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1. 发明专利

JPS52102287A PREPARATION OF CYCLIC LACTONES 失效
公开(公告)号：JPS52102287A
公开(公告)日：1977-08-27
申请号：JP1841476
申请日：1976-02-24
申请人： HASEGAWA CO LTD
发明人： MATSUI MASANAO , OGAWA TOMOYA , TAKAGI KEIICHI , YAMATO TAKESHI , HAYASHI KAZUO
IPC分类号： C07D313/00
摘要： PURPOSE:Convenient method for preparing high-purity large-ring lactones useful as an ingredient for musk-, civet-, or amber-like perfumery.

2. 发明专利

JPS5931728A Preparation of nootkatone 失效
标题翻译： NOOTKATONE的制备
公开(公告)号：JPS5931728A
公开(公告)日：1984-02-20
申请号：JP14162782
申请日：1982-08-17
申请人： T Hasegawa Co Ltd
发明人： TAKAGI KEIICHI , MIZUTANI SHINICHI , HAYASHI KAZUO
IPC分类号： C07C45/33 , B01J31/00 , B01J31/12 , B01J31/22 , C07B61/00 , C07C45/00 , C07C49/653 , C07C67/00
CPC分类号： Y02P20/52
摘要： PURPOSE: To obtain nootkatone useful as a perfume industrially advantageously and selectively in high purity and yield in one step, by catalytically oxidizing valencene with oxygen or a gas containg the oxygen in an inert organic solvent in the presence of an organic heavy metallic catalyst.
CONSTITUTION: Valencene of formula 2 is catalytically oxidized with oxyen or a gas containing the oxygen in an inert organic solvent, e.g. benzene, in the presence of an organic heavy metallic catalyst, preferably an organometallic compound of Group VIII, e.g. Fe, Co, Ni, Ru, Rh, Pd or Ir, etc. to give nootkatone of formula 1 having a grapefruitlike fragrance in one step without passing through an intermediate step of hydroperoxide in danger of causing violent explosion by the technique of industrially advantageous catalytic oxidation industrially and easily in high conversion and yield. Compounds of formulas 3 and 4 formed as by-products in the above-mentioned reaction can be easily converted into the compound of formula 1.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过在有机重金属催化剂存在下，通过在氧气或含有惰性有机溶剂中的气体的气体催化氧化戊烯来获得工业上有效和选择性地高效纯化和产率的香精作为香料。构成：式2的戊烯在含有氧气或惰性有机溶剂中的氧的气体中被催化氧化。苯，在有机重金属催化剂存在下，优选第VIII族的有机金属化合物。 Fe，Co，Ni，Ru，Rh，Pd或Ir等，以一步法得到具有葡萄柚状香料的通式1的诺卡酮，而不经过通过工业上有利催化的技术引起剧烈爆炸的危险中的氢过氧化物的中间步骤在高转化率和产率下工业化和易于氧化。在上述反应中作为副产物形成的式3和4的化合物可以容易地转化成式1的化合物。

3. 发明专利

JPS5412309A 33HEXYNYLLAND CISSHEXENYL ETHERS* THEIR PREPARATION AND USE 失效
公开(公告)号：JPS5412309A
公开(公告)日：1979-01-30
申请号：JP7618777
申请日：1977-06-28
申请人： HASEGAWA CO LTD
发明人： MATSUI MASANAO , FURUHATA AKEMICHI , TADE HARUE , HAYASHI KAZUO
IPC分类号： C07C43/215 , A61K8/33 , A61Q13/00 , C07C41/00 , C07C43/14 , C07C67/00 , C11B9/00
摘要： PURPOSE:To prepare cis-3-hexynyl ethers easily in high yield, by the catalytic hydrogenation reaction of 3-hexynyl ethers which are new compounds useful as durable perfumes or perfume modifiers.

4. 发明专利

JPS5251381A PREPARATION OF LACTONES 失效
公开(公告)号：JPS5251381A
公开(公告)日：1977-04-25
申请号：JP12689075
申请日：1975-10-23
申请人： HASEGAWA CO LTD
发明人： MATSUI MASANAO , OGAWA TOMOYA , TAKAGI KEIICHI , YAMATO TAKESHI , HAYASHI KAZUO
IPC分类号： C07D313/00 , C07D327/02
摘要： PURPOSE:Novel method of preparing selectively and in good yield cyclic lactones useful as an ingredient of perfumery from a, omega-di(tri-substituted alkyl stannyloxy) alkanes.

