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1. 发明专利

JP2013081938A Manufacturing method of composite semipermeable membrane and composite semipermeable membrane 有权
标题翻译：复合可切割膜和复合膜可制膜的制备方法
公开(公告)号：JP2013081938A
公开(公告)日：2013-05-09
申请号：JP2012210686
申请日：2012-09-25
申请人： Toray Ind Inc , 東レ株式会社
发明人： NAKATSUJI HIROHARU , HENMI MASAHIRO , TOMIOKA HIROKI
IPC分类号： B01D61/12 , B01D61/10 , B01D67/00 , B01D69/06 , C08F2/00
CPC分类号： Y02A20/144
摘要： PROBLEM TO BE SOLVED: To provide a composite semipermeable membrane that has high permeability and to provide a manufacturing method of the same.SOLUTION: The manufacturing method of the composite semipermeable membrane consisting of a microporous support membrane and a separation function layer includes: a step of preparing a substrate in which a sacrificial layer is formed; a step in which a composition layer containing a polymerizable compound is formed on the sacrificial layer; a step in which the microporous support membrane is adhered on the layer of the composition; a step in which the polymerizable compound is polymerized; and a step in which the sacrificial layer is removed.
摘要翻译：待解决的问题：提供一种具有高磁导率的复合半透膜并提供其制造方法。解决方案：由微孔支撑膜和分离功能层组成的复合半透膜的制造方法包括：制备其中形成牺牲层的基板的步骤; 在牺牲层上形成含有可聚合化合物的组合物层的步骤; 微孔支撑膜粘附在组合物层上的步骤; 使聚合性化合物聚合的工序; 以及去除牺牲层的步骤。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP2012210582A Composite semipermeable membrane and method for producing the same 有权
标题翻译：复合可切割膜及其制造方法
公开(公告)号：JP2012210582A
公开(公告)日：2012-11-01
申请号：JP2011077677
申请日：2011-03-31
申请人： Toray Ind Inc , 東レ株式会社
发明人： SHIMURA HARUKI , MINEHARA HIROKI , TOMIOKA HIROKI
IPC分类号： B01D69/12 , B01D71/70 , B01D71/82 , C08J7/04 , C08J7/18
摘要： PROBLEM TO BE SOLVED: To provide a composite semipermeable membrane which has high durability to oxidizing agents, high solute removing property, and stability in continuous operation.SOLUTION: The composite semipermeable membrane is obtained by forming a separation function layer on a microporous support membrane. As raw materials of the separation function layer, a compound (A) in which a hydrolyzable group and a reactive group having an ethylenic unsaturated group are bound to a silicon atom, a compound (B) which is a compound except the compound (A) and has one reactive group having the ethylenic unsaturated group and has an acidic group, and a compound (C) which is a compound except the compound (A) and has two or more reactive groups each having the ethylenic unsaturated group are used, and the separation function layer is formed by condensation of the ethylenic unsaturated groups contained in the compound (A) and polymerization of ethylenic unsaturated group contained in the compound (A), the compound (B) and the compound (C).
摘要翻译：要解决的问题：提供一种对氧化剂具有高耐久性，高溶质去除性和连续操作稳定性的复合半透膜。解决方案：复合半透膜通过在微孔支撑膜上形成分离功能层而获得。作为分离功能层的原料，其中可水解基团和具有烯键式不饱和基团的反应性基团与硅原子结合的化合物（A），化合物（A）以外的化合物（B）并且具有一个具有烯属不饱和基团并具有酸性基团的反应性基团，并且使用除了化合物（A）之外的具有两个或更多个具有烯属不饱和基团的反应性基团的化合物的化合物（C），并且通过化合物（A）中所含的烯属不饱和基团与化合物（A），化合物（B）和化合物（C）中所含的烯属不饱和基团的聚合反应形成分离功能层。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2011255255A Composite semipermeable membrane 有权
标题翻译：复合可切片膜
公开(公告)号：JP2011255255A
公开(公告)日：2011-12-22
申请号：JP2010129412
申请日：2010-06-04
申请人： Toray Ind Inc , Univ Of Tokyo , 国立大学法人東京大学 , 東レ株式会社
发明人： KATO TAKASHI , ICHIKAWA NAOHIRO , NAKATSUJI HIROHARU , HENMI MASAHIRO , TOMIOKA HIROKI , SHIMURA HARUKI
IPC分类号： B01D69/12 , B01D69/10 , B01D71/82 , C08F136/04
摘要： PROBLEM TO BE SOLVED: To provide a composite semipermeable membrane having high water permeability.SOLUTION: The composite semipermeable membrane consists of a porous support membrane and a polymerized liquid crystal thin film, wherein the polymerized liquid crystal presents a bicontinuous cubic structure.
摘要翻译：待解决的问题：提供具有高透水性的复合半透膜。解决方案：复合半透膜由多孔支撑膜和聚合液晶薄膜组成，其中聚合液晶具有双连续的立方结构。版权所有（C）2012，JPO＆INPIT

