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1. 发明专利

JP2014074106A Method for producing polycarbonate resin, polycarbonate resin pellet and stretched film 审中-公开
标题翻译：生产聚碳酸酯树脂，聚碳酸酯树脂薄膜和拉伸薄膜的方法
公开(公告)号：JP2014074106A
公开(公告)日：2014-04-24
申请号：JP2012221435
申请日：2012-10-03
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： NAMIKI SHINGO , YAMAMOTO MASANORI
IPC分类号： C08G64/30
摘要： PROBLEM TO BE SOLVED: To provide a polycarbonate resin which is excellent in hue, transparency, heat resistance, weatherability and mechanical strength and has less residual low-molecular weight components.SOLUTION: There is provided a method for producing a polycarbonate by continuously polycondensing a dihydroxy compound having a fluorene structure and a carbonic acid diester using a plurality of reactors. The reactors are connected at least in series, at least one polymerization reactor is a horizontal agitation type reactor having a horizontal rotating shaft in its inside. The polycarbonate resin is filtered with a filter having a filter medium composed of a metal non-woven fabric to obtain a polycarbonate resin having a reduced viscosity of 0.36 to 0.60 dL/g.
摘要翻译：要解决的问题：提供一种色调，透明性，耐热性，耐候性和机械强度优异的聚碳酸酯树脂，并且具有较少的残余低分子量组分。解决方案：提供一种通过连续缩聚具有芴结构的二羟基化合物和使用多个反应器的碳酸二酯。反应器至少串联连接，至少一个聚合反应器是在其内部具有水平旋转轴的卧式搅拌式反应器。用具有由金属无纺布构成的过滤介质的过滤器过滤聚碳酸酯树脂，得到比浓粘度为0.36〜0.60dL / g的聚碳酸酯树脂。

2. 发明专利

JP2013209563A Method for producing polycarbonate resin 有权
标题翻译：生产聚碳酸酯树脂的方法
公开(公告)号：JP2013209563A
公开(公告)日：2013-10-10
申请号：JP2012081820
申请日：2012-03-30
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： NAMIKI SHINGO , YAMAMOTO MASANORI
IPC分类号： C08G64/30
摘要： PROBLEM TO BE SOLVED: To provide a preparation method of a polycarbonate resin raw material for stably producing a polycarbonate resin excellent in transparency, hue, heat resistance, moldability and mechanical strength, and having excellent optical characteristics.SOLUTION: There is provided a production method of a polycarbonate resin using a dihydroxy compound and diester carbonate as raw material monomers and polycondensing the monomers by ester exchange reaction in the presence of an ester exchange catalyst, where the dihydroxy compound at least contains an aliphatic dihydroxy compound having an ethereal oxygen atom at least at one β-position or γ-position of the hydroxy group, and the aliphatic dihydroxy compound contains alkanolamine, the method comprising a step of heating the aliphatic dihydroxy compound to 50°C or higher in advance, and mixing with diester carbonate in a molten state.
摘要翻译：要解决的问题：提供用于稳定生产透明性，色调，耐热性，成型性和机械强度优异的聚碳酸酯树脂的聚碳酸酯树脂原料的制备方法，并且具有优异的光学特性。解决方案：提供了一种生产方法使用二羟基化合物和二酯碳酸酯作为原料单体的聚碳酸酯树脂，并且在酯交换催化剂存在下，通过酯交换反应使单体缩聚，其中二羟基化合物至少含有具有醚性氧原子的脂族二羟基化合物至少在羟基的一个或多个位置或γ-位，并且脂族二羟基化合物含有链烷醇胺，该方法包括预先将脂肪族二羟基化合物加热至50℃以上并与碳酸二酯混合的步骤熔融状态。

