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1. 发明专利

JP2008162929A METHOD FOR PRODUCING SOLUTION OF α-SULFOFATTY ACID ALKYL ESTER SALT 审中-公开
标题翻译：用于生产α-硫酸亚硝酸盐盐溶液的方法
公开(公告)号：JP2008162929A
公开(公告)日：2008-07-17
申请号：JP2006353365
申请日：2006-12-27
申请人： Lion Corp , ライオン株式会社
发明人： KONDO FUSAO , ISHIKAWA TSUTOMU
IPC分类号： C07C303/32 , C07C309/58
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a solution of an α-sulfofatty acid alkyl ester salt for producing a concentrated α-sulfofatty acid alkyl ester salt having excellent storage stability.
SOLUTION: In the method for producing a solution of an α-sulfofatty acid alkyl ester salt by neutralizing an α-sulfofatty acid alkyl ester with an alkali substance, the neutralization process is carried out in the presence of 50-150 pts.mass of a 1-3C alcohol and 5-20 pts.mass of water based on 100 pts.mass of an α-sulfofatty acid alkyl ester salt.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供一种制备具有优异储存稳定性的浓缩α-磺基脂肪酸烷基酯盐的α-磺基脂肪酸烷基酯盐溶液的方法。解决方案：通过用碱性物质中和α-磺基脂肪酸烷基酯制备α-磺基脂肪酸烷基酯盐的溶液的方法中，中和过程在50-150℃的存在下进行。基于100磅的α-磺基脂肪酸烷基酯盐，1-3℃的醇和5-20磅的水的质量。版权所有（C）2008，JPO＆INPIT

2. 发明专利

JP2008024672A METHOD FOR PRODUCING α-SULFOFATTY ACID ALKYL ESTER SALT 审中-公开
标题翻译：生产α-硫酸酸性盐酸盐的方法
公开(公告)号：JP2008024672A
公开(公告)日：2008-02-07
申请号：JP2006201072
申请日：2006-07-24
申请人： Lion Corp , ライオン株式会社
发明人： ISHIKAWA TSUTOMU , NISHIO HIROSHI , ICHITANI TAKESHI , KIMURA YOSHIHIRO , OISHI TAKESHI
IPC分类号： C07C303/06 , C07C303/44 , C07C309/17
摘要： PROBLEM TO BE SOLVED: To provide a method by which an α-sulfofatty acid alkyl ester salt excellent in a color tone can be produced using a falling-film reactor.
SOLUTION: The method comprises a sulfonation process for sulfonating a fatty acid alkyl ester containing ≤0.5 mass% glycerol and its derivatives under a condition in which a coloring suppressant is absent by using the falling-film reactor, an aging process for carrying out an aging treatment by bringing the product prepared in the sulfonation process to contact with the coloring suppressant hardly soluble in the fatty acid alkyl ester in 0.1-10 mass% of the product within 30 minutes from discharge of the product from the falling-film reactor, an esterification process for esterifying the product prepared in the aging process using a 1-6C alcohol, a neutralization process for neutralizing the product prepared in the esterification process and a bleaching process for bleaching the product prepared in the neutralization process.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种通过使用降膜反应器可以产生色调优异的α-磺基脂肪酸烷基酯盐的方法。解决方案：该方法包括在通过使用降膜反应器在不存在着色抑制剂的条件下磺化含有≤0.5质量％甘油及其衍生物的脂肪酸烷基酯的磺化方法，通过将在磺化过程中制备的产物与难溶于脂肪酸烷基酯的着色抑制剂接触来进行时效处理，所述着色抑制剂在0.1-10质量％的产物中，在产物从降膜反应器中排出30分钟内使用1-6C醇酯化在老化过程中制备的产物的酯化方法，用于中和酯化过程中制备的产物的中和方法和漂白在中和过程中制备的产品的漂白方法。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2004250436A Sulfonation method and method for producing salt of alpha-sulfo fatty acid alkyl ester 有权
公开(公告)号：JP2004250436A
公开(公告)日：2004-09-09
申请号：JP2003409316
申请日：2003-12-08
申请人： Lion Corp , ライオン株式会社
发明人： NISHIO HIROSHI , MATOBA SEIJI , KIMURA YOSHIHIRO , ISHIKAWA TSUTOMU
IPC分类号： C07C303/06 , C07C303/28 , C07C309/17 , C07C309/22 , C07C309/70
摘要： PROBLEM TO BE SOLVED: To provide a method and an apparatus for sulfonation in a batch system, efficiently absorbing a sulfonation gas without flooding, dispersing the gas and carrying out a stable external circulation without cavitation, even in a system having ≥0.05 m/s superficial velocity of the gas.
SOLUTION: In the sulfonation method in which a raw material liquid phase is brought into contact with the sulfonation gas using the batch system agitation-mixing type reactor having an agitator, the sulfonation method is to carry out the sulfonation by bringing the position of an agitation blade of the agitator to be 0.20H-0.80H, wherein H expresses the height of the surface of the raw material liquid by bringing the height of reactor bottom to be 0, and a space in the height direction between the agitation blade and a gas inlet nozzle for introducing the sulfonation gas into the reactor to be ≤0.15H. The subject method for producing an α-sulfo fatty acid alkyl ester and a salt of the same is to use a sulfonation product obtained by sulfonating an fatty acid alkyl ester by using this method.
COPYRIGHT: (C)2004,JPO&NCIPI

