为了提供一种有效且廉价地制备环己酮的方法，提高环己烷的转化率和环己酮的选择性，抑制副产物形成，并使用各种钴化合物作为催化剂，在环己烷的氧化中。通过使其与氧气或含氧气体接触使原料环己烷氧化的环己酮的特征在于将作为催化剂的环己烷与钴化合物的混合物作为催化剂加入到原料环己烷中。

8. 发明专利

JP2014193833A METHOD FOR PRODUCING OPTICAL ACTIVITY α-BROMOBENZOYL ACETIC ESTERS 有权
标题翻译：生产光活性α-溴代苯甲酸酯的方法
公开(公告)号：JP2014193833A
公开(公告)日：2014-10-09
申请号：JP2013071123
申请日：2013-03-29
申请人： Yamaguchi Univ , 国立大学法人山口大学 , Tosoh Organic Chemical Co Ltd , 東ソー有機化学株式会社
发明人： YAMAMOTO TOSHIKI , MIYATA TAKUYA , NAGASAKI NOBUTAKA
IPC分类号： C07C67/307 , C07B53/00 , C07B61/00 , C07C69/716
摘要： PROBLEM TO BE SOLVED: To provide a method for producing optical activity α-bromobenzoyl acetic esters at high enantioselectivity using an asymmetric metal complex catalyst.SOLUTION: Benzoyl acetic esters are reacted with a bromination agent in the presence of an asymmetric nickel complex catalyst prepared from a nickel salt and an optical activity bisoxazoline ligand and synthetic zeolite to obtain optical activity α-bromobenzoyl acetic esters at high enantioselectivity.
摘要翻译：要解决的问题：提供一种使用不对称金属配合物催化剂以高对映选择性制备光活性α-溴苯甲酰基乙酸酯的方法。溶液：苯甲酰基乙酸酯与溴化剂在不对称镍络合物催化剂存在下反应，镍盐和光学活性双恶唑啉配体和合成沸石，以获得高对映选择性的光学活性α-溴苯甲酰乙酸酯。

9. 发明专利

JP2013194002A METHOD OF PRODUCING ω-BROMOACETOACETIC ANILIDES 有权
标题翻译：生产ω-溴尿嘧啶的方法
公开(公告)号：JP2013194002A
公开(公告)日：2013-09-30
申请号：JP2012063980
申请日：2012-03-21
申请人： Yamaguchi Univ , 国立大学法人山口大学 , Tosoh Organic Chemical Co Ltd , 東ソー有機化学株式会社
发明人： YAMAMOTO TOSHIKI , MIYATA TAKUYA , NAGASAKI NOBUTAKA
IPC分类号： C07C231/12 , C07C235/80
摘要： PROBLEM TO BE SOLVED: To provide a method of producing ω-bromoacetic anilides which can use not only halogen-based solvent, alcohol solvent or organic acid solvent but also various organic solvents and regioselectively and highly efficiently brominates acetoacetic anilides, thereby producing ω-bromoacetoacetic anilides, the method having a wide range of applying a base.SOLUTION: By reacting acetoacetic anilides with pyridinium bromide perbromide in an organic solvent, ω-bromoacetoacetic anilides are selectively obtained.
摘要翻译：要解决的问题：提供一种不仅可以使用卤素类溶剂，醇溶剂或有机酸溶剂而且可以使用各种有机溶剂并且选择性且高效地溴化乙酰乙酰苯胺的ω-溴乙酰苯胺的生产方法，从而产生ω-溴代乙酰乙酸酰苯胺，该方法具有广泛的施用碱。方法：通过使乙酰乙酰苯胺与溴化吡啶鎓溴化物在有机溶剂中反应，选择性地获得ω-溴代乙酰乙酸酰苯胺。

10. 发明专利

JP2006248910A Method for producing isoxazoline derivative 审中-公开
标题翻译：生产异辛唑衍生物的方法
公开(公告)号：JP2006248910A
公开(公告)日：2006-09-21
申请号：JP2005063713
申请日：2005-03-08
申请人： Tosoh Corp , Yamaguchi Univ , 国立大学法人山口大学 , 東ソー株式会社
发明人： YAMAMOTO TOSHIKI , KAGAWA TAKUMI
IPC分类号： C07D413/06 , C07B61/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a 4,5-trans-isoxazoline derivative.
SOLUTION: The 4,5-trans-isoxazoline derivative is obtained as follows. An imidazolidinone derivative represented by general formula (1) (wherein, R
2 represents an alkyl group, a phenyl group, a substituted phenyl group, a methoxycarbonyl group or an ethoxycarbonyl group; and R
3 represents an alkyl group, a phenyl group or a benzyl group) is reacted with a nitrile oxide precursor represented by general formula (2) (wherein, R
1 represents an alkyl group, a phenyl group, a substituted phenyl group, a methoxycarbonyl group or an ethoxycarbonyl group) in the presence of a Lewis acid catalyst and a base.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种生产4,5-反式异恶唑啉衍生物的方法。解决方案：如下获得4,5-反式异恶唑啉衍生物。由通式（1）表示的咪唑烷酮衍生物（其中，R SB 2表示烷基，苯基，取代的苯基，甲氧基羰基或乙氧基羰基; R“3” 与通式（2）表示的氧化腈前体反应（其中，R SB 1表示烷基，苯基，苯基或苄基）基团，取代的苯基，甲氧基羰基或乙氧基羰基）在Lewis酸催化剂和碱的存在下反应。版权所有（C）2006，JPO＆NCIPI

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