3. 发明专利

JP2013203861A Method for producing polycarbonate resin composition 有权
标题翻译：生产聚碳酸酯树脂组合物的方法
公开(公告)号：JP2013203861A
公开(公告)日：2013-10-07
申请号：JP2012073830
申请日：2012-03-28
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： HYODO NARUTOSHI , NISHIHARA RYOHEI , YAMAMOTO MASANORI , KUMAZAWA KATSUHISA , SHIBATA HIROKI
IPC分类号： C08J3/20 , B29B7/38 , B29B7/60 , B29B7/88 , B29K69/00 , C08L69/00
CPC分类号： B29C47/369 , B29C47/6037 , B29C47/6087 , Y02P70/263
摘要： PROBLEM TO BE SOLVED: To retain quality of an obtained polycarbonate resin composition by suppressing worsening of a color tone in a kneading extrusion apparatus and a deviation in the quality of a product.SOLUTION: When supplying a melted polycarbonate resin, an additive, etc., to a kneading extrusion apparatus and kneading them, specific energy is set to be 0.03 kWh/kg or more and 0.08 kWh/kg or less, and L/D of the kneading extrusion apparatus is set to be 30 or less.
摘要翻译：要解决的问题：通过抑制捏合挤出装置中色调的恶化和产品质量的偏差来保持所得聚碳酸酯树脂组合物的质量。溶解：当提供熔融的聚碳酸酯树脂，添加剂等时在混炼挤出装置中进行混炼，比能量设定为0.03kWh / kg以上且0.08kWh / kg以下，捏合挤出装置的L / D设定为30以下。

4. 发明专利

JP2012214770A Method for manufacturing polycarbonate resin 有权
标题翻译：制备聚碳酸酯树脂的方法
公开(公告)号：JP2012214770A
公开(公告)日：2012-11-08
申请号：JP2012076278
申请日：2012-03-29
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： YOKOKI MASASHI , NAMIKI SHINGO , NAGAO KOICHI , YAMAMOTO MASANORI
IPC分类号： C08G64/40 , B29B7/38 , B29B9/06 , B29C47/36 , B29C47/64 , B29C47/66 , B29C47/68 , B29C47/92 , B29K69/00 , C08G64/16
CPC分类号： B29C47/364 , B29C47/6056 , B29C47/92 , B29C2947/92704 , B29C2947/92895
摘要： PROBLEM TO BE SOLVED: To efficiently and stably manufacture a polycarbonate resin excellent in optical characteristic, thermostability, hue and mechanical strength with less foreign matter.SOLUTION: In the method for manufacturing a polycarbonate resin by supplying a polycarbonate resin including, as raw material monomers, at least 9,9-bis(4-hydroxyphenyl) fluorene or a cyclic ether additive of the fluorene to an extruder, kneading it to have a high molecular weight, and then discharging the resulting resin from a die, the weight W (kg/h) of the amount of resin extruded by the extruder per hour and the cross-sectional area S (m) of the barrel of the extruder satisfy relation (2): 12,000≤W/S≤60,000.
摘要翻译：要解决的问题：为了有效和稳定地制造具有优异的光学特性，热稳定性，色调和机械强度以及较少异物的聚碳酸酯树脂。解决方案：在通过将包含作为原料单体的至少9,9-双（4-羟基苯基）芴或芴的环醚添加剂的聚碳酸酯树脂供给到挤出机的制造聚碳酸酯树脂的方法中，将其捏合以具有高分子量，然后从模具中排出所得树脂，通过挤出机每小时挤出的树脂量的重量W（kg / h）和横截面积S（m 2 ）满足关系式（2）：12,000≤W/S≤60,000。版权所有（C）2013，JPO＆INPIT

5. 发明专利

JP2012214675A Polycarbonate resin composition and molded article 有权
标题翻译：聚碳酸酯树脂组合物和成型品
公开(公告)号：JP2012214675A
公开(公告)日：2012-11-08
申请号：JP2011197534
申请日：2011-09-09
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： YOKOKI MASASHI , YAMAMOTO MASANORI , FUJI MICHIAKI
IPC分类号： C08L69/00 , C08K5/00
CPC分类号： C08K5/07 , C08G64/0208 , C08G64/183 , C08K5/0041 , C08K5/1345 , C08K5/3435 , C08K5/52 , C08K5/526 , C08L69/00 , Y02P20/582
摘要： PROBLEM TO BE SOLVED: To provide a polycarbonate resin excellent in light resistance, transparency, hue, heat resistance, thermostability and mechanical strength.SOLUTION: The polycarbonate resin composition contains a polycarbonate resin including a structural unit having a site represented by formula (1), which is derived from a dihydroxy compound represented by formula (2) as part of the structure thereof; and a bluing agent, (except when the site expressed in formula (1) is -CH-O-H).
摘要翻译：要解决的问题：提供耐光性，透明性，色相，耐热性，热稳定性和机械强度优异的聚碳酸酯树脂。解决方案：聚碳酸酯树脂组合物含有具有由式（1）表示的位置的结构单元的聚碳酸酯树脂，其衍生自由式（2）表示的二羟基化合物作为其结构的一部分; 和蓝色剂（除了当式（1）表示的位点是-CH 2-O-H时）。版权所有（C）2013，JPO＆INPIT

