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1. 发明专利

JP2010275258A Method of producing adamantanol 审中-公开
标题翻译：生产ADAMANTANOL的方法
公开(公告)号：JP2010275258A
公开(公告)日：2010-12-09
申请号：JP2009131313
申请日：2009-05-29
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： KOJIMA AKIO , FUJIKAWA NOBUO
IPC分类号： C07C29/12 , C07C35/37
摘要： PROBLEM TO BE SOLVED: To provide an industrially favorable method of producing an adamantanol from an adamantane with a high yield and high production efficiency without using an expensive carbocation-produced compound or an organic nitrile compound.
SOLUTION: The method includes reacting an adamantane with fuming sulfuric acid, thereafter adding the obtained reaction mixture to water to adjust a sulfuric acid concentration to 30-95 mass%, and hydrolyzing at a temperature of 0-60°C.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种在不使用昂贵的碳阳离子化合物或有机腈化合物的情况下以高产率和高生产效率从金刚烷生产金刚烷的工业上有利的方法。解决方案：该方法包括使金刚烷与发烟硫酸反应，然后将所得反应混合物加入水中以将硫酸浓度调节至30-95质量％，并在0-60℃的温度下水解。版权所有（C）2011，JPO＆INPIT

2. 发明专利

JP2008280315A Method for producing 2-adamantanone 有权
标题翻译：生产2-亚胺丹酮的方法
公开(公告)号：JP2008280315A
公开(公告)日：2008-11-20
申请号：JP2007128465
申请日：2007-05-14
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： KOJIMA AKIO , FUJIKAWA NOBUO , ONO HIDETOSHI , AIDA TETSUO
IPC分类号： C07C45/28 , C07B61/00 , C07C49/453
摘要： PROBLEM TO BE SOLVED: To provide a method for producing 2-adamantanone at high selectivity from adamantane and/or 1-adamantanol without detriment to the characteristic features of a production method using sulfuric acid.
SOLUTION: The method for producing 2-adamantanone is a method for producing 2-adamantanone by oxidizing adamantane and/or 1-adamantanol with sulfuric acid, wherein the oxidation with sulfuric acid is performed in the presence of a 2-5C haloalkane in which at least one halogen atom is bonded to each of two primary carbon atoms.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种以金刚烷和/或1-金刚烷醇的高选择性生产2-金刚烷酮的方法，而不损害使用硫酸的生产方法的特征。解决方案：2-金刚烷酮的制造方法是通过用硫酸氧化金刚烷和/或1-金刚烷来生产2-金刚烷酮的方法，其中用2-5℃卤代烷烃存在下用硫酸进行氧化其中至少一个卤素原子键合到两个伯碳原子中的每一个上。版权所有（C）2009，JPO＆INPIT

3. 发明专利

JP2007210947A Method for producing 2-adamantanol and 2-adamantanone 有权
标题翻译：生产2-植酰胺和2-亚胺丹酮的方法
公开(公告)号：JP2007210947A
公开(公告)日：2007-08-23
申请号：JP2006032680
申请日：2006-02-09
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： KOJIMA AKIO , FUJIKAWA NOBUO
IPC分类号： C07C29/56 , C07B61/00 , C07C35/37 , C07C45/29 , C07C49/643
CPC分类号： C07C29/56 , C07C49/453 , C07C2603/74 , C07C35/37
摘要： PROBLEM TO BE SOLVED: To provide a method for selectively and efficiently producing 2-adamantanol and 2-adamantanone from 1-adamantanol without using sulfuric acid, within an unconventionally short time, eco-friendly and suppressing byproduct (heavy product) production. SOLUTION: The method for producing 2-adamantanol and 2-adamantanone from 1-adamantanol by using at least one acid catalyst selected from Lewis acid and solid acid and coexistence with at least one compound selected from a group consisting of carboxylic acids, sulfonic acids and phosphoric acids, is characterized by producing 2-adamantanol and 2-adamantanone in the coexistence of adamantane. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种在非常规的时间内，从环境友好和抑制副产品（重产品）生产中选择性有效地生产1-金刚烷醇和不含硫酸的1-金刚烷酮的方法。解决方案：使用至少一种选自路易斯酸和固体酸的酸催化剂与1-金刚烷生产2-金刚烷酮和2-金刚烷酮的方法，并与至少一种选自羧酸，磺酸和磷酸的特征是在金刚烷共存下生产2-金刚烷醇和2-金刚烷酮。版权所有（C）2007，JPO＆INPIT

