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    • 2. 发明专利
    • Melted quartz glass and method for manufacturing the same
    • 熔融石英玻璃及其制造方法
    • JP2014005204A
    • 2014-01-16
    • JP2013215033
    • 2013-10-15
    • Tosoh Corp東ソー株式会社Tohos Sgm Kk東ソ−・エスジ−エム株式会社
    • ARAI KAZUYOSHITAKAHATA TSUTOMUHASHIMOTO SHINKICHIUCHIDA MASATOYAMADA SHUSUKEHARADA YOSHINORIHORIKOSHI HIDEHARU
    • C03C3/06C03B3/02C03B5/235C03B20/00
    • C03C4/0085C03B19/066C03B20/00C03B2201/03C03B2201/04C03C3/06C03C4/10C03C2201/23C03C2201/50C03C2201/54Y02P40/57
    • PROBLEM TO BE SOLVED: To inexpensively provide a melted quartz glass which is suitably usable for various optical materials that use ultraviolet rays, visible rays and infrared rays, a member for manufacturing a semiconductor, a member for manufacturing a liquid crystal, a member for manufacturing MEMS, and a glass substrate for a liquid crystal, has a high transmittance to ultraviolet rays, visible rays and infrared rays, has high purity and high heat resistance, and a low diffusion speed of a Cu ion.SOLUTION: In a melted quartz glass, an internal transmittance to ultraviolet light having a wavelength of 245 nm in a thickness of 10 mm is 95% or more, an OH content is 5 ppm or less, and each content of Li, Na, K, Mg, Ca and Cu is less than 0.1 ppm. Preferably, Al is contained therein in weight ratio of 2 ppm or less, the viscosity at 1,215°C is 10Pa s or more, and a diffusion coefficient of a Cu ion in a depth of 20 to 100 μm from the surface in thermal diffusion of the Cu ion at 1,050°C in the atmosphere is 1×10cm/sec or less. Such a melted quartz glass can be obtained by previously converting raw material silica powder into cristobalite, and then melting the cristobalitized silica powder in a non-reducing atmosphere.
    • 要解决的问题:为了廉价地提供适用于使用紫外线,可见光和红外线的各种光学材料的熔融石英玻璃,用于制造半导体的部件,用于制造液晶的部件,制造用部件 MEMS和用于液晶的玻璃基板对紫外线,可见光线和红外线具有高透射率,具有高纯度和高耐热性以及较低的Cu离子扩散速度。在熔融石英玻璃 对于厚度为10mm的波长为245nm的紫外线的内部透射率为95%以上,OH含量为5ppm以下,Li,Na,K,Mg,Ca,Cu的含量为 小于0.1ppm。 优选地,其中含有2重量%以下的Al,1,215℃下的粘度为10Pa·s以上,Cu离子的热扩散表面的深度为20〜100μm的扩散系数 大气中1,050℃的Cu离子为1×10cm /秒以下。 这种熔融的石英玻璃可以通过将原料二氧化硅粉末预先转化为方英石,然后在非还原气氛中熔化澄清二氧化硅粉末来获得。
    • 6. 发明专利
    • Fused quartz glass
    • FUSED QUARTZ玻璃
    • JP2009120436A
    • 2009-06-04
    • JP2007295261
    • 2007-11-14
    • Tohos Sgm KkTosoh Corp東ソ−・エスジ−エム株式会社東ソー株式会社
    • HARADA YOSHINORIYAMADA SHUSUKETAKAHATA TSUTOMU
    • C03B20/00
    • C03B19/01C03B2201/03Y02P40/57
    • PROBLEM TO BE SOLVED: To provide a fused quartz glass having a low dusting property which is suitable for use in a member for manufacturing a semiconductor, a member for manufacturing a liquid crystal and a member for manufacturing a MEMS (micro-electro-mechanical system) by using plasma etching at a low cost. SOLUTION: The fused quartz glass excellent in a low dusting property is made by using a natural silica in which the ratio of elements having corrosion resistance to a gaseous halide as the local concentration of a defective part due to foreign substances is less than 0.4 wt.% and preferably the concentration of both Zr and Al at a defective part due to foreign substances is less than 0.1 wt.%. The fused quartz glass of this kind is manufactured by flowing the melt to generate a shearing stress inside the melt in manufacturing the fused quartz glass and a minute defective part due to foreign substances observed by a schlieren method in the fused quartz glass of this kind has a length of 1.3 mm or more. COPYRIGHT: (C)2009,JPO&INPIT