6. 发明专利

JP2012201817A Method for producing purified pentamethylenediamine, and method for producing polyamide resin 审中-公开
标题翻译：生产纯化的戊烯酰胺的方法和生产聚酰胺树脂的方法
公开(公告)号：JP2012201817A
公开(公告)日：2012-10-22
申请号：JP2011068302
申请日：2011-03-25
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： HITOMI TATSUYA , YAMAMOTO MASANORI , NISHIDA YUICHI , KUSANO KAZUNAO , URASHIMA HIDETOSHI , MIYAOKU KOHEI
IPC分类号： C08G69/28 , C07C209/84 , C07C211/09 , C12N15/09 , C12P13/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing purified pentamethylenediamine, in which the purified pentamethylenediamine is recovered in high yield in a simple production process while preventing trouble in manufacturing such as pipeline clogging in the manufacture of pentamethylenediamine by pyrolysis of pentamethylenediamine carbonate.SOLUTION: The method for producing purified pentamethylenediamine includes a pyrolysis step of heating the aqueous solution of the pentamethylenediamine carbonate to decompose it into crude pentamethylenediamine and carbon dioxide and is characterized in that the pressure at the pyrolysis step is 0.21-1.0 MPa. When the aqueous solution of the pentamethylenediamine carbonate is pyrolyzed to obtain the crude pentamethylenediamine and carbon dioxide, the pyrolysis is performed under specific pressure, so that the risk caused by the trouble in manufacturing such as the pipeline clogging can be reduced and the purified pentamethylenediamine can be obtained in high yield.
摘要翻译：待解决的问题：提供一种纯化的五亚甲基二胺的制备方法，其中在简单的制备方法中以高收率回收纯化的戊二胺，同时防止在制备戊二胺时通过五亚甲基二胺的热解制造中管道堵塞等麻烦碳酸盐。解决方案：纯化的五亚甲基二胺的制备方法包括加热五亚甲基二胺碳酸酯的水溶液以将其分解成粗戊二胺和二氧化碳的热解步骤，其特征在于热解步骤的压力为0.21-1.0MPa。当将五亚甲基二胺碳酸酯的水溶液热解得到粗戊二胺和二氧化碳时，在特定压力下进行热分解，可以降低管道堵塞等制造中的麻烦引起的风险，纯化的五亚甲基二胺可以以高产量获得。版权所有（C）2013，JPO＆INPIT

