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1. 发明专利

JP2014172012A Hydrogen separation method 有权
标题翻译：氢分离方法
公开(公告)号：JP2014172012A
公开(公告)日：2014-09-22
申请号：JP2013049020
申请日：2013-03-12
申请人： Tokyo Gas Co Ltd , 東京瓦斯株式会社 , Nagoya Univ , 国立大学法人名古屋大学 , Institute Of National Colleges Of Technology Japan , 独立行政法人国立高等専門学校機構
发明人： SHIRAKI MASAHIRO , KUROKAWA HIDETO , YUGAWA HIROSHI , SUZUKI ASUKA , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： B01D53/22 , B01D71/02
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation method capable of efficiently separating hydrogen at a comparatively low temperature.SOLUTION: In a hydrogen separation method to separate hydrogen by a Pd-Ag alloy film,: Ag content in the Pd-Ag alloy film is 15-30 mass%; and a temperature at separation treatment is lower than 300°C and is the temperature where the hydrogen transmission flux of the Pd-Ag alloy film becomes 80% or more of the hydrogen transmission flux of hydrogen at 400°C. It is preferable that the primary side pressure Pof the Pd-Ag alloy film at the separation treatment is 100-1,000 kPa and P/Pis 1.4-10.
摘要翻译：要解决的问题：提供能够在较低温度下有效分离氢气的氢气分离方法。解决方案：在通过Pd-Ag合金膜分离氢的氢分离方法中，Pd-Ag合金膜中的Ag含量为15-30质量％; 分离处理温度低于300℃，Pd-Ag合金膜的氢传输通量在400℃时为氢气传输通量的80％以上的温度。 Pd-Ag合金膜在分离处理时的初级侧压力P优选为100〜1000kPa，P / Pis为1.4〜10。

2. 发明专利

JP2012066199A Method and device for separating hydrogen 有权
标题翻译：用于分离氢的方法和装置
公开(公告)号：JP2012066199A
公开(公告)日：2012-04-05
申请号：JP2010213773
申请日：2010-09-24
申请人： Institute Of National Colleges Of Technology Japan , Nagoya Univ , Tokyo Gas Co Ltd , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： B01D53/22 , B01D71/02 , C01B3/56 , C22C5/04 , C22C27/02 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a method and device for separating hydrogen using a hydrogen separation membrane large in a hydrogen permeation rate, and excellent in hydrogen embrittlement resistance as well.SOLUTION: The method and device for separating hydrogen uses the hydrogen separation membrane formed of a V alloy containing W and Mo. The hydrogen separation membrane contains preferably ≤30 mol% of W, ≤30 mol% of Mo and a residual part of V. The hydrogen separation membrane contains particularly preferably 0.1-30 mol% of W, 0.1-30 mol% of Mo and the residual part of V. The hydrogen separation membrane contains further preferably 0.1-15 mol% of W, 0.1-15 mol% of Mo and the residual part of V. According to the method and device, hydrogen can be efficiently separated from various kinds of hydrogen-containing gases. Hydrogen can be efficiently separated from gas.
摘要翻译：要解决的问题：提供一种使用氢透过率大的氢分离膜分离氢的方法和装置，并且耐氢脆性优异。解决方案：用于分离氢的方法和装置使用由含有W和Mo的V合金形成的氢分离膜。氢分离膜优选含有≤30mol％的W，≤30mol％的Mo和残余部分的氢分离膜特别优选含有0.1-30mol％的W，0.1-30mol％的Mo和V的残余部分。氢分离膜进一步优选含有0.1-15mol％的W，0.1-15 Mo的摩尔％和V的残余部分。根据该方法和装置，氢可以有效地从各种含氢气体中分离出来。氢气可以有效地与气体分离。版权所有（C）2012，JPO＆INPIT