4. 发明专利

JP2009011891A Manufacturing method of composite semi-permeable membrane 有权
标题翻译：复合渗透膜的制备方法
公开(公告)号：JP2009011891A
公开(公告)日：2009-01-22
申请号：JP2007173755
申请日：2007-07-02
申请人： Toray Ind Inc , 東レ株式会社
发明人： IWAI KENTA , MINEGISHI SHINICHI , TOMIOKA HIROKI
IPC分类号： B01D71/56 , B01D61/02 , B01D69/12 , C02F1/44
摘要： PROBLEM TO BE SOLVED: To manufacture a composite semi-permeable membrane having high blocking performance against boron not dissociated in a neutral region.
SOLUTION: The composite semi-permeable membrane having performance of a water permeation coefficient of 30×10
-12 m
3 /m
2 ×Pa s or less, is manufactured by a method of forming a separation functional layer consisting of cross-linked polyamide by the interface polycondensation reaction of a multifunctional amine compound to a multifunctional acid-halide. Then, the composite semi-permeable membrane is subjected to steam treatment in a steam atmosphere heated to 101-140°C in a pressurized condition of 104-364 kPa. A boron permeation coefficient is reduced to 1/3 or less by this treatment.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：制造在中性区域中没有解离的对硼具有高阻塞性能的复合半透膜。＆lt; P＆gt;解决方案：具有透水系数为30×10 2 2的复合半透膜 ×Pa s以下，通过由多官能胺化合物与多官能酰卤的界面缩聚反应形成由交联聚酰胺构成的分离功能层的方法制造。然后，在104-364kPa的加压条件下，将复合半透膜在加热至101-140℃的蒸汽环境中进行蒸汽处理。通过这种处理，硼渗透系数降低到1/3以下。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JP2014237130A 複合半透膜有权
标题翻译：复合可切片膜
公开(公告)号：JP2014237130A
公开(公告)日：2014-12-18
申请号：JP2014141157
申请日：2014-07-09
申请人：東レ株式会社 , Toray Ind Inc
发明人： OKABE JUN , TOMIOKA HIROKI , HENMI MASAHIRO
IPC分类号： B01D71/70 , B01D69/10 , B01D69/12 , B01D71/26 , C08G77/48
CPC分类号： B01D71/70 , B01D67/0006 , B01D69/02 , B01D69/125 , B01D2323/345 , B01D2325/14 , B01D2325/30 , C08J7/16
摘要：【課題】耐薬品性、分離性能、透水性に優れた複合半透膜の提供する。【解決手段】微多孔性支持膜上に分離機能層を形成してなり、該分離機能層が、(A)エチレン性不飽和基を有する反応性基および加水分解性基がケイ素原子に直接結合したケイ素化合物、ならびに(B)前記ケイ素化合物以外のエチレン性不飽和基を有する化合物から、(A)のケイ素化合物の加水分解性基の縮合ならびに(A)のケイ素化合物および(B)のエチレン性不飽和基を有する化合物のエチレン性不飽和基の重合により、形成された複合半透膜。前記微多孔性支持膜の平均細孔径が1〜100nmである複合半透膜。【選択図】なし
摘要翻译：要解决的问题：提供耐化学性，分离性能和水渗透性优异的复合半透膜。解决方案：在复合半透膜中，通过水解性基团的缩合在细多孔支持膜上形成分离功能层硅化合物（A）和具有烯属不饱和基团的化合物（B）中的具有烯键式不饱和基团的硅化合物（A）的聚合，其中（A）是具有烯属不饱和基团的反应性基团的硅化合物基团和可水解基团直接偶联，（B）是具有除硅化合物之外的烯属不饱和基团的化合物。细多孔支持膜的平均孔径为1-100nm。

