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1. 发明专利

JPS58192809A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58192809A
公开(公告)日：1983-11-10
申请号：JP7034982
申请日：1982-04-28
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N33/22 , A01N47/36
摘要： PURPOSE: A herbicide having improved safety and prolonged effect, and a wide herbicidal spectrum, containing a substituted phenylsulfonylurea derivative and 2,4-dichlorophenyl 3-methoxy-4-nitrophenyl ether as active ingredients.
CONSTITUTION: A herbicide containing a compound[e.g., N-2-biphenylylsulfonyl, N-(4-methoxy-6-methyl-pyrimidine-2-yl)urea]shown by the formula I [X is O or single bond; Y is H or Cl; R is group shown by the formula II or formula III(R
1 and R
2 are methyl or methoxy)] and a compound shown by the formula IVin a weight ratio of 1:(14W2). The herbicide shows such an excellent synergistic effect as each of the components is not expected to have, and can destroy various kinds of troublesome weeds with a small amount of application. It has low toxicity to warm-blooded animals, no phytotoxicity to cultivated plants, and effective as a soil treatment especially for weeds in paddy fields before germination, and a foliar treatment also used for soil treatment.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：具有改善安全性和延长效果的除草剂，以及含有取代苯基磺酰脲衍生物和2,4-二氯苯基3-甲氧基-4-硝基苯基醚作为活性成分的宽除草光谱。构成：式I [X是O或单键]所示的含有化合物[例如N-2-联苯基磺酰基，N-（4-甲氧基-6-甲基 - 嘧啶-2-基）脲] Y是H或Cl; R为式II或式III所示的基团（R 1和R 2为甲基或甲氧基）]和式IV所示的化合物，其重量比为1：（14-2）。除草剂显示出这样的优异的协同效果，因为每种组分都不会预期具有并且可以以少量的应用破坏各种麻烦的杂草。对温血动物毒性低，对栽培植物无植物毒性，特别是作为土壤处理，特别是萌发前稻田杂草，也用于土壤处理的叶面处理。

2. 发明专利

JPS58183688A Oxadiazole derivative, its preparation and herbicide 失效
标题翻译： OXADIAZOLE DERIVATIVE，其制备和除草剂
公开(公告)号：JPS58183688A
公开(公告)日：1983-10-26
申请号：JP6470082
申请日：1982-04-20
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , SAITOU JIYUNICHI , KUME TOYOHIKO , YASUI KAZUTOMI
IPC分类号： A01N43/82 , A01N43/836 , C07D413/12
CPC分类号： C07D413/12 , A01N43/82
摘要： NEW MATERIAL:The compound of formula I (R is lower alkyl, lower alkoxy- lower alkyl, aralkyl, or aryloxyalkyl).
EXAMPLE: 3-Methyl-5-{1-[4-( 5-trifluoromethyl-2-pyridyloxy )phenoxy]ethyl}-1, 2, 4- oxadiazole.
USE: Herbicide exhibiting excellent herbicidal activity especially to gramineous weeds, and suppressing the sprouting of hardly controllable perennial gramineous weeds for a long period.
PROCESS: The objective compound of formula I can be prepared by reacting the compound of formula II (M is H or alkali metal) with the compound of formula III(X is halogen) in a solvent such as water, hexane, methanol, etc. in the presence of an acid acceptor (e.g. alkali metal hydroxide, etc.) at 0W100°C.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：新材料：式Ⅰ化合物（R为低级烷基，低级烷氧基 - 低级烷基，芳烷基或芳氧基烷基）。实施例：3-甲基-5- {1- [4-（5-三氟甲基-2-吡啶氧基）苯氧基]乙基} -1,4-恶二唑。用途：除草剂具有优异的除草活性，特别是对禾本科杂草，并且长期抑制几乎可控的多年生禾本科杂草的发芽。方法：式I的目的化合物可以通过使式II化合物（M为H或碱金属）与式III化合物（X为卤素）在溶剂如水，己烷，甲醇等中反应来制备。在0-100℃下在酸受体（例如碱金属氢氧化物等）存在下进行。

