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1. 发明专利

JP2014064980A Low-energy electromagnetic wave reaction apparatus 有权
标题翻译：低能电磁波反应装置
公开(公告)号：JP2014064980A
公开(公告)日：2014-04-17
申请号：JP2012210875
申请日：2012-09-25
申请人： Nippon Kagaku Kikai Seizo Kk , 日本化学機械製造株式会社 , Kyoto Univ , 国立大学法人京都大学
发明人： CHIKADA TSUKASA , NOZAKI YOSHIHIRO , MITANI TOMOHIKO , HASEGAWA NAOKI , SHINOHARA MASATAKE , WATANABE TAKASHI
IPC分类号： B01J19/12 , H05B6/80
摘要： PROBLEM TO BE SOLVED: To provide a low-energy electromagnetic wave reaction apparatus which is able to irradiate reaction raw material efficiently with low-energy electromagnetic waves of a broad frequency band.SOLUTION: A low-energy electromagnetic wave reaction apparatus comprises a low-energy electromagnetic wave oscillation unit 2 of low-energy electromagnetic wave variable frequency type which outputs low-energy electromagnetic waves of a frequency of the whole or a partial frequency band of 0.03 to 300 GHz band, a low-energy electromagnetic wave transmission unit 3 which transmits the low-energy electromagnetic waves outputted from the low-energy electromagnetic wave oscillation unit 2, and a low-energy electromagnetic wave irradiation unit 4 which includes a reaction raw material filling space 12 to be filled with reaction raw material, and irradiates the reaction raw material in the reaction raw material filling space 12 with the low-energy electromagnetic waves from the low-energy electromagnetic wave transmission unit 3.
摘要翻译：要解决的问题：提供一种能够以较宽频带的低能电磁波有效照射反应原料的低能电磁波反应装置。解决方案：一种低能电磁波反应装置，低能量电磁波可变频率型能量电磁波振荡单元2，其输出全频率或0.03-300GHz频带的部分频带的低能电磁波，低能电磁波传输单元3，发送从低能量电磁波振荡单元2输出的低能量电磁波，以及低能量电磁波照射单元4，其包括反应原料填充空间12，填充反应原料，并照射反应反应原料填充空间12中的原料与低能电磁波一起从低温 ergy电磁波传输单元3。

2. 发明专利

JP2013206537A Microwave irradiation device 审中-公开
标题翻译：微波辐射器件
公开(公告)号：JP2013206537A
公开(公告)日：2013-10-07
申请号：JP2012070740
申请日：2012-03-27
申请人： Nippon Kagaku Kikai Seizo Kk , 日本化学機械製造株式会社
发明人： NOZAKI YOSHIHIRO , CHIKADA TSUKASA , TAKAMI YASUHIRO
IPC分类号： H05B6/72 , B01J19/12 , H05B6/80
摘要： PROBLEM TO BE SOLVED: To provide a microwave irradiation device which can irradiate a microwave with high efficiency by minimizing the energy loss and whose maintainability is excellent.SOLUTION: A microwave receiving part 6 which transmits a microwave guided through a waveguide 5 and introduces it into a container through the opening of the container comprises: a mounting seat 7 having a circular hole; a first connection member 8 which is mounted on the tube end of the waveguide 5 and has a microwave guiding passage (rectangular inner peripheral surface 8e) having a rectangular section whose inner size is almost the same as that of the waveguide 5; a second connection member 9 having an inside diameter to which the microwave guiding passage of the first connection member 8 is fitted; and a dielectric member 10 which is held between the mounting seat 7 and the second connection member 9.
摘要翻译：要解决的问题：提供一种能够通过最小化能量损失并且其可维护性优异地以高效率照射微波的微波照射装置。解决方案：微波接收部分6，其传输通过波导5引导的微波并将其引入通过容器的开口的容器包括：具有圆形孔的安装座7; 第一连接部件8，安装在波导管5的管端，并具有微波引导通路（矩形内周面8e），该微波引导通路（矩形内周面8e）的内径与波导5的内径几乎相同。具有内径的第二连接构件9，第一连接构件8的微波引导通道安装在该内径上; 以及保持在安装座7和第二连接构件9之间的电介质构件10。

