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    • 8. 发明专利
    • Method for sintering titanium-based powder compact
    • 烧结钛酸钡粉末的方法
    • JP2006104559A
    • 2006-04-20
    • JP2004296274
    • 2004-10-08
    • Toyota Central Res & Dev Lab Inc株式会社豊田中央研究所
    • TAKAMIYA HIROYUKIKONDO MIKIO
    • B22F3/10C22C14/00
    • PROBLEM TO BE SOLVED: To provide a method for sintering a titanium-based powder compact capable of producing a titanium-based sintered compact having reduced contamination caused by oxygen or the like even in an inert gas atmosphere and having satisfactory mechanical properties.
      SOLUTION: A titanium-based powder compact 1 compacted from raw material powder essentially consisting of titanium is sintered by a heating furnace using a graphite heater in an inert gas atmosphere under the pressure of atmospheric pressure or higher, under an oxygen concentration of ≤50 ppm, and under a CO concentration of ≤100 ppm. At this time, the titanium-based powder compact 1 is supported by a supporting member 2 and is installed inside a case 3 made of graphite. The supporting member 2 is composed of a base part 20 and a reaction control part 21 comprising at least either Y
      2 O
      3 or ZrO
      2 , and comes into contact with the titanium-based powder compact 1 via the reaction control part 21. Further, a sintering promotion member 5 made of titanium for forming a sintering promotion atmosphere is arranged around the titanium-based powder compact 1.
      COPYRIGHT: (C)2006,JPO&NCIPI
    • 解决问题的方法:提供一种即使在惰性气体气氛中也能够制造具有由氧等引起的污染减少并具有令人满意的机械性能的钛基烧结体的钛基粉末成形体的烧结方法。 解决方案:由基本上由钛组成的原料粉末压实的钛基粉末成形体1在大气压或更高压力的惰性气体气氛中使用石墨加热器的加热炉在氧气浓度为 ≤50ppm,CO浓度≤100ppm时。 此时,钛基粉末压块1由支撑构件2支撑并安装在由石墨制成的壳体3内。 支撑构件2由基部20和包括至少Y 2 SB 3 O 3 / SB 3或ZrO 2 SB 2的反应控制部21组成, 并且经由反应控制部21与钛基粉末压块1接触。此外,在钛基粉末成形体1的周围配置有由用于形成烧结促进气氛的钛制成的烧结促进部件5。 (C)2006,JPO&NCIPI