3. 发明专利

JP2011056485A Hydrogen separation membrane comprising v-w based alloy membrane and hydrogen separation method 有权
标题翻译：包含V-W基合金膜的氢分离膜和氢分离方法
公开(公告)号：JP2011056485A
公开(公告)日：2011-03-24
申请号：JP2009212550
申请日：2009-09-14
申请人： Institute Of National Colleges Of Technology Japan , Nagoya Univ , Tokyo Gas Co Ltd , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , NISHII TAKUMI , SHIRASAKI YOSHINORI , YASUDA ISAMU , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： B01D71/02 , B01D53/22 , C01B3/56 , C22C27/02
摘要： PROBLEM TO BE SOLVED: To provide a new hydrogen separation membrane comprising a V-W based alloy, a hydrogen separation method by the hydrogen separation membrane, and a method of setting a hydrogen separation condition by a specified method.
SOLUTION: The V-W based alloy membrane and the hydrogen separation method by the V-W based alloy membrane are provided. For a condition for the separation of hydrogen by the V-W based alloy membrane, (b) the hydrogen pressure P of a hydrogen atmosphere to the V-W based alloy membrane and (c) a solid solution hydrogen amount C to the V-W based alloy membrane (a) at a temperature T are measured, and (d) a using temperature and hydrogen pressure conditions on the primary side and the secondary side are set by preparing a PCT curve for which the three elements are related on the basis of the actual measurement data of the temperature T, the hydrogen pressure P and the solid solution hydrogen amount C, obtaining the relation of the solid solution hydrogen amount C and the brittle fracture of the V-W based alloy membrane on the basis of the PCT curve, and evaluating a limit solid solution hydrogen amount relating to hydrogen-resistant brittleness.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种包含V-W基合金的新型氢分离膜，通过氢分离膜的氢分离方法和通过指定方法设定氢分离条件的方法。解决方案：提供V-W系合金膜和V-W系合金膜的氢分离方法。对于通过VW基合金膜分离氢的条件，（b）氢气氛的氢压力P向VW系合金膜，（c）为VW系合金膜的固溶氢量C（a ），并且（d）通过根据实际测量数据制备三元素相关的PCT曲线来设定初级侧和次级侧的使用温度和氢气压力条件温度T，氢压P和固溶氢量C，基于PCT曲线获得固溶氢量C与VW基合金膜的脆性断裂的关系，并评价极限固溶体与耐氢脆性相关的氢量。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2013215717A Hydrogen separation membrane and hydrogen separation method 有权
标题翻译：氢分离膜和氢分离方法
公开(公告)号：JP2013215717A
公开(公告)日：2013-10-24
申请号：JP2013046770
申请日：2013-03-08
申请人： Tokyo Gas Co Ltd , 東京瓦斯株式会社 , Nagoya Univ , 国立大学法人名古屋大学 , Institute Of National Colleges Of Technology Japan , 独立行政法人国立高等専門学校機構
发明人： KANEKO YUDAI , SHIRAKI MASAHIRO , KUROKAWA HIDETO , NANBU TOMONORI , MATSUMOTO YOSHIHISA , YUGAWA HIROSHI
IPC分类号： B01D71/02 , B01D53/22 , C01B3/56 , C22C27/02
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation membrane that does not include a surface layer of Pd or Pd alloy.SOLUTION: A hydrogen separation membrane comprises a group 5A metal or its alloy. The hydrogen separation membrane does not include a surface layer of Pd or Pd alloy on the surface thereof. Preferably, the hydrogen separation membrane substantially comprises only the group 5A metal or its alloy. By using the hydrogen separation membrane, 7N or above high purity hydrogen gas can be extracted from 2-7N purity hydrogen gas.
摘要翻译：要解决的问题：提供不包括Pd或Pd合金的表面层的氢分离膜。解决方案：氢分离膜包含5A族金属或其合金。氢分离膜在其表面上不包括Pd或Pd合金的表面层。优选地，氢分离膜基本上仅包含5A族金属或其合金。通过使用氢分离膜，可以从2-7N纯度的氢气中提取7N以上的高纯度氢气。

