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1. 发明专利

JP2002301301A METHOD FOR REGENERATING WASTE SOLVENT 失效
公开(公告)号：JP2002301301A
公开(公告)日：2002-10-15
申请号：JP2001104653
申请日：2001-04-03
申请人： NIPPON REFINE KK
发明人： KAWASE YASUHITO , SAKAMOTO MITSUYOSHI , ODA AKIMASA
IPC分类号： B01D3/00 , B01D3/34
摘要： PROBLEM TO BE SOLVED: To provide a new method for regenerating a waste solvent to solve problems of regenerated solvents by unknown cause. SOLUTION: The method for regenerating a waste solvent includes the following processes. (1) The waste solvent is inspected whether it is originally neutral or not. (2) If the solvent is originally neutral, (i) a neutralizer is added to neutralize the solvent and then the solvent is refined by distillation and recovered, or (ii) while a neutralizer is intermittently or continuously added during distillation to carry out neutralization, the solvent is recovered. (3) If the solvent is not originally neutral, (a) the waste solvent is analyzed to determine the quantity of impurities consisting of an acid component or an alkali component and (b) (i) a neutralizer in an amount corresponding to the above quantity is added and the solvent is refined by distillation and recovered or (ii) while an alkali component or an acid component in an amount corresponding to the above quantity is intermittently or continuously added to carry out the neutralization during distillation, the solvent is recovered.

2. 发明专利

JP2000107748A DRAINAGE TREATMENT METHOD 失效
公开(公告)号：JP2000107748A
公开(公告)日：2000-04-18
申请号：JP29608598
申请日：1998-10-02
申请人： NIPPON REFINE KK
发明人： RYU HOSHI , ODA AKIMASA , OGAWA TOSHIHIRO , KAWASE YASUHITO
IPC分类号： C02F1/04 , B01D3/36 , B01D3/40 , C07C7/06 , C07C29/82 , C07C39/04
摘要： PROBLEM TO BE SOLVED: To treat drainage containing phenol stably and to recover high quality phenol by the azeotropic distillation of the drainage in the presence of an azeotropic agent. SOLUTION: Before the operation of a sieve tray distillation column 200 mm in diameter and 25 in number of stages, 15 kg of p-xylene (azeotropic agent) is charged into a decanter. The flow rate of an azeotropic agent layer from the decanter to the column is controlled so that the temperature of fifth stage from the top is 93 deg.C, the column is operated continuously for 13 hr at 20 kg/hr raw material feed late to make the concentration of phenol in drainage under 2500 ppm. the purity of phenol recovered from the bottom of the column is made to be at least 99 wt.%, and the phenol is separated/recovered. In this way, stable treated drainage and high quality phenol can be obtained.

3. 发明专利

JPH09257369A LONGITUDINAL DOUBLED DRUM DRIER 失效
公开(公告)号：JPH09257369A
公开(公告)日：1997-10-03
申请号：JP9482096
申请日：1996-03-25
申请人： NIPPON REFINE KK
发明人： KAWASE YASUHITO
IPC分类号： F26B9/04 , B01D1/22 , B01D5/00 , F26B25/20
摘要： PROBLEM TO BE SOLVED: To improve heat efficiency and hereby obviate the need of concentration means in a previous process by surrounding an internal chamber with a group of heating drums formed by orienting a specific number of heating drums vertically and bringing them into pressure contact at their rotation surfaces, providing an outside container for accommodating the group of the heating drums, and oppositely rotating adjacent ones among the heating drums. SOLUTION: An internal chamber is surrounded by a group of heating drums formed by orienting heating drums 1 comprising an even number of 4 or more vertically and bringing them into pressure contact at their rotation surfaces, and an outside container 4 is provided for accommodating the heating drum group. A scraper blade 2 is provided for scraping a dried material adhering to the heating drum 1, and a dried material recovery region 3 is provided in which a dried material is dried and to which the dried material is scraped and collected. The adjacent heating drums 1 are oppositely rotated with time aid of a motor 6, a V belt, a chane 7, and rotary shafts 8 of the heating drums 1. Hereby, heat efficiency is sharply improved, and there is eliminated the need of concentration means in a previous process even though the material to be dried is a thin solution.

4. 发明专利

JPH0886682A TREATMENT SYSTEM 失效
公开(公告)号：JPH0886682A
公开(公告)日：1996-04-02
申请号：JP24991894
申请日：1994-09-19
申请人： NIPPON REFINE KK
发明人： KAWASE YASUHITO
IPC分类号： G01F23/00 , B01D1/30
摘要： PURPOSE: To obtain a treatment system in which a treating liquid has no adverse effect on the control of liquid level which can thereby be kept within a correct range constantly. CONSTITUTION: The treatment system comprises a treatment tank 6, a stock solution storage tank 2 having a height and volume sufficient for sustaining an appropriate treating liquid level 10 in the treatment tank 6, and a pipe 3 for communicating the treatment tank 6 and the stock solution storage tank 2. The pipe 3 is coupled with the treatment tank 6 on the side wall thereof at a part lower than the appropriate treating liquid level in the tank 6 and coupled with the stock solution storage tank 2 at a part lower than the appropriate treating liquid level in the tank 6.