4. 发明专利

JP2003081933A Method for producing sulfonated substance and method for producing surfactant 审中-公开
标题翻译：生产硫化物质的方法和生产表面活性剂的方法
公开(公告)号：JP2003081933A
公开(公告)日：2003-03-19
申请号：JP2001269565
申请日：2001-09-05
申请人： Lion Corp , ライオン株式会社
发明人： NISHIO HIROSHI , ISHIKAWA TSUTOMU , MIYAWAKI YOZO , TERAO TOSHIMI
IPC分类号： C07C303/06 , C07C305/10 , C07C309/30
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a sulfonated substance, with which the multi-product production of a sulfonated substance having an excellent color tone can simultaneously be carried out at a low cost, and to provide a method for producing a surfactant, using the sulfonated substance.
SOLUTION: In this method for producing the sulfonated substance, when gas containing SO
3 gas is branched from an SO
3 gas generation system through a branching route and introduced into a sulfonation reactor, the pressure difference (pressure before the branching-pressure under which the gas is introduced into the sulfonation reactor) of the gas containing SO
3 gas between pressure before the branching and pressure under which the gas is introduced into the sulfonation reactor is 0.005-0.04 MPa.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种生产磺化物质的方法，可以以低成本同时进行具有优异色调的多种产物的多产物生产，并提供一种制备表面活性剂的方法，使用磺化物质。解决方案：在制备磺化物质的方法中，当SO 3气体从SO 3气体发生系统通过分支路线分支并引入磺化反应器时，压力差（气体分支压力之前的压力引入到磺化反应器中）在分支压力之前的含有SO 3气体的气体和引入到磺化反应器中的压力之间的压力为0.005-0.04MPa。

5. 发明专利

JPH11172293A PRODUCTION OF CONCENTRATED AND DRIED SURFACTANT 失效
公开(公告)号：JPH11172293A
公开(公告)日：1999-06-29
申请号：JP35217797
申请日：1997-12-06
申请人： LION CORP
发明人： KATO DAISUKE , INOTSUKA TAKASHI , WATABIKI EMIKO , ISHIKAWA TSUTOMU
IPC分类号： F26B3/24 , B01D1/00 , B01F17/00 , C11D11/00 , C11D17/06 , F26B5/04
摘要： PROBLEM TO BE SOLVED: To obtain a concentrated and dried surfactant in one stage and to thereby reduce energy and the space of equipment by continuously flash- vaporizing an acidic solution containing an anionic surfactant precursor and a neutralizing alkali solution. SOLUTION: An acidic solution containing an acid precursor of an anionic surfactant and a neutralizing alkali solution are continuously fed into a heater and heated in a vacuum to form a gas-liquid mixed phase stream and to effect a neutralization, and the product is then introduced in a flash evaporator 13 and subjected to flash vaporization to remove water from the mixture and to thereby recover a concentrated and dried anionic surfactant. The obtained concentrated and dried surfactant has a low b value and an excellent hue because it has undergone little thermal deterioration during the neutralization.

6. 发明专利

JPH10219299A THIN FILM EVAPORATOR AND PRODUCTION OF SURFACTANT CONCENTRATE USING THE SAME 失效
公开(公告)号：JPH10219299A
公开(公告)日：1998-08-18
申请号：JP2302697
申请日：1997-02-05
申请人： LION CORP
发明人： INOTSUKA TAKASHI , HASHIMOTO SHINICHI , ISHIKAWA TSUTOMU , WATABIKI EMIKO
IPC分类号： B01D1/22 , C11D11/00
摘要： PROBLEM TO BE SOLVED: To grasp the water content of a concentrate produced with a thin film evaporator on a real time system and instantaneously correct the deviation from the target quality (water content). SOLUTION: This thin film evaporator 1 is designed to previously grasp the relationship between the temperature of a concentrate and a value of water content using the vacuum degree in the thin film evaporator 1 as a parameter, measure the temperature of the concentrate at the outlet with a concentrate temperature sensor 12, convert the temperature into the water content and control the evaporator 1. Thereby, control of high quick reponsiveness can be performed to reduce the dispersion of quality (water content) of the concentrate.