6. 发明专利

JP2011078980A Composite semipermeable membrane and manufacturing method of the same 审中-公开
标题翻译：复合膜可制膜及其制造方法
公开(公告)号：JP2011078980A
公开(公告)日：2011-04-21
申请号：JP2011003680
申请日：2011-01-12
申请人： Toray Ind Inc , 東レ株式会社
发明人： TOMIOKA HIROKI , SUGITA KAZUYA , ONE KATSUFUMI
IPC分类号： B01D71/56 , B01D20060101 , B01D61/00 , B01D67/00 , B01D69/02 , B01D69/12 , B01D71/00 , B01D71/82 , C08G69/28
CPC分类号： B01D67/0088 , B01D67/0093 , B01D69/02 , B01D69/125 , B01D71/56 , B01D2323/30 , C02F1/44 , C02F2101/108 , C02F2103/08 , Y02A20/131
摘要： PROBLEM TO BE SOLVED: To provide a composite semi-permeable membrane having a high salt removal rate, capable of separating boron which is non-dissociative in the neutral region at a high removal rate, and a manufacturing method of the same.
SOLUTION: The composite semi-permeable membrane includes a fine porous supporting membrane on which a polyamide separation functional layer is formed. Inside and/or on the surface of the polyamide separation functional layer, a monofunctional amine and an aliphatic acyl group are bonded and/or adsorbed.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种具有高脱盐速率的复合半透膜及其制造方法，能够以高去除率分离在中性区域中非离解的硼。解决方案：复合半透膜包括形成有聚酰胺分离功能层的细多孔支撑膜。在聚酰胺分离功能层的内部和/或表面上结合和/或吸附单官能胺和脂族酰基。版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2011016097A Composite semipermeable membrane 审中-公开
标题翻译：复合可切片膜
公开(公告)号：JP2011016097A
公开(公告)日：2011-01-27
申请号：JP2009163194
申请日：2009-07-09
申请人： Kobe Univ , Toray Ind Inc , 国立大学法人神戸大学 , 東レ株式会社
发明人： MATSUYAMA HIDETO , IMANISHI MASAAKI , HENMI MASAHIRO , TOMIOKA HIROKI
IPC分类号： B01D67/00 , B01D69/12
摘要： PROBLEM TO BE SOLVED: To provide a composite semipermeable membrane which simultaneously satisfies both of separation film performance (solute removability and water permeability) controlled at a high level.SOLUTION: This composite semipeabeable membrane includes a porous support film and an alternate adsorption film. In addition, the composite semipermeable membrane is formed by a process A to form the alternate adsorption film by making a polymer with a positive charge and a polymer with a negative charge alternately adsorbed on the surface of the porous support film, and a process B to bring an aqueous sodium chloride solution into contact with the obtained alternate adsorption film.
摘要翻译：要解决的问题：提供一种同时满足控制在高水平的分离膜性能（溶质去除性和透水性）两者的复合半透膜。解决方案：该复合半导电膜包括多孔载体膜和交替吸附膜。此外，复合半透膜由方法A形成，通过使具有正电荷的聚合物和具有负电荷的聚合物交替吸附在多孔载体膜的表面上形成交替吸附膜，方法B至使氯化钠水溶液与获得的交替吸附膜接触。

8. 发明专利

JP2009030024A Method for producing composite semipermeable membrane 审中-公开
标题翻译：生产可复合膜的方法
公开(公告)号：JP2009030024A
公开(公告)日：2009-02-12
申请号：JP2008146552
申请日：2008-06-04
申请人： Toray Ind Inc , 東レ株式会社
发明人： OKABE ATSUSHI , TOMIOKA HIROKI , NAKATSUJI HIROHARU
IPC分类号： C08G69/46 , B01D69/10 , B01D69/12 , B01D71/56
摘要： PROBLEM TO BE SOLVED: To efficiently remove unreacted components from a composite semipermeable membrane without inhibiting boron removing performances and to produce the composite semipermeable membrane with a high boron removal ratio and little residual amount of the unreacted components.
SOLUTION: A method for production comprises carrying out interfacial polycondensation of a polyfunctional amine with a polyfunctional acid derivative, forming a separation functional layer of a cross-linked aromatic polyamide on a porous supporting membrane and producing the composite semipermeable membrane. In the method, a washing treatment with a wash liquid containing sulfate ions is conducted at 70-100°C after the interfacial polycondensation.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了有效地从复合半透膜中除去未反应的组分而不抑制除硼性能，并制备具有高硼去除率和少量未反应组分残留量的复合半透膜。解决方案：一种生产方法，包括进行多官能胺与多官能酸衍生物的界面缩聚，在多孔支撑膜上形成交联芳香族聚酰胺的分离功能层，制备复合半透膜。在该方法中，在界面缩聚之后，在70-100℃下进行含有硫酸根离子的洗涤液的洗涤处理。版权所有（C）2009，JPO＆INPIT