3. 发明专利

JPS58192808A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58192808A
公开(公告)日：1983-11-10
申请号：JP7034382
申请日：1982-04-28
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N33/22 , A01N47/36
摘要： PURPOSE: A herbicide showing extremely excellent cooperative action and synergistic action, exhibiting properly selective herbicidal action, having improved prolonged effect, obtained by blending a substituted phenylsulfonylurea derivative with a diphenyl ether derivative.
CONSTITUTION: A herbicide comprising a substituted phenylsulfonylurea derivative [e.g., N-2-biphenylylsulfonyl, N'-(4-methoxy-6-methyl-pyrimidine-2-yl)urea, etc.] shown by the formula I [X is O, or single bond; Y is H or Cl; R is group shown by the formula II or formula III (R
1 and R
2 are methyl or methoxy)] and a diphenyl ether derivative (e.g., 2,4-dichlorophenyl 3-methoxycarbonyl-4-nitrophenyl ether, etc.) shown by the formula IV(X is Cl or CF
3 ; Y is H or Cl; Z is H, alkoxy, etc.) as active ingredients.
EFFECT: Having improved safety, showing a wide herbicidal spectrum and durability with improved effect.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：通过将取代的苯基磺酰脲衍生物与二苯醚衍生物混合而获得的除草剂具有非常优异的协同作用和协同作用，表现出适当的选择性除草作用，具有改善的延长效果。构成：由式I表示的包含取代的苯基磺酰脲衍生物[例如N-2-联苯基磺酰基，N' - （4-甲氧基-6-甲基 - 嘧啶-2-基）脲等]的除草剂[X为O ，或单键; Y是H或Cl; R为式II或式III所示的基团（R 1和R 2为甲基或甲氧基）]和二苯醚衍生物（例如2,4-二氯苯基3-甲氧基羰基-4-硝基苯基醚等（X为Cl或CF 3; Y为H或Cl; Z为H，烷氧基等））作为活性成分。效果：安全性提高，除草效果好，耐久性好。

4. 发明专利

JPS58188806A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58188806A
公开(公告)日：1983-11-04
申请号：JP7034782
申请日：1982-04-28
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N57/14 , A01N57/16
摘要： PURPOSE: A herbicide, containing a substituted phenylsulfonylurea derivative and O,O-dipropyl-S-2-methylpiperidinocarbonylmethyl phosphorodithioate, etc. as active constituents, and exhibiting potentiating and synergistic action.
CONSTITUTION: A herbicide containing a substituted phenylsulfonylurea derivative of formula I [X is O or direct bond; Y is H or Cl; R is formula II (R
1 and R
2 are methyl or methoxyl) or formula III] and O,O-dipropyl S-2-methylpiperidinocarbonylmethyl phosphorodithioate of formula IV or O, O-dimethyl S-[N- (4-chlorophenyl)-N-isopropyl-carbamoylmethyl]-phosphorothioate of formula V. The resultant mixed herbicide has improved safety, exhibits a remarkable herbicidal activity, a wide herbicidal spectrum and lasting improved efficacy, and is suitable particularly to a pre-emergence soil treating agent and foliar and soil treating agent for weeds in paddy fields.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：一种除草剂，含有取代苯基磺酰脲衍生物和O，O-二丙基-S-2-甲基哌啶羰基甲基二硫代磷酸酯等作为活性成分，具有增效作用和协同作用。构成：含有式I的取代的苯基磺酰基脲衍生物的除草剂[X是O或直接键; Y是H或Cl; R为式Ⅱ（R 1和R 2为甲基或甲氧基）或式III]和式IV的O，O-二丙基S-2-甲基哌啶基羰基甲基二硫代磷酸酯或O，O-二甲基S- [N- 4-氯苯基）-N-异丙基 - 氨基甲酰基甲基] - 硫代磷酸酯。所得混合除草剂具有改善的安全性，显示出显着的除草活性，广泛的除草谱和持久改善的功效，并且特别适合于出苗前的土壤水稻杂草处理剂和叶面和土壤处理剂。