5. 发明专利

JP2012223754A Hydrogen separation membrane and manufacturing method therefor, and hydrogen manufacturing apparatus 有权
标题翻译：氢分离膜及其制造方法及氢制造装置
公开(公告)号：JP2012223754A
公开(公告)日：2012-11-15
申请号：JP2012067204
申请日：2012-03-23
申请人： Tokyo Gas Co Ltd , Nagoya Univ , Institute Of National Colleges Of Technology Japan , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： B01D71/02 , B01D53/22 , B01D69/10 , B01D69/12 , C01B3/56 , C22C5/04 , C22C27/02
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation membrane in which a middle layer for preventing the mutual diffusion between a base metallic layer and a coated metallic layer, and the oxidation of alloy components of the base metallic layer is formed at low cost, a manufacturing method therefor, and a hydrogen manufacturing apparatus provided therewith.SOLUTION: The hydrogen separation membrane 11 includes the base metallic layer 12 composed of a group 5A metal or its alloy, the middle layer 13 formed on the surface of the base metallic layer 12 and the coated metallic layer 14 formed on the middle layer 13; and the middle layer 13 is formed by anodic oxidation of the base metallic layer 12. The manufacturing method for the hydrogen separation membrane 11 has a step of forming the middle layer 13 by anodic oxidation of the base metallic layer 12 and a step of forming the coated metallic layer 14 on the middle layer 13, and the hydrogen manufacturing apparatus has the hydrogen separation membrane 11.
摘要翻译：要解决的问题：提供一种氢分离膜，其中用于防止基底金属层和涂覆的金属层之间的相互扩散的中间层，并且基底金属层的合金成分的氧化形成为低成本，其制造方法以及与此相应的氢制造装置。解决方案：氢分离膜11包括由5A族金属或其合金构成的基底金属层12，形成在基底金属层12的表面上的中间层13和形成在中间的金属层14 层13; 中间层13由基底金属层12的阳极氧化形成。氢分离膜11的制造方法具有通过基底金属层12的阳极氧化形成中间层13的工序，以及形成中间层13上的涂覆金属层14，氢制造装置具有氢分离膜11.版权所有（C）2013，JPO＆INPIT

6. 发明专利

JP2011144088A Two-stage hydrogen separation type reformer 有权
标题翻译：两级氢分离式改型机
公开(公告)号：JP2011144088A
公开(公告)日：2011-07-28
申请号：JP2010007516
申请日：2010-01-15
申请人： Institute Of National Colleges Of Technology Japan , Nagoya Univ , Tokyo Gas Co Ltd , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , NISHII TAKUMI , SHIRASAKI YOSHINORI , YASUDA ISAMU , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： C01B3/38 , B01D53/22 , B01D63/06 , B01D63/08 , B01D69/10 , B01D71/02 , C01B3/56
摘要： PROBLEM TO BE SOLVED: To obtain a hydrogen separation type reformer in which both of a Pd-alloy hydrogen separation membrane and a group 5A metal-alloy hydrogen separation membrane are used simultaneously to obtain the hydrogen recovery rate higher than those of the conventional reformers.
SOLUTION: The hydrogen separation type reformer is formed by arranging the hydrogen separation membrane on the outer peripheral surface of a boxy or cylindrical porous support or another support comprising a perforated plate, each of which plays a role in supporting the hydrogen separation membrane, and arranging a reforming catalyst layer on the outer periphery of the arranged hydrogen separation membrane. A hydrogen separation system is formed by arranging a plurality of the hydrogen separation type reformers in series. A two-stage hydrogen separation type reformer is characterized in that the Pd-alloy hydrogen separation membrane is used on the upstream side of the gas to be treated and the group 5A metal-alloy hydrogen separation membrane is used on the downstream side of the gas to be treated.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题为了获得氢分离型重整器，其中同时使用Pd合金氢分离膜和5A族金属合金氢分离膜，以获得高于常规改良者。解决方案：氢分离型重整器通过在氢氧化物或圆柱形多孔载体的外周表面上布置氢分离膜或者包括多孔板的另一载体来形成，每个载体起到支撑氢分离膜的作用并且在配置的氢分离膜的外周配置重整催化剂层。通过串联布置多个氢分离型重整器形成氢分离系统。两级氢分离型重整器的特征在于，在合成气体的上游侧使用Pd合金氢分离膜，在气体的下游侧使用5A族金属合金氢分离膜待处理版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2012031021A Method of estimating hydrogen permeation rate, hydrogen manufacturing device, and method of operating the same 有权
标题翻译：计算氢气渗透速率的方法，氢制造装置及其操作方法
公开(公告)号：JP2012031021A
公开(公告)日：2012-02-16
申请号：JP2010172964
申请日：2010-07-30
申请人： Institute Of National Colleges Of Technology Japan , Nagoya Univ , Tokyo Gas Co Ltd , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： C01B3/56 , B01D53/22 , B01D71/02 , G01N15/08
摘要： PROBLEM TO BE SOLVED: To provide a method capable of accurately predicting a hydrogen permeation rate of a hydrogen permeable film, a hydrogen manufacturing device employing the same, and a method of operating the same.SOLUTION: In this method of estimating a hydrogen permeation rate of a hydrogen separation film in a hydrogen separation process of supplying a material gas to a primary chamber and extracting hydrogen having permeated the hydrogen separation film from a secondary chamber, a relationship between a chemical potential difference Δμ of hydrogen between the primary chamber and the secondary chamber obtained from hydrogen partial pressure Pin the primary chamber, hydrogen partial pressure Pin the secondary chamber, and temperatures T thereof, and a hydrogen permeation rate J is previously obtained, and the hydrogen permeation rate when the hydrogen partial pressure in the primary chamber and that in the secondary chamber are assumed to be P'and P', respectively is obtained from the relationship. Gas pressure values and temperatures of the primary chamber and the secondary chamber are controlled so that a product J*A with a value J estimated by the method is set at a target hydrogen extraction amount.
摘要翻译：要解决的问题：提供能够准确地预测氢渗透膜的氢渗透速率的方法，使用该方法的氢制造装置及其操作方法。解决方案：在用于将原料气体供应到初级室并从第二室提取渗透了氢分离膜的氢气的氢分离过程中，估计氢分离膜的氢气渗透速率的方法中，在主室中由氢气分压P 1 获得的主室和次室之间的氢的化学势差Δμ，氢分压P 2 ，并且预先获得其温度T和氢渗透速率J，并且假设主室中的氢分压和次室中的氢分压为从该关系中分别获得P' 1 和P' 2 。控制主室和次室的气压值和温度，使得通过该方法估计的具有值J的乘积J * A被设定为目标氢提取量。版权所有（C）2012，JPO＆INPIT

