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    • 1. 发明专利
    • Ultrasonic flowmeter, flow quantity control system, flow quantity measuring method and flow quantity control method
    • 超声波流量计,流量控制系统,流量测量方法和流量数控制方法
    • JP2012078270A
    • 2012-04-19
    • JP2010225441
    • 2010-10-05
    • Honda Electronic Co LtdKurita Water Ind Ltd本多電子株式会社栗田工業株式会社
    • NAGAREDA KENJIMATSUSHITA NAOTAKAYAMAKAWA HARUYOSHINAGAI TATSUO
    • G01F1/66G01F15/02
    • PROBLEM TO BE SOLVED: To provide an ultrasonic flowmeter capable of accurately measuring flow quantity of fluid even if a flowing characteristic of the fluid changes according to temperature or density of the fluid.SOLUTION: An ultrasonic sensor portion 33 in an ultrasonic flowmeter 27 includes a pair of ultrasonic vibrators 41 and 42 that are arranged on the upstream side and on the downstream side in a liquid pressure sending line 44 for flowing a cleaning liquid W1. The flowmeter 27 conducts: a step for measuring travel time of ultrasonic wave transmitted and received between the ultrasonic vibrators 41 and 42; a step for calculating a sonic speed and flow speed of the cleaning liquid W1 through computation based on the travel time of ultrasonic wave; a step for calculating the density of the cleaning liquid W1 through computation based on the sonic speed of the cleaning liquid W1 and a temperature measured by a temperature sensor part 45; a step for correcting the flow speed of the cleaning liquid W1 according to the temperature and density of the cleaning liquid W1; and a step for obtaining flow quantity of the cleaning liquid W1 based on the corrected flow speed.
    • 要解决的问题:提供一种能够精确地测量流体的流量的超声波流量计,即使流体的流动特性根据流体的温度或密度而变化。 解决方案:超声波流量计27中的超声波传感器部分33包括一对超声波振动器41和42,它们布置在用于使清洗液W1流动的液体压力输送管线44的上游侧和下游侧。 流量计27进行以下步骤:测量超声波振子41和42之间发送和接收的超声波的行进时间的步骤; 通过基于超声波的行进时间的计算来计算清洗液W1的声速和流速的步骤; 通过基于清洗液W1的声速和由温度传感器部45测定的温度进行计算来计算清洗液W1的密度的步骤; 根据清洗液W1的温度和密度校正清洗液W1的流速的步骤; 以及基于校正后的流速来求出清洗液W1的流量的步骤。 版权所有(C)2012,JPO&INPIT
    • 3. 发明专利
    • Cleaning method
    • 清洁方法
    • JP2008085150A
    • 2008-04-10
    • JP2006264788
    • 2006-09-28
    • Kurita Water Ind Ltd栗田工業株式会社
    • UCHIDA MINORUNAGAI TATSUO
    • H01L21/027H01L21/304
    • PROBLEM TO BE SOLVED: To provide a cleaning method for sufficiently cleaning a semiconductor substrate and the like on which a micro-pattern is formed.
      SOLUTION: Prior to bringing a cleaning liquid (chemical 60) into contact with an object (a semiconductor substrate 50) for cleaning, vacuum deairing, contacting surfactant and an osmotic solution, and deairing through supersonic are performed to improve surface wettability of the object. With the wettability improved, the cleaning liquid gets into concave parts of the pattern on the semiconductor substrate, etc., where a micro-pattern is formed, and as a result, poor cleaning caused by inappropriate wettability is circumvented, attaining a good cleaning effect. In addition, applying pressure with a cleaning liquid in contact with a cleaned object after wettability improvement enables the cleaning liquid to be effectively impregnated up to micro-depressions of the cleaned object, thus further enhancing the cleaning effect.
      COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题:提供一种用于充分清洁其上形成有微图案的半导体衬底等的清洁方法。 解决方案:在将清洁液(化学物质60)与用于清洁的物体(半导体基板50)接触之前,进行真空脱气,表面活性剂和渗透溶液接触,以及通过超音速脱气,以改善表面润湿性 物体。 随着润湿性的提高,清洗液进入形成有微图案的半导体基板等上的图案的凹部,结果,避免了由不适当的润湿性引起的不良清洗,达到良好的清洁效果 。 此外,在润湿性改善后,用与清洁物体接触的清洁液体施加压力使得清洗液能够有效地浸渍到被清洁物体的微凹陷处,从而进一步提高清洁效果。 版权所有(C)2008,JPO&INPIT
    • 4. 发明专利
    • Semiconductor substrate cleaning system
    • 半导体基板清洗系统
    • JP2007266477A
    • 2007-10-11
    • JP2006091899
    • 2006-03-29
    • Kurita Water Ind Ltd栗田工業株式会社
    • NAGAI TATSUOIKEMIYA NORITOYAMAKAWA HARUYOSHI
    • H01L21/027H01L21/304
    • PROBLEM TO BE SOLVED: To remove a resist suspended solid that shifts to a cleaning liquid and cannot be decomposed easily from the cleaning liquid effectively when cleaning a semiconductor substrate.
      SOLUTION: A semiconductor substrate cleaning system comprises: a clogging detection means 201 for arranging, in parallel, a plurality of filters 200a, 200b for capturing a resist shifted to the cleaning liquid by cleaning the semiconductor substrate, in a cleaning liquid transfer path 15 for transferring the cleaning liquid discharged from the cleaning device for cleaning the semiconductor substrate, and for detecting clogging in the filter; and a liquid leakage control means 220 for stopping liquid leakage to the filter in which clogging is detected and leaks liquid to other filters, when clogging is detected in one of the filters by the clogging detection means. As a result, the resist suspended solid generated by cleaning the semiconductor substrate is removed from the cleaning liquid effectively, and the filters are maintained without stopping the operation of the system, thus continuing a stable degree of cleaning.
      COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题:在清洗半导体衬底时,要去除转移到清洗液体上并且不能有效地从清洗液中分解的抗蚀剂悬浮固体。 解决方案:半导体衬底清洁系统包括:堵塞检测装置201,用于并行布置多个过滤器200a,200b,用于通过清洁半导体衬底捕获移动到清洁液体的抗蚀剂,在清洁液体转移 用于传送从用于清洁半导体衬底的清洁装置排出的清洁液体并且用于检测过滤器中的堵塞的路径15; 以及液体泄漏控制装置220,用于当通过堵塞检测装置在一个过滤器中检测到堵塞时,阻止液体泄漏到其中检测到堵塞的过滤器并将液体泄漏到其它过滤器。 结果,通过清洁半导体衬底产生的抗蚀剂悬浮固体被有效地从清洁液体中除去,并且保持过滤器而不停止系统的操作,从而持续稳定的清洁程度。 版权所有(C)2008,JPO&INPIT
    • 6. 发明专利
    • Cleaning equipment and method
    • 清洁设备和方法
    • JP2007103518A
    • 2007-04-19
    • JP2005289240
    • 2005-09-30
    • Kurita Water Ind Ltd栗田工業株式会社
    • IKEMIYA NORITONAGAI TATSUOYAMAKAWA HARUYOSHI
    • H01L21/304B08B3/08B08B3/10H01L21/027
    • PROBLEM TO BE SOLVED: To clean an electronic material substrate requiring a highly clean surface such as a silicon wafer, a glass substrate for liquid crystal, a photomask substrate and the like efficiently and surely, in a cleaning system employing a sulfuric acid.
      SOLUTION: This cleaning equipment comprises a pressurization vessel 1 containing a cleaned material (a semiconductor substrate 30) and cleaning the cleaned material by making it touch to a heated sulfuric acid solution 4. Preferably, the cleaning equipment comprises a means (SPM decomposition tub 15) for decomposing contaminants removed from the cleaned material in the pressurization vessel 1 and shifted to the sulfuric acid solution 4. Principally organic substances adhering to the cleaned material can be removed certainly by making the heated sulfuric acid solution 4 touch to the cleaned material in a pressurized atmosphere, and contaminants removed from the cleaned material and shifted to the sulfuric acid solution can be decomposed certainly in another process.