5. 发明专利

JP2010172842A Gas-liquid reaction method and apparatus using microbubble 有权
标题翻译：气体反应方法和使用微生物的装置
公开(公告)号：JP2010172842A
公开(公告)日：2010-08-12
申请号：JP2009019366
申请日：2009-01-30
申请人： Nippon Refine Kk , 日本リファイン株式会社
发明人： BANDO YOSHIYUKI , KAWASE YASUHITO , YASUDA KEIJI , TAKEYAMA TOMOKIYO
IPC分类号： C02F1/78 , B01F1/00 , B01F3/04 , B01F5/10
摘要： PROBLEM TO BE SOLVED: To provide a gas-liquid reaction method and apparatus which can improve ozone use efficiency from a standpoint of equipment engineering paying attention to a flow behavior of ozone microbubbles in an air-lift type gas-liquid reaction apparatus by installing a particular draft tube or partition plate in the apparatus. SOLUTION: In the gas-liquid reaction method and apparatus, a microbubble generator is incorporated in an air-lift bubble column, a ratio of the cross section of a downflow portion to the column is controlled by a diameter of the draft tube and a position of the partition plate to control the flow behavior of the microbubbles in the column. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：解决的问题：提供一种气液反应方法和装置，其可以从设备工程的观点来提高臭氧利用效率，注意空气提升式气液反应装置中臭氧微泡的流动行为通过在设备中安装特定的引流管或分隔板。解决方案：在气液反应方法和装置中，将微泡发生器结合到气泡泡罩塔中，下流部分与塔的横截面的比例由引流管的直径以及分隔板的位置，以控制柱中微泡的流动行为。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2009109559A Method and apparatus for regenerating releasing liquid from releasing liquid waste water 有权
标题翻译：释放液体废水中再生液体的方法与装置
公开(公告)号：JP2009109559A
公开(公告)日：2009-05-21
申请号：JP2007278988
申请日：2007-10-26
申请人： Nippon Refine Kk , 日本リファイン株式会社
发明人： TAKEYAMA TOMOKIYO , KONO MASAFUMI , ODA AKIMASA , MIZUTANI EIICHI , KAWASE YASUHITO
IPC分类号： G03F7/42 , B01D1/22 , B01D3/00 , G02F1/13
摘要： PROBLEM TO BE SOLVED: To provide a method and an apparatus for regenerating a new releasing liquid, decreasing replenishment of an expensive releasing liquid having purity available to electronic industry, and regenerating refined releasing liquid from the releasing liquid waste water at a higher recovery percentage than before.
SOLUTION: In the method for separating and removing resist from the releasing liquid waste water containing resist which is discharged from a manufacturing process for a liquid crystal display panel to regenerate a releasing liquid, this method and apparatus for regenerating the releasing liquid is characterized in that alkaline of weight 0.01-0.2 times as large as the resist weight is added to the resist in the releasing liquid waste water.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供一种再生新型释放液体的方法和装置，减少了对电子工业具有可用纯度的昂贵的释放液体的补充，并且从较高的释放液体废水再生精制液恢复百分比。解决方案：在从用于液晶显示面板的制造工序排出的释放液体废水含有抗蚀剂中分离除去抗蚀剂以再生释放液体的方法中，用于再生释放液体的方法和装置是其特征在于，在释放液体废水中的抗蚀剂中加入重量为抗蚀剂重量的0.01-0.2倍的碱。版权所有（C）2009，JPO＆INPIT