8. 发明专利

JP2011143375A Hydrogen separation system using 5a group metallic hydrogen separation membrane 有权
标题翻译：使用5A组金属氢分离膜的氢分离系统
公开(公告)号：JP2011143375A
公开(公告)日：2011-07-28
申请号：JP2010007613
申请日：2010-01-16
申请人： Institute Of National Colleges Of Technology Japan , Nagoya Univ , Tokyo Gas Co Ltd , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , NISHII TAKUMI , SHIRASAKI YOSHINORI , YASUDA ISAMU , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： B01D61/58 , B01D53/22 , B01D69/10 , B01D71/02
CPC分类号： Y02C10/10
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation system providing a hydrogen recovery higher than in conventional reformers, by using both a Pd-based alloy hydrogen separation membrane and a 5A group metal alloy hydrogen separation membrane.
SOLUTION: In the hydrogen separation system, the hydrogen separation membrane is disposed on the outer peripheral face of a support body consisting of a casing-like or a cylindrical porous support body or a support body consisting of a perforated plate serving for supporting the hydrogen separation membrane, and a plurality of hydrogen separation reformers formed by arranging a reforming catalyst layer are serially arranged on the outer periphery of the hydrogen separation membrane. The hydrogen separation membrane uses the Pd-based alloy hydrogen separation membrane on the upstream of the treating object gas, and the 5A group metal alloy hydrogen separation membrane on the downstream of the treating object gas.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：通过使用Pd基合金氢分离膜和5A族金属合金氢分离膜，提供比常规重整器高的氢回收率的氢分离系统。解决方案：在氢气分离系统中，氢分离膜设置在由壳体或圆柱形多孔支撑体或由用于支撑的多孔板组成的支撑体的支撑体的外周面上氢分离膜和通过配置重整催化剂层形成的多个氢分离重整器连续排列在氢分离膜的外周。氢分离膜在处理对象气体的上游使用Pd基合金氢分离膜，在处理对象气体的下游使用5A族金属合金氢分离膜。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2010240637A HYDROGEN SEPARATING SYSTEM USING Nb MEMBRANE AND PERIODIC TABLE 5A GROUP METAL ALLOY MEMBRANE 审中-公开
标题翻译：使用Nb膜和周期表5A的氢分离系统组合金属合金膜
公开(公告)号：JP2010240637A
公开(公告)日：2010-10-28
申请号：JP2010007428
申请日：2010-01-15
申请人： Institute Of National Colleges Of Technology Japan , Nagoya Univ , Tokyo Gas Co Ltd , 国立大学法人名古屋大学 , 東京瓦斯株式会社 , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , NISHII TAKUMI , SHIRASAKI YOSHINORI , YASUDA ISAMU , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： B01D53/22 , B01D71/02 , C01B3/38 , C01B3/56
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen producing system for separating hydrogen from a gas of low-concentration hydrogen with a small difference of partial pressure of hydrogen making use of the characteristic of a Nb membrane, and to provide a hydrogen producing system for reforming methane in a gas of low-concentration hydrogen containing methane of high temperature and producing and separating hydrogen from the obtained reformed gas with a small difference of partial pressure of hydrogen. SOLUTION: The system is for separating hydrogen using the Nb membrane from the gas of low-concentration hydrogen at room temperature and atmospheric pressure generated from a generator of the gas of low-concentration hydrogen at room temperature. The hydrogen separating system includes (a) the Nb membrane, (b) a heating means equipped with a burner, (c) a means for supplying the upstream side of the Nb membrane with the gas of low-concentration hydrogen at room temperature and (d) a means for recovering hydrogen in the downstream side of the Nb membrane. The hydrogen separating system is for selectively separating hydrogen from the gas of low-concentration hydrogen by heating the Nb membrane to 300-500°C with (b) the heating means equipped with a burner under (e) the condition that the solid solubility of hydrogen in the Nb membrane C(H/M) is 0.26 or lower. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种利用Nb膜的特征，以小的氢分压差从低浓度氢气中分离氢的氢气制备系统，并提供产氢用于在含有高温甲烷的低浓度氢气的气体中重整甲烷的系统，并从所获得的重整气体中分离氢并以较小的氢分压差。
解决方案：该系统用于在室温下从低浓度氢气中分离氢气，室温下由低浓度氢气发生器产生的大气压。氢分离系统包括（a）Nb膜，（b）装有燃烧器的加热装置，（c）在室温下向Nb膜的上游侧供应低浓度氢气的装置和 d）在Nb膜的下游侧回收氢的方法。氢分离系统用于通过将Nb膜加热至300-500℃来选择性地从低浓度氢气中分离出氢气，（b）在（e）下配备有燃烧器的加热装置，条件是固体溶解度 Nb膜C（H / M）中的氢为0.26以下。版权所有（C）2011，JPO＆INPIT