    • 要解决的问题:提供适用于半导体制造部件的粉尘特性低的熔融石英玻璃,制造液晶的部件和用于制造MEMS的部件(微电子 机械系统),通过以低成本使用等离子体蚀刻。 解决方案:通过使用其中具有耐腐蚀性的元素与卤化物的比例作为由于异物引起的缺陷部分的局部浓度的比例小于 0.4重量%,优选由于异物而在缺陷部分的Zr和Al的浓度小于0.1重量%。 这种熔融石英玻璃通过使熔体流动而在熔融石英玻璃的制造中在熔融物内部产生剪切应力,并且由于在这种熔融石英玻璃中由于schlieren法观察到的异物而产生的微小缺陷部分具有 长度为1.3mm以上。 版权所有(C)2009,JPO&INPIT
    • 7. 发明专利
    • Fused quartz glass and process for producing the same
    • 熔融石英玻璃及其制造方法
    • JP2008208017A
    • 2008-09-11
    • JP2007235031
    • 2007-09-11
    • Tohos Sgm KkTosoh Corp東ソ−・エスジ−エム株式会社東ソー株式会社
    • ARAI KAZUYOSHITAKAHATA TSUTOMUHASHIMOTO SHINKICHIUCHIDA MASAHITOYAMADA SHUSUKEHARADA YOSHINORIHORIKOSHI HIDEHARU
    • C03B20/00
    • C03C4/0085C03B19/066C03B20/00C03B2201/03C03B2201/04C03C3/06C03C4/10C03C2201/23C03C2201/50C03C2201/54Y02P40/57
    • PROBLEM TO BE SOLVED: To inexpensively provide a fused quartz glass capable of being preferably used for preparing various optical materials utilizing ultraviolet ray, visible light and infrared ray, a member for producing a semiconductor, a member for producing a liquid crystal, a member for producing MEMS(micro-electro-mechanical system), and a glass substrate for the liquid crystal, and having high permeability of ultraviolet ray, visible light and infrared ray, high purity, high heat resistance, and a low diffusion velocity of Cu ions.
      SOLUTION: The fused quartz glass has an internal transmittance of not less than 95% for ultraviolet ray of 245 nm wavelength at 10 mm depth, a viscosity coefficient at 1,215°C of not less than 10
      12.0 Pa s, a Cu ion diffusion coefficient in a depth of 20-100 μm from the surface in Cu ion heat diffusion in the atmosphere at 1,050°C of not greater than 1×10
      -10 cm
      2 /sec, an OH content of not grater than 5 ppm, a Li, Na, K, Mg, Ca and Cu content of each less than 0.1 ppm, and preferably contains 2 ppm of Al by weight ratio. The fused quartz glass can be obtained by converting a raw material silica powder to cristobalite in advance and thereafter fusing the same in a non-reducing atmosphere.
      COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题为了廉价地提供一种能够优选用于制备利用紫外线,可见光和红外线的各种光学材料的熔融石英玻璃,用于制造半导体的部件,用于制造液晶的部件, 用于制造MEMS(微电子机械系统)的构件和用于液晶的玻璃基板,并且具有高的紫外线,可见光和红外线的透过性,高纯度,高耐热性和低扩散速度 Cu离子。 解决方案:熔融石英玻璃对于10mm深度的245nm波长的紫外线具有不小于95%的内部透射率,1,215℃下的粘度系数不小于10 SP SP 12.0 SP > Pa时,在1050℃的大气中的Cu离子热扩散中与表面的深度为20-100μm的Cu离子扩散系数不大于1×10 -10 < SP> 2 /秒,不超过5ppm的OH含量,Li,Na,K,Mg,Ca和Cu的含量均小于0.1ppm,优选含有2ppm的Al重量比 。 熔融石英玻璃可以通过将原料二氧化硅粉末预先转化为方英石,然后在非还原气氛中将其熔融而获得。 版权所有(C)2008,JPO&INPIT
    • 9. 发明专利
    • Method for producing ito sintered compact
    • 用于生产ITO烧结紧密度的方法
    • JP2007302556A
    • 2007-11-22
    • JP2007194347
    • 2007-07-26
    • Tosoh Corp東ソー株式会社
