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1. 发明专利

JPS6193192A Preparation of powdery oligosaccharide 失效
标题翻译：制备低密度脂蛋白
公开(公告)号：JPS6193192A
公开(公告)日：1986-05-12
申请号：JP21389484
申请日：1984-10-12
申请人： Mitsubishi Chem Ind Ltd , Sanwa Kosan Kk
发明人： YOSHINO ZENICHI , SHIODA TSUYOSHI , NAKAZAWA ISAO , MURAYAMA MASAKATSU , KIHARA TETSUAKI
IPC分类号： C07H1/06 , C07H3/06
摘要： PURPOSE: To obtain powdery oligosaccharide, economically in an industrial scale, by carrying out the chromatographic separation, concentration, drying, and recovery successively in respective specific methods.
CONSTITUTION: A pseudo-moving bed is formed in a bed filled with a cation exchange material, by circulating a fluid through a bed in a manner to form an adsorption zone, a refining zone, a desorption zone and a concentration zone from the upstream- side to the downstream side, and shifting the positions of the feeding zone and the extraction zone of the liquid intermittently toward downstream-side. An aqueous solution containing maltose and an oligosaccharide is passed through said pseudo- moving bed under the following conditions. The ratio (ϕ
2 ) of the volume flow rate to the apparent volume flow rate of the cation exchange material in the refining zone is controlled to 0.3W0.5, and the ratio (ϕ
4 ) in the concentration zone is controlled to 0.3W0.6. The solution is separated into the adsorbed maltose solution and the non- adsorbed oligosaccharide solution continuously by the above chromatographic process. The aqueous solution of the oligosaccharide is made to contact with hot air in the form of mist in a drying chamber furnished with an atomizer, a hot-air inlet, and an air outlet, and is pulverized. The powder of the oligosaccharide is separated from the exhaust discharged from the drying chamber.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过各种具体方法连续进行色谱分离，浓缩，干燥和回收，从经济上获得工业规模的低分子量寡糖。构成：在填充有阳离子交换材料的床上形成假移动床，通过使流体通过床形成从上游侧形成吸附区，精炼区，解吸区和浓缩区的方式，侧向下游侧，并且将液体的供给区域和提取区域的位置间歇地向下游侧移动。含有麦芽糖和寡糖的水溶液在以下条件下通过所述伪移动床。将体积流量与澄清区中阳离子交换材料的表观体积流量的比率（phi2）控制在0.3-0.5，将浓度区域中的比例（phi4）控制在0.3-0.6。通过上述色谱法将溶液连续分离成吸附的麦芽糖溶液和未吸附的寡糖溶液。使寡糖的水溶液与设置有雾化器，热风入口和空气出口的干燥室中的雾状热空气接触，并被粉碎。寡糖的粉末与从干燥室排出的废气分离。

2. 发明专利

JPH0544477B2 失效
公开(公告)号：JPH0544477B2
公开(公告)日：1993-07-06
申请号：JP21389484
申请日：1984-10-12
申请人： SANWA KOSAN KK , MITSUBISHI CHEM IND
发明人： YOSHINO ZENICHI , SHIODA TSUYOSHI , NAKAZAWA ISAO , MURAYAMA MASAKATSU , KIHARA TETSUAKI
IPC分类号： C07H1/06 , C07H3/06

3. 发明专利

JPS5478361A REMOVING METHOD FOR SULFATE ADHERED ON AIR PREHEATER 失效
公开(公告)号：JPS5478361A
公开(公告)日：1979-06-22
申请号：JP14640177
申请日：1977-12-06
申请人： MITSUBISHI CHEM IND
发明人： KONYA TAKESHI , KOIKE SAKAE , SAKURADA HIKARI , KIHARA TETSUAKI
IPC分类号： B01D53/56 , B01D53/34 , F23J15/00
摘要： PURPOSE:To enable to easily remove the above mentioned sulfate, by inducing power of a fixed inactive subustance in combstion exhaust gas of low temperature zone. CONSTITUTION:More than one kind of the following powders are added in combustion exhaust gas from the space between the coal economizer and air preheater, at the publicly known fuel oil combustion boilder carrying out reducing decomposition of NOx in the exhaust gas, by adding ammonia in more than 700 deg.C of combustion exhaust gas produced from combustion chamber. More than one kind of powders of diatomaceous earth, zirconium sand, pearlite and titanium oxide and/or metal powders, such as each powder of Al, copper and iron, are used for the above adding powders. Also, about 0.1-100mu of grain diameter is preferable and a good result is obtained by adding in such a concentration in the exhaust gas as about 100mg-20g/Nm .