5. 发明专利

JPS58185506A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58185506A
公开(公告)日：1983-10-29
申请号：JP6806382
申请日：1982-04-24
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N47/36
摘要： PURPOSE: To obtain a herbicide exhibiting excellent synergistic effect for the control of weeds at a low rate of application compared with the separate use of each component, and having excellent long activity and safety, by using an active component composed of a mixture of a novel substituted phenylsulfonylurea derivative and another compound.
CONSTITUTION: The active component of the objective herbicide is a mixture of (A) a novel substituted phenylsulfonylurea derivative of formula I [X is O or single bond; Y is H or Cl; R is group of formula II (R
1 and R
2 are CH
3 or OCH
3 ) or formula III] and (B) S-ethylhexahydro-1H-azepine-1-carbothioate of formula IV or S-(α,α-dimethylbenzyl)-piperidine-1-carbothioate of formula Vwhich are known herbicides, at a weight ratio of preferably 1:(20W2). The mixture has low toxicity and no phytotoxicity to crops, and can be used as a pregermination soil-treating agent or foliar and soil-treating agent for the weeds in paddy field.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：为了获得与单独使用各成分相比，以较低的施用率显示出优异的防治杂草的协同效果，并且具有优异的长活性和安全性的除草剂，通过使用由新颖的混合物组成的活性成分取代的苯基磺酰脲衍生物和另一种化合物。构成：目的除草剂的活性组分是（A）式I的新型取代的苯基磺酰基脲衍生物的混合物[X是O或单键; Y是H或Cl; R为式IV基团（R 1和R 2为CH 3或OCH 3）或式III]和（B）式IV的S-乙基六氢-1H-吖庚因-1-硫代硫酸酯或S-（α，α 二甲基苄基） - 哌啶-1-硫代硫酸酯，其为已知的除草剂，重量比优选为1：（20-2）。该混合物毒性低，对作物无植物毒性，可用作稻田杂草的预发芽土壤处理剂或叶面和土壤处理剂。

6. 发明专利

JPS57123168A Substituted phenylsulfonylurea derivative, its preparation and herbicide containing the same as active constituent 失效
标题翻译：取代的苯乙烯衍生物，其制备和除草剂含有活性成分
公开(公告)号：JPS57123168A
公开(公告)日：1982-07-31
申请号：JP897781
申请日：1981-01-26
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , SAITOU JIYUNICHI , YASUI HITOSHI , SHIOKAWA KOUZOU , MORISHIMA NORIHISA , GOSHIMA TOSHIO
IPC分类号： C07D251/16 , A01N20060101 , A01N47/28 , A01N47/36 , A01N57/00 , C07D20060101 , C07D239/24 , C07D239/42 , C07D239/47 , C07D251/12 , C07D251/46
摘要： NEW MATERIAL:A substituted phenylsulfonylurea derivative expressed by forformulaI[X is phenyl or phenoxy; R is formula II (R
1 and R
2 are methyl or methoxyl) or formula III].
EXAMPLE: N-2-Biphenylylsulfonyl-N'-(4-methoxy-6-methyl-pyrimidin-2-yl)urea. expressed by formula IV.
USE: A herbicide capable of exhibiting an accurate and selective herbicedal effect in a small amount of a chemical without giving the phytotoxicity, particularly exhibiting a remarkable controlling effect in use as a soil treating agent or foliar and soil treating agent in weeds in paddy fields, and having improved safety and a wide herbicidal spectrum.
PROCESS: A compound expressed by formula V is reacted with a compound expressed by the formula NH
2 -R to give the aimed compound expressed by formulaI.
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：新材料：由下式表示的取代苯基磺酰脲衍生物[X是苯基或苯氧基; R是式II（R 1和R 2是甲基或甲氧基）或式III]。实施例：N-2-联苯基磺酰基-N' - （4-甲氧基-6-甲基 - 嘧啶-2-基）由公式四表示。用途：能够在不产生植物毒性的情况下，在少量化学物质中显示精确和选择性除草效果的除草剂，特别是在稻田杂草中用作土壤处理剂或叶面和土壤处理剂时具有显着的控制作用，并具有改善的安全性和广泛的除草频谱。方法：将由式V表示的化合物与由式NH 2 -R表示的化合物反应，得到由式I表示的目标化合物。