7. 发明专利

JP2012177093A Polycarbonate resin composition and method for manufacturing the same 审中-公开
标题翻译：聚碳酸酯树脂组合物及其制造方法
公开(公告)号：JP2012177093A
公开(公告)日：2012-09-13
申请号：JP2011256727
申请日：2011-11-24
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： NISHIHARA RYOHEI , HITOMI TATSUYA , YAMAMOTO MASANORI , NAKADA MICHIO
IPC分类号： C08L69/00 , C08G64/06
摘要： PROBLEM TO BE SOLVED: To provide a polycarbonate resin composition excellent in surface hardness, heat-resistant moldability, color tone and impact resistance.SOLUTION: The polycarbonate resin composition is characterized in that the polycarbonate resin composition includes at least a polycarbonate resin (a) and a polycarbonate resin (b) having a different structural unit from that of the polycarbonate resin (a), and satisfies the following conditions. (i) The pencil hardness prescribed by ISO 15184 of the polycarbonate resin (a) is higher than the pencil hardness prescribed by ISO 15184 of the polycarbonate resin (b). (ii) The weight ratio of the polycarbonate resin (a) and the polycarbonate resin (b) in the polycarbonate resin composition is in a range of 1:99-45:55. (iii) The melt viscosity at temperature 280°C and shearing speed of 122 secof the polycarbonate resin (b) is higher than the melt viscosity at temperature 280°C and shearing speed of 122 secof the polycarbonate resin (a).
摘要翻译：要解决的问题：提供表面硬度，耐热成型性，色调和耐冲击性优异的聚碳酸酯树脂组合物。聚碳酸酯树脂组合物的特征在于，聚碳酸酯树脂组合物至少含有与聚碳酸酯树脂（a）的结构单元不同的聚碳酸酯树脂（a）和聚碳酸酯树脂（b），并且满足以下条件。（i）由聚碳酸酯树脂（a）的ISO 15184规定的铅笔硬度高于聚碳酸酯树脂（b）的ISO 15184规定的铅笔硬度。（ii）聚碳酸酯树脂组合物中的聚碳酸酯树脂（a）和聚碳酸酯树脂（b）的重量比在1:99-45:55的范围内。（iii）聚碳酸酯树脂（b）的280℃温度下的熔体粘度和122秒的剪切速度高于280℃的熔融粘度，聚碳酸酯树脂（a）的剪切速度为122秒。版权所有（C）2012，JPO＆INPIT

8. 发明专利

JP2012177091A Polycarbonate resin composition and method for manufacturing the same 审中-公开
标题翻译：聚碳酸酯树脂组合物及其制造方法
公开(公告)号：JP2012177091A
公开(公告)日：2012-09-13
申请号：JP2011256725
申请日：2011-11-24
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： NISHIHARA RYOHEI , HITOMI TATSUYA , YAMAMOTO MASANORI , NAKADA MICHIO
IPC分类号： C08L69/00
摘要： PROBLEM TO BE SOLVED: To provide a polycarbonate resin composition excellent in surface hardness, heat-resistant moldability or the like.SOLUTION: The polycarbonate resin composition includes at least a polycarbonate resin (a) and a polycarbonate resin (b) having a different structural unit from that of the polycarbonate resin (a), and the polycarbonate resin composition satisfies the following conditions. (i) The pencil hardness prescribed by ISO 15184 of the polycarbonate resin (a) is higher than the pencil hardness prescribed by ISO 15184 of the polycarbonate resin (b). (ii) The glass transition point Tg(a) of the polycarbonate resin (a) and the glass transition point Tg(b) of the polycarbonate resin (b) satisfy a relation of the equation 1. (iii) The pencil hardness prescribed by ISO 15184 of the polycarbonate resin composition is at least 2 rank higher than the pencil hardness prescribed by ISO 15184 of the polycarbonate resin (b).
摘要翻译：待解决的问题：提供表面硬度，耐热成型性等优异的聚碳酸酯树脂组合物。解决方案：聚碳酸酯树脂组合物至少包含与聚碳酸酯树脂（a）的结构单元不同的聚碳酸酯树脂（a）和聚碳酸酯树脂（b），聚碳酸酯树脂组合物满足以下条件。（i）由聚碳酸酯树脂（a）的ISO 15184规定的铅笔硬度高于聚碳酸酯树脂（b）的ISO 15184规定的铅笔硬度。（ii）聚碳酸酯树脂（a）的玻璃化转变点Tg（a）和聚碳酸酯树脂（b）的玻璃化转变点Tg（b）满足式（1）的关系。（iii）由聚碳酸酯树脂组合物的ISO 15184比聚碳酸酯树脂（b）的ISO 15184规定的铅笔硬度至少高2级。版权所有（C）2012，JPO＆INPIT