7. 发明专利

JPH10204479A SURFACTANT POWDER AND GRANULAR DETERGENT COMPOSITION 失效
公开(公告)号：JPH10204479A
公开(公告)日：1998-08-04
申请号：JP896197
申请日：1997-01-21
申请人： LION CORP
发明人： ISHIKAWA TSUTOMU , IWABUCHI HIROYUKI , HASHIMOTO SHINICHI , ABE SEIJI
IPC分类号： C11D1/28 , C11D3/30 , C11D3/34 , C11D3/36
摘要： PROBLEM TO BE SOLVED: To obtain the subject powder capable of exhibiting excellent oxidation resistance and suppressing discoloring due to long-term storage without impairing good aggregation resistance and solidification resistance and water soluble property and useful for granular detergent by compounding a specific amount of a chelating agent or antioxidant therein. SOLUTION: This surfactant powder comprises (A) >=40% α-sulfofatty acid alkyl ether salt, e.g. a compound of the formula [R is an 8-18C alkyl or alkenyl; R is a 1-5C alkyl or a monovalent alkali (earth) metal or a (substituted) ammonium] and (B) 0.001-0.4% chelating agent [e.g. ethylenediamine tetraacetic acid (salt)] or antioxidant (e.g. 2,6-di-tert.butyl-4-methylphenol), and in the surfactant powder, pH of 1wt.% aqueous solution thereof is >=7.5.

8. 发明专利

JPH10195497A PRODUCTION OF SURFACTANT POWDER AND GRANULAR DETERGENT COMPOSITION 失效
公开(公告)号：JPH10195497A
公开(公告)日：1998-07-28
申请号：JP587197
申请日：1997-01-16
申请人： LION CORP
发明人： WATABIKI EMIKO , HASHIMOTO SHINICHI , ISHIKAWA TSUTOMU , IWABUCHI HIROYUKI
IPC分类号： C11D1/04 , C11D1/28 , C11D3/37 , C11D10/04 , C11D11/00 , C11D17/06
摘要： PROBLEM TO BE SOLVED: To provide a method for producing surfactant powder high in solubility even in an aqueous alkaline solution, and to obtain a granular detergent composition capable of fully exhibiting the detergent performance of the surfactant powder. SOLUTION: First, a mixed slurry containing an α-sulfofatty acid alkyl ester salt, soap and water-soluble polycarboxylic acid and/or its salt is prepared, and then concentrated to a water content of =40wt.% of the α-sulfofatty acrid alkyl ester salt, >=10wt.% of the soap and 0.01-5wt.% of the water-soluble polycarboxylic acid and/or its salt based on the total amount of the above two ingredients. The granular detergent composition is obtained by incorporating the above surfactant powder.

9. 发明专利

JPH0920900A PRODUCTION OF SURFACTANT POWDER AND PRODUCTION OF GRANULAR DETERGENT COMPOSITION USING THE SAME 失效
公开(公告)号：JPH0920900A
公开(公告)日：1997-01-21
申请号：JP13580496
申请日：1996-05-01
申请人： LION CORP
发明人： ISHIKAWA TSUTOMU , WATABIKI EMIKO , MATSUI KOTARO
IPC分类号： C11D10/04 , C11D11/00 , C11D17/06
摘要： PROBLEM TO BE SOLVED: To efficiently obtain a surfactant powder of high concentration in no need of spray drying which requires a large amount of energy by concentrating a mixed slurry of a specific fatty acid ester salt and soap. SOLUTION: (A) an α-sulfofatty alkyl ester salt, for example, α-sulfo-10-20C (un)saturated fatty acid 1-5C alkyl ester salt, and (B) soap, for example, an alkali or alkaline earth metal salt of 10-18C (un)saturated fatty acid are mixed at a ratio of 10/90-95/5, the mixed slurry is concentrated to

10. 发明专利

JPH0711299A PRODUCTION OF SURFACTANT POWDER COMPOSITION 失效
公开(公告)号：JPH0711299A
公开(公告)日：1995-01-13
申请号：JP18440093
申请日：1993-06-28
申请人： LION CORP
发明人： INOTSUKA TAKASHI , IDE YASUHIKO , ISHIKAWA TSUTOMU
IPC分类号： C11D3/42 , C11D11/00 , C11D17/06
摘要： PURPOSE:To obtain the subject composition having improved color tone and high concentration economically in high yield by mixing a concentrated paste of a surfactant containing an anionic surfactant with an alkali builder, an aluminosilicate and a fluorescent brighter by a prescribed method and granulating. CONSTITUTION:The total of a granular material obtained by blending and granulating is 100wt.%. When (A) 20-70wt.% of a concentrated paste of a surfactant which contains an anionic surfactant (preferably sulfuric ester salt type or sulfonate type) and has >=60% surfactant concentration is mixed with (B) 15-60wt.% of an alkali builder containing a salt (e.g. potassium carbonate) of carbonic acid (hydrogen) and potassium and (C) 5-50wt.% of an aluminosilicate, (D) 0-01-4wt.% of a fluorescent brighter (e.g. compound of the formula) is added to the mixture or the component D is previously added to the component A and the resulting substance is mixed and granulated to give the objective composition. Preferably the component D is dissolved or dispersed into the component A, premixed and then blended with the components B and C and granulated.

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