10. 发明专利

JP2014133696A Two-stage hydrogen separation type reformer 有权
标题翻译：两级氢分离式改型机
公开(公告)号：JP2014133696A
公开(公告)日：2014-07-24
申请号：JP2014045870
申请日：2014-03-10
申请人： Tokyo Gas Co Ltd , 東京瓦斯株式会社 , Nagoya Univ , 国立大学法人名古屋大学 , Institute Of National Colleges Of Technology Japan , 独立行政法人国立高等専門学校機構
发明人： KUROKAWA HIDETO , NISHII TAKUMI , SHIRASAKI YOSHINORI , YASUDA ISAMU , MORINAGA MASAHIKO , YUGAWA HIROSHI , NANBU TOMONORI , MATSUMOTO YOSHIHISA
IPC分类号： C01B3/38 , B01D53/22 , B01D69/10 , B01D69/12 , B01D71/02 , C01B3/56 , C01B32/50
CPC分类号： Y02C10/10
摘要： PROBLEM TO BE SOLVED: To obtain a hydrogen separation type reformer in which both of a Pd-based alloy hydrogen separation membrane and a group 5A metal alloy hydrogen separation membrane are used so that the hydrogen recovery rate higher than those of the conventional reformers can be obtained.SOLUTION: A two-stage hydrogen separation type reformer being the hydrogen separation type reformer is constituted so that the hydrogen separation membrane is disposed on the outer peripheral surface of a support, which plays a part in supporting the hydrogen separation membrane and comprises a cylindrical porous support or a perforated plate, and a reforming catalyst layer is disposed on the outer periphery of the hydrogen separation membrane. The Pd-based alloy hydrogen separation membrane is used on the upstream side of the gas to be treated and the V alloy or Ta alloy hydrogen separation membrane, which can be used without being fractured brittlely even under 0.10 MPa (1 atmosphere as absolute pressure) or higher, is used on the downstream side of the gas to be treated.
摘要翻译：要解决的问题为了获得使用Pd基合金氢分离膜和5A族金属合金氢分离膜两者的氢分离型重整器，使得比常规重整器高的氢回收率可以是得到的溶液。作为氢分离型重整器的两级氢分离型重整器构成为使氢分离膜配置在支撑氢分离膜的部分的支撑体的外周面上，圆柱形多孔载体或多孔板，并且重整催化剂层设置在氢分离膜的外周。 Pd系合金氢分离膜用于待处理气体的上游侧以及V合金或Ta合金氢分离膜，即使在0.10MPa（绝对压力为1个大气压）下也能够脆性地使用，或更高，用于待处理气体的下游侧。

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