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1. 发明专利

JPS61101505A Dehydrohalogenation of halogen-containing polymer 失效
标题翻译：含氢聚合物的脱氢脱氢酶
公开(公告)号：JPS61101505A
公开(公告)日：1986-05-20
申请号：JP22378884
申请日：1984-10-24
申请人： Mitsubishi Petrochem Co Ltd
发明人： KISE HIDEO , UNO YASUMITSU
IPC分类号： C08F8/00 , C08F8/26
摘要： PURPOSE: To obtain a porous substance of a porous polyacetylene structure, by dehydrohalogenating a halogen-containing polymer by immersing a solution of the polymer and a phase transfer catalyst component in an alkali solution.
CONSTITUTION: A halogen-containing polymer (e.g., polyvinyl halide or polyvinylidene halide polymer) and a phase transfer catalyst (e.g., tetrabutylammonium bromide or chloride) are dissolved in an organic solvent comprising a mixture of tetrahydrofuran, dioxane, etc. The concentration of the halogen-containing polymer is generally 1W50wt%, preferably, 3W30wt% and the amount of the phase transfer catalyst compound used is preferably 0.01W0.02g equivalent, based on the hydrogen halide. This polymer solution is immersed in an alkali solution to dehydrohalogenate the polymer.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了获得多孔聚乙炔结构的多孔物质，通过将聚合物和相转移催化剂组分的溶液浸入碱溶液中，使含卤聚合物脱卤化氢。构成：将含卤聚合物（例如，聚卤乙烯或聚偏二氯乙烯聚合物）和相转移催化剂（例如四丁基溴化铵或氯化物）溶解在包含四氢呋喃，二恶烷等的混合物的有机溶剂中。含卤聚合物通常为1-50重量％，优选3-30重量％，相对于所述卤化氢，相转移催化剂化合物的使用量优选为0.01-0.02g当量。将该聚合物溶液浸入碱溶液中以使聚合物脱卤化氢。

2. 发明专利

JPS617337A Bonding of formed article of fluorine-containing polymer 失效
标题翻译：含氟聚合物形成物品的结合
公开(公告)号：JPS617337A
公开(公告)日：1986-01-14
申请号：JP12884984
申请日：1984-06-22
申请人： Mitsubishi Petrochem Co Ltd
发明人： UNO YASUMITSU
IPC分类号： C08J5/12 , C08J7/12
摘要： PURPOSE: To carry out the bonding of a molded article of a fluorine-containing polymer, easily and effectively, by treating the article with an alkaline solution and a phase-transfer catalyst, and using the surface of the dehydrofluorinated layer formed to the surface of the molded article as the bonding face.
CONSTITUTION: A molded article of a fluorine-containing polymer, e.g. film or various molded articles of a homopolymer or copolymer of polyvinyl fluoride, polyvinylidene fluoride, etc. is treated with a mixture of (A) an aqueous solution or methyl alcohol solution etc. of an alkaline substance such as a 5W30wt% solution of NaOH, KOH, organic amine, etc. and (B) 1×10
-4 W1%, preferably 0.01W0.1% phase-transfer catalyst such as a quaternary ammonium salt, quaternary phosphonium salt, etc., at 40W150°C, preferably 80W110°C for ≥10sec, preferably 30secW3hr. The dehydrofluorinated layer formed on the surface is used as the bonding face of the titled process.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过用碱性溶液和相转移催化剂处理制品，并且使用形成在表面上的脱氟化氢层的表面，容易且有效地进行含氟聚合物的模塑制品的粘合模制品作为粘合面。构成：含氟聚合物的成型品，例如聚氟乙烯，聚偏二氟乙烯等的均聚物或共聚物的膜或各种成型体用（A）碱性物质的水溶液或甲醇溶液等的混合物处理，所述碱性物质例如5-30重量％ NaOH，KOH，有机胺等，和（B）在40-150℃下的1X10 -4％，优选0.01-0.1％的相转移催化剂如季铵盐，季鏻盐等优选80-110℃，> 10秒，优选30秒-3小时。表面上形成的脱氟化氢层用作标题工艺的粘合面。

3. 发明专利

JPS60210493A Recording material 失效
标题翻译：记录材料
公开(公告)号：JPS60210493A
公开(公告)日：1985-10-22
申请号：JP6717784
申请日：1984-04-04
申请人： Mitsubishi Petrochem Co Ltd
发明人： ICHIHARA YOSHIJI , UNO YASUMITSU
IPC分类号： B41M5/26 , G06K19/06 , G11B7/24 , G11B7/241 , G11B7/244
CPC分类号： G11B7/241
摘要： PURPOSE:To enable to record information and optically read the recorded information, by applying thermal energy to a recording material to generate a thermal hysteresis. CONSTITUTION:Thermal energy is applied to an amorphous substance having a change of specific heat at a glass transition temperature [DELTACp (J.K .g )] satisfying the relationship of DELTACp>=0.86exp(-Tg/394.3) and a change of specific heat per one mole of an average molecular weight of molecular component units constituting the substance at the glass transition temperature [M'.DELTACp (J.K . mol )] satisfying the relationship of M'.DELTACp>=10.9 to generate a thermal hysteresis. The recording material is once heated to a temperature not lower than the glass transition temperature, followed by slowly or rapidly cooling to obtain a uniform state. After this pretreatment, the positions for recording in the material are irradiated with IR rays, laser light or the like to partially heating the material to a temperature not lower then the glass transition point, followed by rapidly or slowly cooling to impart a thermal hysteresis, whereby parts differing from other parts in density or refractive index are provided, resulting in performing recording.
摘要翻译：目的：通过将热能应用于记录材料以产生热滞后，能够记录信息和光学读取记录的信息。构成：满足DELTACp> = 0.86exp（-Tg / L）的玻璃化转变温度[DELTACp（JK <-1> .g -1）]的比热变化的非晶物质， 394.3），并且在玻璃化转变温度[M'DELTACp（JK <-1> mol -1））下，每1摩尔构成该物质的分子组分单元的平均分子量的比热变化满足关系的M'.DELTACp> = 10.9以产生热滞后。将记录材料一次加热至不低于玻璃化转变温度的温度，然后缓慢或快速冷却以获得均匀的状态。在该预处理之后，用红外线，激光等照射材料中记录的位置，以将材料部分加热到不低于玻璃化转变点的温度，然后快速或缓慢冷却以赋予热滞后，由此提供与密度或折射率的其它部分不同的部分，从而进行记录。

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