7. 发明专利

JPS58188807A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58188807A
公开(公告)日：1983-11-04
申请号：JP7034882
申请日：1982-04-28
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N57/30
摘要： PURPOSE: A herbucide, containing a substituted phenylfulfonylurea derivative and O-methyl O-(2-p-toly) N-iso-propylphosphoramidothionate, etc., and capable of exhibiting very remarkable potentiating and synergistic action.
CONSTITUTION: A herbicide containing a substituted phenylsulfonylurea derivative expressed by formula I [X is O or direct bond; Y is H or Cl; R is formula II(R
1 and R
2 are methyl or methoxyl) or formula III] and O-methyl-(2-nitro-p- tolyl) N-iso-propylphosphoramidothionate expressed by formula IV or O-ethyl O-(6-nitro-m-tolyl) N-sec-butyl phosphoramidothionate expressed by formula V. The resultant mixed herbicide has improved safety, exhibits a remarkable herbicidal activity, a wide herbicidal spectrum and improved lasting efficacy, and is suitable particularly to a pre-emergence soil treating agent and foliar and soil treating agent for weeds in paddy fields.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：一种草甘膦，含有取代苯基呋喃基脲衍生物和O-甲基O-（2-对甲苯甲酰）N-异丙基磷酰胺硫代磷酸酯等，能显示非常显着的增效和协同作用。构成：含有式I表示的取代苯基磺酰脲衍生物的除草剂[X为O或直接键; Y是H或Cl; R是式II（R 1和R 2是甲基或甲氧基）或式III]和由式IV表示的O-甲基 - （2-硝基 - 对甲苯基）N-异丙基磷酰胺硫代磷酸酯或O-乙基由式V表示的O-（6-硝基间甲苯基）N-仲丁基氨基硫代磷酸酯。所得混合除草剂具有改善的安全性，显示出显着的除草活性，广泛的除草谱和改善的持久功效，并且特别适用于一种出苗前的土壤处理剂和稻田杂草的叶面和土壤处理剂。

8. 发明专利

JPS58185507A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58185507A
公开(公告)日：1983-10-29
申请号：JP6806482
申请日：1982-04-24
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N37/22 , A01N47/36
摘要： PURPOSE: To obtain a herbicide exhibiting excellent synergistic effect for the control of weeds at a low rate of application compared with the separate use of each component and having excellent long activity and safety, by using an active component composed of a mixture of a novel substituted phenylsulfonylurea derivative and butachlor.
CONSTITUTION: The objective herbicide is prepared by using an active component obtained by mixing (A) a novel substituted phenylsulfonylurea derivative of formula I [X is O or single bond; Y is H or Cl; R is group of formula II (R
1 and R
2 are CH
3 or OCH
3 ) or formula III] having excellent selective herbicidal activity with (B) butachlor [=2-chloro-2',6'-diethyl-N-(butoxymethyl)acetanilide] which is a known herbicide, at a weight ratio of 1:10W2:2, preferably 1:5W1:1. The mixture has low toxicity and no phytotoxicity to crops, and can be used as a pregermination soil-treating agent or foliar and soil-treating agent for the control of the weeds in paddy field.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：通过使用由新型取代基的混合物组成的活性成分，获得与单独使用每种成分相比，以低的施用率显示优异的协同效果的除草剂，具有优异的长活性和安全性苯磺酰脲衍生物和丁草胺。构成：通过使用通过混合（A）新的式I的取代的苯基磺酰基脲衍生物[X是O或单键而得到的活性成分， Y是H或Cl; R是具有优异选择性除草活性的式（II）（R 1和R 2是CH 3或OCH 3）或式III]的基团，其中（B）丁草胺[= 2-氯-2'，6'-二乙基-N - （丁氧基甲基）乙酰苯胺]，它是已知的除草剂，重量比为1:10-2:2，优选为1：5-1：1。该混合物对作物毒性低，无植物毒性，可用作预处理土壤处理剂或叶面和土壤处理剂，用于控制稻田杂草。