4. 发明专利

JPH0458320B2 失效
公开(公告)号：JPH0458320B2
公开(公告)日：1992-09-17
申请号：JP19125983
申请日：1983-10-13
申请人： MITSUBISHI CHEM IND
发明人： KIHARA TETSUAKI , MURAYAMA MASAKATSU , TANABE TAKAYUKI
IPC分类号： C13K11/00 , C13K3/00

5. 发明专利

JPH059080B2 失效
公开(公告)号：JPH059080B2
公开(公告)日：1993-02-03
申请号：JP17239483
申请日：1983-09-19
申请人： MITSUBISHI CHEM IND
发明人： SHIODA TSUYOSHI , KIHARA TETSUAKI , NAKAZAWA ISAO , MURAYAMA MASAKATSU
IPC分类号： C13K7/00 , C07H3/04

6. 发明专利

JPS6083600A ADSORPTIVE SEPARATION OF FRUCTOSE 失效
公开(公告)号：JPS6083600A
公开(公告)日：1985-05-11
申请号：JP19125983
申请日：1983-10-13
申请人： MITSUBISHI CHEM IND
发明人： KIHARA TETSUAKI , MURAYAMA MASAKATSU , TANABE TAKAYUKI
IPC分类号： C13K11/00 , C13K3/00

7. 发明专利

JPS6067000A MALTOSE SEPARATING METHOD 失效
公开(公告)号：JPS6067000A
公开(公告)日：1985-04-17
申请号：JP17239483
申请日：1983-09-19
申请人： MITSUBISHI CHEM IND
发明人： SHIODA TSUYOSHI , KIHARA TETSUAKI , NAKAZAWA ISAO , MURAYAMA MASAKATSU
IPC分类号： C13K7/00 , C07H3/04

8. 发明专利

JPS5478362A REMOVING METHOD FOR SULFATE ADHERED ON AIR PREHEATER 失效
公开(公告)号：JPS5478362A
公开(公告)日：1979-06-22
申请号：JP14640277
申请日：1977-12-06
申请人： MITSUBISHI CHEM IND
发明人： KONYA TAKESHI , KOIKE SAKAE , SAKURADA HIKARI , KIHARA TETSUAKI
IPC分类号： B01D53/56 , B01D53/34 , F23J15/00
摘要： PURPOSE:To enable to easily remove the above mentioned sulfate, by inducing a fixed inorganic powder in combustion exhaust gas of low temperature zone. CONSTITUTION:More than one kind of the following inorganic powders are added from the space between the coal economizer and air preheater, at the publicly known fuel oil combustion boiler carrying out reducing decomposition of NOx in the exhaust gas, by adding ammonia in more than 700 deg.C of the exhaust gas produced from combustion chamber. More than one kind of zeolite, bentonite, kaolin, allophane, Shirasu, fly ash, talc, wallastonite, blast furnace slag, red mud, agalmatolite and mica, are used for the above inorganic powder. Also, about 0.1-100mu of grain diameter is preferable and a good result is obtained by adding in such a concentration in the exhaust gas as about 1-200mg/Nm3.

9. 发明专利

JPH059079B2 失效
公开(公告)号：JPH059079B2
公开(公告)日：1993-02-03
申请号：JP16619283
申请日：1983-09-09
申请人： MITSUBISHI CHEM IND
发明人： SHIODA TSUYOSHI , KIHARA TETSUAKI , IMANARA TOORU
IPC分类号： C13K7/00 , C13B20/14 , C13K11/00 , C13K13/00

10. 发明专利

JPS60130400A SEPARATION AND PURIFICATION OF SUGARS BY ION EXCHANGE RESIN 失效
公开(公告)号：JPS60130400A
公开(公告)日：1985-07-11
申请号：JP23698383
申请日：1983-12-15
申请人： MITSUBISHI CHEM IND
发明人： KIHARA TETSUAKI , NAKAZAWA ISAO , TANABE TAKAYUKI
IPC分类号： C13B35/06 , C13K7/00 , C13K11/00 , C13K13/00

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