7. 发明专利

JP2008114203A Method and apparatus for recovering and enriching voc from voc-containing exhaust gas and cleaning exhaust gas 有权
标题翻译：从含VOC的排气和清洁排气中回收和增加VOC的方法和装置
公开(公告)号：JP2008114203A
公开(公告)日：2008-05-22
申请号：JP2006302400
申请日：2006-11-08
申请人： Nippon Refine Kk , 日本リファイン株式会社
发明人： KAWASE YASUHITO , ODA AKIMASA , TAKEYAMA TOMOKIYO , IKEDA TSUYOSHI , MIZUTANI EIICHI
IPC分类号： B01D53/44 , B01D53/14 , B01D53/77
CPC分类号： Y02A50/235
摘要： PROBLEM TO BE SOLVED: To provide a method and an apparatus for cleaning exhaust gas containing volatile organic compounds [VOC(VOC having physical properties such as a higher boiling point than that of water, hydrophilicity and easy dissolvability in water, and having no azeotropic point with water)] discharged from a hot air dryer of a chemical plant, and recovering enriched liquid. SOLUTION: By using this VOC recovering and enriching apparatus which is composed of a VOC enriching section having one block of vapor-liquid contact mechanism and a recovering section in the gas downstream side of the enriching section, water serving as an absorbent supplied from the gas downstream side of the recovering section is made to flow down through the enriching section while absorbing VOC contained in exhaust gas in the recovering section, VOC-containing exhaust gas is introduced from the gas upstream side of the enriching section, and water, the absorbent, is vaporized in the enriching section to discharge cleaned gas to the system outside through the recovering section. The VOC enriched liquid enriched in the enriching section is sent to a storage part provided at the lower end of the apparatus. Stored VOC liquid is circulated to the gas downstream side of the enriching section, VOC is enriched by vaporization of water in the circulation liquid, and the enriched circulation liquid is discharged to the system outside, when reaching a given concentration. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种清洁含有挥发性有机化合物的废气的方法和装置[VOC（VOC（VOC）具有比水的沸点高的物理性质，亲水性和易溶于水的溶剂，并具有与水的共沸点）]从化工厂的热空气干燥器排出，并回收富集液体。解决方案：通过使用该VOC回收和富集装置，其由具有一个气 - 液接触机构块的VOC富集部分和在富集部分的气体下游侧的回收部分组成，用作吸收剂的水从回收部的气体下游侧，在吸收回收部中的废气中含有VOC的同时，向富集部流下，从富集部的气体上游侧引入含有VOC的排气，吸收剂在富集部分中蒸发，以通过回收部分将清洁的气体排出到外部的系统。富集富集部分的富含VOC的液体被送到设置在下端的储存部分。储存的VOC液体循环到富集部分的气体下游侧，VOC通过循环液体中的水的蒸发而富集，并且当达到给定浓度时，富集的循环液体被排出到系统外部。版权所有（C）2008，JPO＆INPIT

8. 发明专利

JP2006111487A Method for recovering hydrofluoric acid 有权
标题翻译：回收氢氟酸的方法
公开(公告)号：JP2006111487A
公开(公告)日：2006-04-27
申请号：JP2004300350
申请日：2004-10-14
申请人： Mitsubishi Chemical Engineering Corp , Nippon Refine Kk , Ryoka Forward Kk , 三菱化学エンジニアリング株式会社 , 日本リファイン株式会社 , 菱化フォワード株式会社
发明人： MIYATA KENYO , KAMEYAMA KAORU , KAWASE YASUHITO
IPC分类号： C01B7/19 , B01D1/00 , B01D3/14 , C02F1/04
摘要： PROBLEM TO BE SOLVED: To provide a method for recovering hydrofluoric acid, which is a batch-type hydrofluoric acid recovery method for recovering purified hydrofluoric acid from a hydrofluoric acid waste solution discharged from the etching process of a glass substrate, or the like by a distillation method, and by which production of scales is completely suppressed and the purified hydrofluoric acid containing further reduced impurities can be recovered in a high yield, and with which it is possible to simplify an apparatus.
SOLUTION: In the method for recovering the hydrofluoric acid, crude hydrofluoric acid is taken out as vapor by heating a hydrofluoric acid waste solution in an evaporation pot (1), and at the same time, in recovery operations for recovering distillates by distilling the crude hydrofluoric acid with a distillation tower (2), the distillate is recovered as recovery water when the concentration of hydrogen fluoride in the distillate is not higher than the upper limit of the concentration of hydrogen fluoride in the recovery water, the distillate is recovered as an intermediate solution when the concentration of hydrogen fluoride in the distillate is not lower than the upper limit of the concentration of hydrogen fluoride in the recovery water and lower than the concentration of hydrogen fluoride in the hydrofluoric acid to be recovered, and the distillate is recovered as the purified hydrofluoric acid when the concentration of hydrogen fluoride in the distillate is not lower than the concentration of hydrogen fluoride in the hydrofluoric acid to be recovered. Further, in the method, sulfuric acid is added to the hydrofluoric acid waste solution of the distillation tower (2) in an amount sufficient to suppress the deposition of metal components.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种回收氢氟酸的方法，该方法是从由玻璃基板的蚀刻工艺排出的氢氟酸废液中回收纯化氢氟酸的间歇式氢氟酸回收方法，或者通过蒸馏法，通过其完全抑制氧化皮的生成，可以高收率地回收含有进一步还原的杂质的纯化氢氟酸，并且可以简化装置。解决方案：在回收氢氟酸的方法中，通过加热蒸发罐（1）中的氢氟酸废液，蒸馏除去粗氢氟酸，同时在回收馏出物的回收操作中用蒸馏塔（2）蒸馏粗制氢氟酸，当馏出物中的氟化氢浓度不高于回收水中氟化氢浓度的上限时，馏出物作为回收水回收，馏出物为当馏出物中的氟化氢浓度不低于回收水中的氟化氢浓度的上限并且低于待回收的氢氟酸中的氟化氢浓度时，作为中间溶液回收，馏出物当馏出物中的氟化氢浓度不低于c时，作为纯化氢氟酸回收在待回收的氢氟酸中氟化氢的浓度。此外，在该方法中，将硫酸以足以抑制金属成分沉积的量添加到蒸馏塔（2）的氢氟酸废液中。版权所有（C）2006，JPO＆NCIPI