      COPYRIGHT: (C)2007,JPO&INPIT
    • 要解决的问题:在使用硫酸的清洁系统中,为了清洁需要高度清洁表面的电子材料基板,例如硅晶片,液晶玻璃基板,光掩模基板等, 。 解决方案:该清洁设备包括含有清洁材料(半导体衬底30)的加压容器1,并通过使其与加热的硫酸溶液4接触来清洁被清洁的材料。优选地,清洁设备包括一种装置 分解桶15),用于分解从加压容器1中清洁的材料中去除的污染物并转移到硫酸溶液4.主要是通过使加热的硫酸溶液4接触到清洁的物质,可以清除粘附到清洁的材料上的有机物质 在加压气氛中的材料和从清洁的材料中移出并转移到硫酸溶液中的污染物可以在另一个过程中被肯定地分解。 版权所有(C)2007,JPO&INPIT
    • 7. 发明专利
    • Sulfuric acid recycling type cleaning system
    • 硫酸回收型清洗系统
    • JP2007059603A
    • 2007-03-08
    • JP2005242743
    • 2005-08-24
    • Kurita Water Ind Ltd栗田工業株式会社
    • IKEMIYA NORITONAGAI TATSUOYAMAKAWA HARUYOSHI
    • H01L21/304B08B3/02B08B3/08B08B3/10H01L21/027
    • PROBLEM TO BE SOLVED: To improve throughput while obtaining a cleaning system which can continue cleaning, in a cleaning system using persulfate ions.
      SOLUTION: The sulfuric acid recycling type cleaning system comprises: a single wafer process cleaning equipment 1 for cleaning a material 30 to be cleaned by using a persulfuric acid solution as a cleaning fluid; electrolysis reaction tubs 20 and 25 for reproducing the persulfuric acid solution by generating persulfate ions from sulfuric acid ions contained in the solution by an electrolysis reaction; circulation lines 10a, 10b, 11a and 11b for circulating the persulfuric acid solution between a cleaning tub 1 and the electrolysis reaction tubs 20 and 25 which generate; and an ultraviolet-ray irradiation means 5 for irradiating ultraviolet-ray to the material 30 to be cleaned. Since a sulfuric acid solution is repeatedly used, the persulfuric acid solution can be reused in an on-site way for cleaning by utilizing an electrolysis reaction device. When cleaning, the generation of the sulfuric acid radicals is promoted while being irradiated by ultraviolet-ray to the cleaning solution, resulting in the improvement in the cleaning effect. It becomes possible to shorten working hours and to improve the throughput.
      COPYRIGHT: (C)2007,JPO&INPIT
    • 要解决的问题:在使用过硫酸根离子的清洁系统中,为获得能够继续清洗的清洁系统提高产量。 解决方案:硫酸循环型清洗系统包括:单晶硅工艺清洗设备1,用于通过使用过硫酸溶液作为清洗液来清洗待清洗的材料30; 电解反应槽20和25,用于通过电解反应从溶液中所含的硫酸离子产生过硫酸根离子来再现过硫酸溶液; 循环管路10a,10b,11a,11b,用于使过硫酸溶液在洗涤桶1和产生的电解反应槽20和25之间循环; 以及用于向待清洁的材料30照射紫外线的紫外线照射装置5。 由于重复使用硫酸溶液,所以可以通过利用电解反应装置,将现有的过硫酸溶液以现场的方式进行清洗。 当清洗时,通过紫外线照射到清洗溶液中促进了硫酸根的产生,从而提高了清洗效果。 可以缩短工作时间并提高吞吐量。 版权所有(C)2007,JPO&INPIT
    • 8. 发明专利
    • Sulfuric acid recycle type persulfuric acid feeder
    • 硫酸回收型磷酸供料器
    • JP2007051340A
    • 2007-03-01
    • JP2005237687
    • 2005-08-18
    • Kurita Water Ind Ltd栗田工業株式会社
    • IKEMIYA NORITONAGAI TATSUOYAMAKAWA HARUYOSHI
    • C25B15/02B08B3/08C25B1/30G03F7/42H01L21/027H01L21/304
    • PROBLEM TO BE SOLVED: To provide a persulfuric acid feeder where the concentration of persulfuric acid is sufficiently increased, thus recycling is repeatedly made possible, and an operation having increased safety is made possible. SOLUTION: The feeder is equipped with: a cleaning tank 1 of cleaning the material 30 to be cleaned with a persulfuric acid solution 2 as a cleaning liquid; electrolytic reaction tanks 10a, 10b of producing persulfate acid ions from sulfate