4. 发明专利

JP2006076895A Method for producing internal olefin, internal olefin mixture and oil-drilling base oil containing internal olefin mixture 审中-公开
标题翻译：用于生产内部烯烃的方法，内部烯烃混合物和含有内部烯烃混合物的油钻井基油
公开(公告)号：JP2006076895A
公开(公告)日：2006-03-23
申请号：JP2004259967
申请日：2004-09-07
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： SARUWATARI TETSUYA , FUJIKAWA NOBUO , YAMANE HIDEKI
IPC分类号： C07C5/25 , C07B61/00 , C07C11/02 , C09K8/58
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an internal olefin in which α-olefin which is a raw material is stably isomerized while suppressing adverse reaction such as skeletal isomerization reaction or heavy reaction of the α-olefin by using an inexpensive catalyst.
SOLUTION: In the method for producing the internal olefin by isomerizing a 16-18C α-olefin in the presence of a zeolite and/or montmorillonite catalyst, dried air or nitrogen having ≤-50°C dew point is previously made to flow at ≥150°C and water attached to the catalyst is removed until dew point of outlet gas of a catalyst layer becomes ≤-40°C and the 16-18C α-olefin is isomerized at 70-175°C.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：解决问题的方法：提供一种内部烯烃的制造方法，其中，作为原料的α-烯烃在抑制骨架异构化反应或α-烯烃的重反应等不良反应的同时，通过使用廉价的催化剂。解决方案：在沸石和/或蒙脱石催化剂存在下使16-18Cα-烯烃异构化制备内烯烃的方法中，预先将干燥的空气或具有≤-50℃露点的氮气流动在≥150℃，除去附着在催化剂上的水，直到催化剂层的出口气体的露点为≤-40℃，并且16-18℃的α-烯烃在70-175℃异构化。版权所有（C）2006，JPO＆NCIPI

5. 发明专利

JP2005350372A Method for producing internal olefin 有权
标题翻译：生产内部烯烃的方法
公开(公告)号：JP2005350372A
公开(公告)日：2005-12-22
申请号：JP2004170258
申请日：2004-06-08
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： SARUWATARI TETSUYA , FUJIKAWA NOBUO
IPC分类号： C07C5/25 , C07B61/00 , C07C11/00
摘要： PROBLEM TO BE SOLVED: To provide a method for industrially advantageously producing an internal olefin with a high isomeric conversion ratio, by selectively conducting internal isomerization of an α-olefin by the use of catalysts given at a low cost, while preventing side reactions, such as skeletal isomerization, oligomerization, and cracking.
SOLUTION: This method for producing the internal olefin comprises bringing the α-olefin into contact with a zeolite catalyst and/or a montmorillonite-based catalyst, so as to isomerize the olefin, wherein the α-olefin comprises a 12-20C olefin which has a concentration of oxygen derived from an oxo compound of ≤20 mass ppm.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种工业上有利地制备具有高异构转化率的内烯烃的方法，通过使用以低成本给出的催化剂选择性地导入α-烯烃的内部异构化，同时防止侧反应，如骨架异构化，低聚和裂解。解决方案：用于制备内烯烃的方法包括使α-烯烃与沸石催化剂和/或蒙脱石类催化剂接触以使烯烃异构化，其中α-烯烃包括12-20℃ 烯烃，其具有衍生自≤20质量ppm的氧化合物的氧的浓度。版权所有（C）2006，JPO＆NCIPI