9. 发明专利

JP2012148579A Method of manufacturing particle-like polymer and device of manufacturing particle-like polymer 有权
标题翻译：制造颗粒状聚合物的方法和制造颗粒状聚合物的装置
公开(公告)号：JP2012148579A
公开(公告)日：2012-08-09
申请号：JP2012115038
申请日：2012-05-18
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： KUMAZAWA KATSUHISA , TAURA TAKAYUKI , YAMAMOTO MASANORI
IPC分类号： B29B9/06 , B29K69/00
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing a particle-like polymer such as a pellet having a uniform size or the like.SOLUTION: When a molten polymer is let to pass through a die head 11 having a plurality of holes and is made into strands followed by cutting the strands into the particle-like polymer, the molten polymer is supplied from the horizontal direction to the die head 11, and is extruded from the lower part of the die head 11 while the difference between the highest value and the lowest value of the temperature of the outlet of the die head 11 is controlled within a temperature of 5°C. The applicable molten polymer is for example a polycarbonate obtained by molten polycondensation by transesterification of an aromatic dihydroxy compound and a diester carbonate or the like.
摘要翻译：解决的问题：提供具有均匀尺寸等的颗粒状聚合物如颗粒的制造方法。解决方案：当使熔融的聚合物通过具有多个孔的模头11并制成股线，然后将线切割成颗粒状聚合物时，熔融聚合物从水平方向被供应到模头11，并且从模头11的下部挤出，同时模头11的出口的温度的最高值和最低值之间的差被控制在5℃的温度内。适用的熔融聚合物是例如通过芳族二羟基化合物和二酯碳酸酯等的酯交换而熔融缩聚获得的聚碳酸酯。版权所有（C）2012，JPO＆INPIT

10. 发明专利

JP2011214015A Polycarbonate resin 有权
标题翻译：聚碳酸酯树脂
公开(公告)号：JP2011214015A
公开(公告)日：2011-10-27
申请号：JP2011168646
申请日：2011-08-01
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： NAMIKI SHINGO , FUJI MICHIAKI , YAMAMOTO MASANORI
IPC分类号： C08G64/30
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently and stably producing a polycarbonate resin having excellent light resistance, transparency, hue, heat resistance, thermal stability and mechanical strength and stable performances.SOLUTION: The method for producing a polycarbonate resin comprises carrying out polycondensation by transesterification using a catalyst and, as raw material monomers, a carbonic acid diester and a dihydroxy compound, in a multistage process in a plurality of reactors. The carbonic acid diester used is purified by distillation. The dihydroxy compound comprises a plurality of kinds of dihydroxy compounds, in which at least one compound includes a -CH-O- moiety as a part of the structure (however, a moiety as a part of -CH-O-H is excluded). At least one reactor gives a distillation amount of monohydroxy compounds as a byproduct of the transesterification reaction, amounting to 20% or more of the theoretical distillation amount, and has an internal volume of 20 L or more, including a heating means for heating the reactor by use of a heating medium, and a reflux cooler, wherein the temperature difference between the heating medium and a reaction liquid in the reactor is at least 5°C. When the difference between a molar percentage of the dihydroxy compound upon feeding the compound as a raw material to the reactor, and a molar percentage of dihydroxy compound structural units in the obtained polycarbonate resin is divided by the molar percentage of the dihydroxy compound upon feeding the compound as a raw material to the reactor, the obtained value in terms of an absolute value falls in a specified range.
摘要翻译：要解决的问题：提供一种高效稳定地制造具有优异的耐光性，透明性，色调，耐热性，热稳定性和机械强度以及稳定性能的聚碳酸酯树脂的方法。解决方案：聚碳酸酯树脂的制造方法包括进行通过在多个反应器中的多级方法中使用催化剂和作为原料单体的碳酸二酯和二羟基化合物的酯交换进行缩聚。使用的碳酸二酯通过蒸馏纯化。二羟基化合物包含多种二羟基化合物，其中至少一种化合物包括-CH-O-部分作为结构的一部分（然而，作为-CH-O-H的一部分的部分被排除）。至少一个反应器产生作为酯交换反应的副产物的单羟基化合物的蒸馏量，其为理论蒸馏量的20％或更多，并且具有20L或更大的内部容积，包括用于加热反应器的加热装置通过使用加热介质和回流冷却器，其中加热介质和反应器中的反应液体之间的温度差为至少5℃。当将作为原料的化合物与反应器一起供给的二羟基化合物的摩尔百分数与得到的聚碳酸酯树脂中的二羟基化合物结构单元的摩尔百分比除以二羟基化合物在进料时的摩尔百分数化合物作为反应器的原料，所获得的绝对值的值落在指定范围内。

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