9. 发明专利

JP2004230265A Method and apparatus for concentrating substance of higher boiling point than that of water in exhaust gas 有权
标题翻译：浓度较高的沸点高于排气中的水的物质的方法和装置
公开(公告)号：JP2004230265A
公开(公告)日：2004-08-19
申请号：JP2003020725
申请日：2003-01-29
申请人： Nippon Refine Kk , 日本リファイン株式会社
发明人： KAWASE YASUHITO , RI MOTOYOSHI
IPC分类号： B01D53/72 , B01D47/00 , B01D47/14 , B01D53/02 , B01D53/14 , B01D53/77 , B01D53/78
摘要： PROBLEM TO BE SOLVED: To efficiently recover volatile chemical substances of higher boiling points than that of water such as a water-soluble solvent contained in exhaust gas by replacing it with steam and to recover powder of active carbon, or the like, having adsorbed chemical substances such as dioxins from exhaust gas containing the powder of the active carbon, or the like, having adsorbed chemical substances such as dioxins. SOLUTION: The apparatus is constituted so that the exhaust gas containing the substances of higher boiling points than that of water is introduced into a plate column provided with a plurality of stages of trays, having the structure in which gas cannot escape to an upper part without passing through water existing on the trays or into a packed column packed with a hydrophilic filler from a lower part thereof and meanwhile water is fed from an upper part of the column to concentrate the substances of higher boiling points than that of water based on the gas-liquid equilibrium relation between the exhaust gas and water at the lower part of the column and further to shift the residual substances in the exhaust gas into water at the upper part of the column. COPYRIGHT: (C)2004,JPO&NCIPI
摘要翻译：待解决的问题：为了通过用蒸汽替换并回收活性炭等的粉末来有效地回收比废气中所含的水溶性溶剂等水的沸点高的挥发性化学物质，从含有活性炭粉等的废气中吸收二恶英等化学物质，吸附有二恶英等化学物质。解决方案：该装置的结构使得含有比水的沸点高的物质的排气被引入设置有多级塔盘的塔板中，其具有气体不能逸出的结构上部没有通过存在于托盘上的水或从其下部装入填充有亲水填料的填充柱，同时从塔的上部供给水以将沸点高于水基的物质基于排气与柱下部的水之间的气液平衡关系，并进一步将废气中的残留物质转移到塔上部的水中。版权所有（C）2004，JPO＆NCIPI

10. 发明专利

JPH1112390A SEPARATION OF ORGANIC SOLVENT AND RESIN FROM ORGANIC SOLVENT SOLUTION CONTAINING RESIN AND DEVICE THEREFOR 失效
公开(公告)号：JPH1112390A
公开(公告)日：1999-01-19
申请号：JP18581797
申请日：1997-06-26
申请人： NIPPON REFINE KK
发明人： KAWASE YASUHITO , ODA AKIMASA
IPC分类号： B01D5/00 , B29B17/00 , C08J11/02 , C08J11/14
摘要： PROBLEM TO BE SOLVED: To provide a method for recovering from a resin-containing organic solvent solution a resin having a low solvent content comparable with that in a case using a drum drier without using the drum drier, and to provide a device therefor. SOLUTION: This method for recovering an organic solvent and a resin from a resin-containing organic solvent solution comprises mistily spraying the resin-containing organic solvent solution (raw solution) from the upper portion of an evaporator 1 with a rotary atomizer or a pressure nozzle atomizer 2, charging steam from the lower portion 3 of the evaporator 1 to bring the steam into contact with the sprayed solution in the evaporator 1, condensing a gas component recovered from the top of the evaporator in a condenser 4, separating the condensed liquid into water and the organic solvent, recovering the separated organic solvent, taking out the resin and water from the lower portion of the evaporator 1, recovering the resin and recycling the water as a steam source to be supplied from the lower portion of the evaporator 1 through a reboiler 7.

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