9. 发明专利

JP2004307373A Method for recovering hydrocarbon 审中-公开
标题翻译：回收烃的方法
公开(公告)号：JP2004307373A
公开(公告)日：2004-11-04
申请号：JP2003101214
申请日：2003-04-04
申请人： Toray Ind Inc , 東レ株式会社
发明人： TOMIOKA HIROKI
IPC分类号： B01D69/12 , B01D11/04 , B01D17/025 , B01D71/56 , B01D71/82 , C07C7/10 , C07C9/14
摘要： PROBLEM TO BE SOLVED: To provide a method for recovering a hydrocarbon, comprising removing solutes from a hydrocarbon / water immiscible solution containing a multi-functional amine, a multi-functional acid halide and a polar functional group-having aliphatic organic compound as the solutes and drained on the production of a composite semi-permeable membrane.
SOLUTION: This method for recovering the hydrocarbon is characterized by comprising a process for contacting the immiscible solution of hydrocarbon solution / aqueous solution containing the multi-functional amine, the multi-functional acid halide and the polar functional group-having aliphatic organic compound as the solutes and the hydrocarbon or the water as a solvent with an alkaline solution and an alcohol, and then separating the alcohol and the alkaline solution transferred to the solutes to remove the solutes.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种回收烃的方法，包括从含有多官能胺，多官能酰卤和极性官能团的脂族有机化合物的烃/水不混溶溶液中除去溶质作为溶质并在生产复合半透膜时排干。解决方案：这种回收烃的方法的特征在于包括使含有多官能胺，多功能酰卤和极性官能团的脂族有机物的烃溶液/水溶液的不混溶溶液接触的方法作为溶质的化合物和烃或作为溶剂的水用碱溶液和醇，然后将转移到溶质中的醇和碱性溶液分离以除去溶质。版权所有（C）2005，JPO＆NCIPI

10. 发明专利

JP2014124567A Composite semipermeable membrane and method for producing the same 审中-公开
标题翻译：复合可切割膜及其制造方法
公开(公告)号：JP2014124567A
公开(公告)日：2014-07-07
申请号：JP2012282098
申请日：2012-12-26
申请人： Toray Ind Inc , 東レ株式会社
发明人： MINEHARA HIROKI , TOMIOKA HIROKI , NAKATSUJI HIROHARU
IPC分类号： B01D71/70 , B01D69/12 , B01D71/58
摘要： PROBLEM TO BE SOLVED: To provide a composite semipermeable membrane excellent in selective separation property of a bivalent ion with respect to a univalent ion, and also excellent in durability.SOLUTION: The composite semipermeable membrane includes a microporous support membrane and a separation functional layer formed on the microporous support membrane. The separation functional layer contains a polymer formed by condensation of a hydrolyzable group of a compound (A) and polymerization of the compound (A) and a compound (B). (A) a silicon compound having a silicon atom, a reactive group having an ethylenic unsaturated group directly coupled with the silicon atom and the hydrolyzable group directly coupled with the silicon atom, and (B) a compound except for the compound (A) and having one or more of each of a basic group and the ethylenic unsaturated group.
摘要翻译：要解决的问题：提供二价离子相对于一价离子的选择性分离性优异的复合半透膜，耐久性优异。解决方案：复合半透膜包括微孔支撑膜和形成的分离功能层在微孔支撑膜上。分离功能层含有通过化合物（A）的可水解基团与化合物（A）和化合物（B）的聚合缩合形成的聚合物。（A）具有硅原子的硅化合物，具有与硅原子直接连接的烯键式不饱和基团的反应性基团和与硅原子直接结合的可水解基团，（B）除化合物（A）和具有碱性基团和烯属不饱和基团中的一个或多个。

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