3. 发明专利

JP2012120976A Multilayer pressure-resistant structure type reactor using microwave as heating source 审中-公开
标题翻译：使用微波作为加热源的多层耐压结构型反应器
公开(公告)号：JP2012120976A
公开(公告)日：2012-06-28
申请号：JP2010273525
申请日：2010-12-08
申请人： Nippon Kagaku Kikai Seizo Kk , 日本化学機械製造株式会社
发明人： CHIKADA TSUKASA , KAJIWARA SUSUMU
IPC分类号： B01J19/24 , B01J3/00 , B01J3/04
摘要： PROBLEM TO BE SOLVED: To provide a device for safely executing high pressure liquid phase continuous reaction using a microwave capable of accelerating chemical reaction a heating source.SOLUTION: The multilayer pressure-resistant structure type reactor is constituted by attaching a pressure-resistance shell capable of safely collecting and recovering a high temperature and high pressure reaction material to the outer periphery of the reaction tube when the reaction material is projected by the pressure-resistant reaction tube being broken constituted of a microwave transmitting material such as glass, a plastic, and a ceramic due to an unexpected event during reaction. In this case, it is possible to form the shell with one layer but the safety is further enhanced by forming the shell with two layers of an inner shell and an outer shell. In the case of two layer shell, a pressure inside of the inner shell can be held and controlled in the same level as the pressure in the reaction tube. Thereby, in this case it is possible to suppress the generation of the unexpected event such as the breakage of the reaction tube.
摘要翻译：要解决的问题：提供一种使用能够加速化学反应的加热源的微波安全执行高压液相连续反应的装置。解决方案：多层耐压结构型反应器通过在反应材料投射时将能够安全地收集和回收高温高压反应材料的耐压外壳连接到反应管的外周而构成由于反应期间出现意外事件而由玻璃，塑料和陶瓷等微波传输材料构成的耐压反应管被破坏。在这种情况下，可以形成具有一层的壳，但是通过用两层内壳和外壳形成外壳进一步增强了安全性。在两层壳的情况下，内壳内部的压力可以保持并控制在与反应管中的压力相同的水平。因此，在这种情况下，可以抑制诸如反应管的断裂的意外事件的产生。版权所有（C）2012，JPO＆INPIT

4. 发明专利

JP2013163618A Liquid phase high speed synthesis method for olivine type compound or carbon composite thereof 审中-公开
标题翻译：液体类型化合物或其复合物的液相高速合成方法
公开(公告)号：JP2013163618A
公开(公告)日：2013-08-22
申请号：JP2012027989
申请日：2012-02-13
申请人： Nippon Kagaku Kikai Seizo Kk , 日本化学機械製造株式会社
发明人： CHIKADA TSUKASA , NOZAKI YOSHIHIRO , KATSURA YOKO , KAJIWARA SUSUMU
IPC分类号： C01B25/45 , H01M4/36 , H01M4/58
CPC分类号： Y02E60/12
摘要： PROBLEM TO BE SOLVED: To provide a method for speedily and efficiently manufacturing an olivine type compound or a carbon composite thereof for a positive electrode material of a lithium ion secondary battery.SOLUTION: A liquid raw material synthesized by adding a Li source raw material, a P source raw material, and a metal M (here, M is Co, Fe, or Mn) source raw material to a solvent such as water, and a liquid raw material prepared by mixing is reacted under conditions of microwave irradiation, a temperature of 180°C or less, and a period of 1 h or less to synthesize an olivine type compound of LiMPOat a low temperature in a short period of time. On the other hand, if a similar reaction is carried out by previously adding and uniformly dispersing inorganic particulate carbon powder in the liquid raw material for the olivine type compound, as a temperature near the carbon powder easily absorbing microwaves rises rapidly, and as, here the synthesis reaction of the olivine type compound will selectively occur, a homogeneous LiMPO/C composite is easily manufactured as a result.
摘要翻译：要解决的问题：要迅速和高效地制造的橄榄石型化合物或碳纤维复合材料，其用于锂离子二次battery.SOLUTION的正极材料的方法：通过添加Li源原料合成的液体原料， P源原料和金属M（这里，M为Co，Fe或Mn）的源原料的溶剂如水，和通过混合在微波辐射，温度的条件下反应而制备的液体原料 180℃以下，时间为1小时以下，在短时间内合成低温的LiMPO的橄榄石型化合物。在另一方面，如果一个类似反应通过预先加入并均匀地在液体原料为橄榄石型化合物的无机颗粒碳粉末分散，作为碳粉末容易吸收微波附近的温度下进行快速升高，并且如在这里将选择性地发生橄榄石型化合物的合成反应，因此容易制造均匀的LiMPO / C复合材料。

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