9. 发明专利

JPS58185505A Herbicide 失效
标题翻译：除草剂
公开(公告)号：JPS58185505A
公开(公告)日：1983-10-29
申请号：JP6806282
申请日：1982-04-24
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , YASUI KAZUTOMI , KAJI SHIYUUZOU
IPC分类号： A01N47/34 , A01N37/22 , A01N47/36
摘要： PURPOSE: To prepare a herbicide capable of controlling all kind of weeds completely, safely, without causing phytotoxicity, with single application, by using a substituted phenylsulfonylurea derivative and 2-chloro-2',6'-diethyl-N-(2-propoxyethyl)acetanilide a active components.
CONSTITUTION: The objective herbicide contains a substituted phenylsulfonylurea derivative of formula I [X is O or single bond; Y is H or Cl; R is group of formula II (R
1 and R
2 are methyl or methoxy) or formula III] [e.g. N-2-biphenylylsulfonyl-N'-(4-methoxy-6-methylpyrimidin-2-yl)-urea, etc.] and 2-chloro-2',6- diethyl-N-(2-propoxyethyl)acetanilide of formula IV as active components. The herbicide exhibits remarkable synergistic effect. Especially, it exhibits remarkable selective controlling activity and excellent durability of the effect when used as a pregermination soil-treating agent for the weeds in paddy field or a foliar and soil-treating agent.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：通过使用取代的苯基磺酰脲衍生物和2-氯-2'，6'-二乙基-N-（2-丙氧基乙基）丙烯酸酯来制备能够完全，安全地控制所有种类杂草的除草剂，而不引起植物毒性）乙酰苯胺是一种活性成分。构成：目标除草剂含有式I的取代的苯基磺酰基脲衍生物[X是O或单键; Y是H或Cl; R是式II的基团（R 1和R 2是甲基或甲氧基）或式III] [例如， N-2-联苯基磺酰基-N' - （4-甲氧基-6-甲基嘧啶-2-基） - 脲等]和2-氯-2'，6-二乙基-N-（2-丙氧基乙基）乙酰苯胺 IV作为活性成分。除草剂显示出显着的协同效应。特别地，当用作稻田杂草的预发芽土壤处理剂或叶面和土壤处理剂时，其具有显着的选择性控制活性和优异的耐久性。

10. 发明专利

JPS59172440A Substituted phenoxypropionic ester, its intermediate, its preparation, and herbicide 失效
标题翻译：取代的苯氧基酯，其中间体，其制备和除草剂
公开(公告)号：JPS59172440A
公开(公告)日：1984-09-29
申请号：JP4702783
申请日：1983-03-23
申请人： Nippon Tokushu Noyaku Seizo Kk
发明人： AYA MASAHIRO , SAITOU JIYUNICHI , YASUI KAZUTOMI , SHIOKAWA KOUZOU , KAJI SHIYUUZOU
IPC分类号： A01N37/12 , A01N39/02 , A01N43/40 , C07C219/06 , C07D213/64 , C07D213/643
CPC分类号： C07D213/643 , A01N39/02 , A01N43/40
摘要： NEW MATERIAL:A compound shown by the formula I [Ar is group shown by the formula II (Y is halogen, or trifluoromethyl; b is 1 or 2), or group shown by the formula III; R
1 and R
3 are H, or methyl; R
2 is lower alkyl, or lower alkenyl; X is H, halogen, or lower alkoxy; a and m are 1 or 2].
EXAMPLE: 2-[4-(3,5-Dichloro-2-pyridyloxy)phenoxy]propionic acid 2-(N-methylbenzylamino)ethyl.
USE: A herbicide. Showing improved herbicidal effect especially on gramineous weeds, having low toxicity.
PREPARATION: A compound shown by the formula IV (M is H, or alkali metal) is reacted with a compound shown by the formula V (Z' is halogen) at -20°CW the boiling temperature of the mixture, preferably at 0W100°C to give a compound shown by the formula I .
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：由式I表示的化合物[Ar为式II所示的基团（Y为卤素，或三氟甲基; b为1或2）或式III所示的基团; R 1和R 3是H或甲基; R 2是低级烷基或低级烯基; X是H，卤素或低级烷氧基; a和m为1或2]。实施例：2- [4-（3,5-二氯-2-吡啶基氧基）苯氧基]丙酸2-（N-甲基苄基氨基）乙基。用途：除草剂。显示出特别是对禾本科杂草的除草效果，毒性低。制备：将式IV化合物（M为H或碱金属）与式V所示的化合物（Z'为卤素）在-20℃ - 混合物的沸点温度下反应，优选在 0-100℃，得到式I所示的化合物。

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