6. 发明专利

JP2013032344A Process for production of 2-adamantanone 有权
标题翻译： 2-亚胺丹酮生产方法
公开(公告)号：JP2013032344A
公开(公告)日：2013-02-14
申请号：JP2012146243
申请日：2012-06-29
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： FUJIKAWA NOBUO , KOJIMA AKIO
IPC分类号： C07C45/28 , C07B61/00 , C07C49/453
摘要： PROBLEM TO BE SOLVED: To provide an industrially feasible highly productive simple process for completing reaction in a short period of time for production of 2-adamantanone.SOLUTION: The process for production of 2-adamantanone is the oxidation of adamantane at 70-90°C using 90-95 wt.% of sulfuric acid in the presence of a 2-5C halogenated alkane bound with at least one halogen atom to each of two primary carbons, with consecutive addition of sulfur trioxide gas and/or fuming sulfuric acid during oxidation, while maintaining the weight ratio (sulfuric acid/adamantane) of the total amount of sulfuric acid (total use weight of sulfuric acid, sulfur trioxide and fuming sulfuric acid, each based on 100% sulfuric acid) to the weight of the adamantane at 6 to 12 and maintaining the concentration of the sulfuric acid at 90-95 wt.% in the reaction system.
摘要翻译：要解决的问题：为了提供在短时间内完成用于生产2-金刚烷酮的反应的工业上可行的高生产率简单方法。解决方案：2-金刚烷酮的生产方法是在与至少一种卤素结合的2-5C卤代烷烃的存在下，使用90-95重量％的硫酸在70-90℃下氧化金刚烷原子与两个伯碳中的每一个，氧化期间连续加入三氧化硫气体和/或发烟硫酸，同时保持硫酸总量的重量比（硫酸/金刚烷）（硫酸的总使用重量，三氧化硫和发烟硫酸，各自基于100％硫酸）至6至12的金刚烷重量，并将反应体系中硫酸的浓度保持在90-95重量％。版权所有（C）2013，JPO＆INPIT

7. 发明专利

JP2010270028A Method for producing adamantanols 有权
标题翻译：生产苹果酸的方法
公开(公告)号：JP2010270028A
公开(公告)日：2010-12-02
申请号：JP2009121813
申请日：2009-05-20
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： KOJIMA AKIO , TAKAHASHI IKUKO , FUJIKAWA NOBUO
IPC分类号： C07C29/48 , C07B61/00 , C07C35/37
摘要： PROBLEM TO BE SOLVED: To industrially advantageously produce adamantanols from adamantanes in a short time in high yield. SOLUTION: A method for producing the adamantanols includes reacting the adamantanes in a mixed solution comprising a fuming sulfuric acid and an organic nitrile compound, and subjecting the obtained reaction liquid to hydrolytic treatment. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：在工业上有利地以高产率在短时间内从金刚烷生产金刚烷醇。解决方案：用于制备金刚烷醇的方法包括使金刚烷在包含发烟硫酸和有机腈化合物的混合溶液中反应，并将所得反应液进行水解处理。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2006070208A Internal olefin composition and oil drilling base oil containing this composition 有权
标题翻译：内部烯烃组合物和含有该组合物的油钻井基油
公开(公告)号：JP2006070208A
公开(公告)日：2006-03-16
申请号：JP2004257386
申请日：2004-09-03
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： SARUWATARI TETSUYA , FUJIKAWA NOBUO , YAMANE HIDEKI
IPC分类号： C09K8/32
CPC分类号： C09K8/32 , C10M105/04 , C10M2203/0206 , C10N2220/028 , C10N2220/10
摘要： PROBLEM TO BE SOLVED: To provide an olefin composition which has favorable biodegradability even when discharged in the environment and low toxicity to marine organisms and the like, and has sufficient fluid physicality when used for an oil drilling base oil and the like.
SOLUTION: An internal olefin composition is a mixture comprising a 16C olefin of 60-80 mass% and an 18C olefin of 40-20 mass%, wherein the content of α-olefin contained in this mixture is not more than 10 mass% and the content of a branched olefin is not more than 10 mass%.
COPYRIGHT: (C)2006,JPO&NCIPI

9. 发明专利

JP2005239651A Method for producing internal olefin 有权
标题翻译：生产内部烯烃的方法
公开(公告)号：JP2005239651A
公开(公告)日：2005-09-08
申请号：JP2004053153
申请日：2004-02-27
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： FUJIKAWA NOBUO
IPC分类号： C07C5/373 , C07B37/08 , C07B61/00 , C07C5/25 , C07C11/02
CPC分类号： C07B37/08 , C07C5/2518 , C07C11/02
摘要： PROBLEM TO BE SOLVED: To provide an industrially advantageous method for efficiently producing an internal olefin by selectively internally isomerizing α-olefin of a raw material while suppressing deterioration of catalyst and adverse reactions such as isomerization of skeleton, oligomerization and cracking by using an inexpensive catalyst.
SOLUTION: The method for producing the internal olefin comprises bringing α-olefin in which water content measured by a Karl Fischer titration method is ≤50 ppm into contact with zeolite and/or montmorillonite catalyst and isomerizing the α-olefin.
COPYRIGHT: (C)2005,JPO&NCIPI

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