    • UCHIUMI KENTAROTAKAHATA TSUTOMUYOSHIMURA RYOJI
    • C04B35/457C04B35/00C23C14/34
    • PROBLEM TO BE SOLVED: To provide a method for producing an Indium Tin Oxide (ITO) sintered compact inexpensively by utilizing scrapped ITO sintered compact through a simple process. SOLUTION: The method for producing an ITO sintered compact comprises the steps of pulverizing an ITO sintered compact into granules of 0.5 mm or less, mixing the ITO granules with a virgin powder substantially consisting of indium, tin and oxygen, forming and sintering the resultant mixture. Alternatively, the method comprises the steps of pulverizing an ITO sintered compact into granules of 0.5 mm or less, mixing the ITO granules with virgin powder substantially consisting of indium and oxygen, forming and sintering the resultant mixture. COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题:通过简单的方法利用废弃的ITO烧结体,廉价地提供一种生产氧化铟锡(ITO)烧结体的方法。 解决方案:制造ITO烧结体的方法包括将ITO烧结体粉碎成0.5mm以下的颗粒的步骤,将ITO颗粒与基本上由铟,锡和氧组成的原始粉末混合,形成和烧结 所得混合物。 或者,该方法包括以下步骤:将ITO烧结体粉碎成0.5mm以下的颗粒,将ITO颗粒与基本上由铟和氧组成的原始粉末混合,形成并烧结所得到的混合物。 版权所有(C)2008,JPO&INPIT
    • 10. 发明专利
    • Black-colored quartz glass, its producing method, and member using the quartz glass
    • 黑色彩色玻璃,其生产方法和使用QUARTZ玻璃的会员
    • JP2006027930A
    • 2006-02-02
    • JP2004206457
    • 2004-07-13
    • Tosoh Corp東ソー株式会社
    • TODOKO SHIGEHISAUCHIDA MASAHITOTAKAHATA TSUTOMU
    • C03C4/02C03B20/00C03C3/06
    • C03B19/06C03B19/066C03B20/00
    • PROBLEM TO BE SOLVED: To provide highly light-shielding black-colored quartz glass which is substantially free from metal impurities and has mechanical and thermal characteristics equivalent to those of transparent quartz glass, in other words, bending strength, hardness, coefficient of thermal expansion, thermal conductivity and the like, equivalent to those of the transparent quartz glass; and to provide a method for producing the same.
      SOLUTION: The black-colored quartz glass is silica glass in which crystalline carbon fine particles having an average diameter of 0.05-1 μm are dispersed in an amount of 0.05-2 wt.% and which has a density of 2.15-2.21 g/cm
      3 . The black-colored quartz glass has a transmittance in a wavelength region of 200-10,000 nm of ≤1% when its thickness is 1 mm. The black-colored quartz glass is obtained by mixing an amorphous silica powder having an average diameter of 0.1-1 μm and containing hydroxy group in a content of ≥50 ppm and the crystalline carbon fine particles having an average diameter of 0.05-1 μm so that the addition amount of the carbon fine particles to the weight of the silica powder becomes 0.05-2 wt.%, then forming the resulting mixture, and sintering the formed body at 1,100-1,500°C.
      COPYRIGHT: (C)2006,JPO&NCIPI
    • 要解决的问题:为了提供基本上没有金属杂质的高度遮光的黑色石英玻璃,并且具有与透明石英玻璃相当的机械和热特性,换句话说,弯曲强度,硬度,系数 的热膨胀,导热性等,与透明石英玻璃相当; 并提供其制造方法。 解决方案:黑色石英玻璃是二氧化硅玻璃,其中平均直径为0.05-1μm的结晶碳细颗粒以0.05-2重量%的量分散,密度为2.15-2.21 克/厘米 3 。 黑色石英玻璃的厚度为1mm时,在200〜10000nm的波长范围内具有≤1%的透射率。 黑色石英玻璃是通过混合平均直径为0.1-1μm,含有≥50ppm的羟基的无定形二氧化硅粉末和平均直径为0.05-1μm的结晶碳微粒而获得的 碳微粒相对于二氧化硅粉末的添加量为0.05〜2重量%,然后形成所得混合物,并在1100-1,500℃烧结成形体。 版权所有(C)2006,JPO&NCIPI