ions comprised in the solution by electrolytic reaction, so as to produce a persulfuric acid solution; and circulation lines 4, 4a, 5 of circulating the persulfuric acid solution among the cleaning tank 1, and the electrolytic reaction tanks 10a, 10b. The feeder is further equipped with measurement means 21, 22, 23 for measuring the changing amount of operational physical property showing abnormal value upon an abnormal operation in the electrolytic reaction tanks or the like. The feeder is also equipped with safety devices 25a, 25b, 26 of performing a security operation to the electrolytic reaction tanks or the like upon the abnormal operation. A persulfuric acid solution is recycled and fed to the electrolytic reaction devices. Exact safety control and a security operation upon abnormality are secured. COPYRIGHT: (C)2007,JPO&INPIT
    • 要解决的问题:为了提供过硫酸的浓度充分增加的过硫酸给料器,因此可以重复进行再循环,并且可以实现增加安全性的操作。

      解决方案:进料器配有:清洗槽1,用作为清洗液的过硫酸溶液2清洗待清洗的材料30; 通过电解反应从溶液中含有的硫酸根离子生成过硫酸根离子的电解反应槽10a,10b,以产生过硫酸溶液; 以及使清洗槽1中的过硫酸溶液循环的循环管线4,4a,5以及电解反应槽10a,10b。 进料器还配备有测量装置21,22,23,用于测量在电解反应罐等中的异常操作时显示异常值的操作物理性能的变化量。 进料器还配备有在异常操作时对电解反应罐等进行安全操作的安全装置25a,25b,26。 将过硫酸溶液再循环并进料至电解反应装置。 确保正确的安全控制和异常时的安全操作。 版权所有(C)2007,JPO&INPIT

    • 9. 发明专利
    • Sulfuric acid recycling type cleaning system
    • 硫酸回收型清洗系统
    • JP2007050355A
    • 2007-03-01
    • JP2005237671
    • 2005-08-18
    • Kurita Water Ind Ltd栗田工業株式会社
    • IKEMIYA NORITONAGAI TATSUOYAMAKAWA HARUYOSHI
    • B08B3/08C25B1/30C25B11/12G03F7/42H01L21/027H01L21/304
    • Y02P20/52
    • PROBLEM TO BE SOLVED: To make the concentration of persulfuric acid sufficiently high to be repeatedly recycled, and to determine the life of a solution in a persulfuric acid supply apparatus.
      SOLUTION: The sulfuric acid recycling type cleaning system has: a cleaning tank 1 for cleaning a material 30 to be cleaned using a persulfate solution 2 as a cleaning liquid; electrolytic tanks 10a, 10b for electrolyzing the cleaning liquid discharged from the cleaning tank to generate persulfate ions from sulfate ions contained in the cleaning liquid to produce a persulfate solution; and circulation lines 4, 4a, 5, 5a for circulating the persulfate solution between the cleaning tank 1 and the electrolytic tanks 10a, 10b. The system further has impurity amount measuring means 16, 17a-17c, 18 for measuring the amount of impurity accumulated in the persulfate solution accompanied by cleaning. The sulfate solution is repeatedly used to regenerate the persulfate solution using an electrolytic apparatus on site, so as to use it for cleaning. Moreover, the life of the persulfate solution is accurately determined, thereby preventing the cleaning action from being lowered.
      COPYRIGHT: (C)2007,JPO&INPIT
    • 要解决的问题:使过硫酸的浓度足够高以重复循环,并确定过硫酸供应装置中的溶液的寿命。 解决方案:硫酸循环型清洗系统具有:清洗槽1,用于清洗使用过硫酸盐溶液2作为清洗液体的清洗材料30; 电解槽10a,10b,用于电解从清洗槽排出的清洗液体,以从洗涤液体中所含的硫酸根离子产生过硫酸根离子,生成过硫酸盐溶液; 以及用于在清洗槽1和电解槽10a,10b之间循环过硫酸盐溶液的循环管线4,4a,5,5a。 该系统还具有用于测量伴随清洗的在过硫酸盐溶液中积累的杂质量的杂质量测量装置16,17b-17c,18。 重复使用硫酸盐溶液,使用现场的电解设备再生过硫酸盐溶液,以用于清洗。 此外,能够精确地确定过硫酸盐溶液的寿命,防止清洗动作的降低。 版权所有(C)2007,JPO&INPIT