5. 发明专利

JPS5318507A PREPARATION OF 2*66DIMETHYLL1*33OCTADIENEE66OL 失效
公开(公告)号：JPS5318507A
公开(公告)日：1978-02-20
申请号：JP10104877
申请日：1977-08-25
申请人： HASEGAWA CO LTD
发明人： YAMATO TAKESHI , KOSHIMIZU SHIGERU , HAYASHI KAZUO
IPC分类号： C07C29/132 , C07C27/00 , C07C33/02 , C07C67/00 , C11B9/00
摘要： PURPOSE:2,6-Dimethyl-1-,3-octadiene-6-ol of formula I.

6. 发明专利

JPS5257141A PROCESS FOR PREPARATION OF 33METHYLL22FORMYLMETHYLL22CYCLOPENTENEE11ON E 失效
公开(公告)号：JPS5257141A
公开(公告)日：1977-05-11
申请号：JP13054375
申请日：1975-10-31
申请人： HASEGAWA CO LTD
发明人： IWAMOTO MINORU , RIYOU HARUE , KOGAMI KUNIO , HAYASHI KAZUO
IPC分类号： C07C49/757 , C07C45/00 , C07C67/00 , C11B9/00
摘要： PURPOSE:The title compound of high purity, useful as intermediates of perfumery and pharmaceuticals, is prepared in high selectivity by the gas-phase dehydrogenation of 3-methyl-2-(2-hydroxyethyl)-2-cyclopentene-1-one under reduced pressure.

7. 发明专利

JPS5251341A PREPARATION OF CISSJASMONE 失效
公开(公告)号：JPS5251341A
公开(公告)日：1977-04-25
申请号：JP12688975
申请日：1975-10-23
申请人： HASEGAWA CO LTD
发明人： IWAMOTO MINORU , TADE HARUE , KOGAMI KUNIO , HAYASHI KAZUO
IPC分类号： C07C49/647 , C07C45/00 , C07C67/00
摘要： PURPOSE:Cis-jasmone of high purity is prepared in marketly improved yield from a halagenated-n-propyl-triphenylphosphonium salt in two steps.

8. 发明专利

JPS5238036A LONGGACTING TASTE AND FLAVOR MODULATOR AND METHOD OF PRODUCING THE SAM E 失效
公开(公告)号：JPS5238036A
公开(公告)日：1977-03-24
申请号：JP11207575
申请日：1975-09-18
申请人： HASEGAWA CO LTD
发明人： FUJITA AKIRA , YAMATO TAKESHI , KOGAMI KUNIO , HAYASHI KAZUO
IPC分类号： A23L27/20 , A61K8/00 , A61K8/49 , A61Q5/00 , C07D241/02 , C07D241/12 , C11B9/00
摘要： PURPOSE:Compound for modulating taste and flavor of foods, beverages, and perfumes for a prolonged period of time.

9. 发明专利

JPS51125205A PRECESS FOR PREPARATION OF CISS33HEXENOL AND ITS DERIVATIVES 失效
公开(公告)号：JPS51125205A
公开(公告)日：1976-11-01
申请号：JP3488975
申请日：1975-03-25
申请人： HASEGAWA CO LTD
发明人： FURUHATA AKEMICHI , YAMATO TAKESHI , KOGAMI KUNIO , HAYASHI KAZUO
IPC分类号： C07C69/145 , B01J31/00 , B01J31/22 , C07B61/00 , C07C27/00 , C07C29/00 , C07C29/17 , C07C33/02 , C07C33/025 , C07C41/00 , C07C43/14 , C07C43/15 , C07C43/166 , C07C43/20 , C07C43/215 , C07C67/00 , C07C69/00 , C07C69/007
摘要： PURPOSE:Cis-3-hexenol II,useful for perfumery,is prepared in high yield and high selectivity by the hydrogenation of 2,4-hexadienol I in the presence of catalysts.

10. 发明专利

JPS52102288A PREPARATION OF LARGE RING LACTONES 失效
公开(公告)号：JPS52102288A
公开(公告)日：1977-08-27
申请号：JP1841576
申请日：1976-02-24
申请人： HASEGAWA CO LTD
发明人： MATSUI MASANAO , OGAWA TOMOYA , TAKAGI KEIICHI , YAMATO TAKESHI , HAYASHI KAZUO
IPC分类号： C07D313/00
摘要： PURPOSE:To prepare high-purity large-ring lactones, useful as perfumes having musk-like odor, in high yield from readily available alpha, omega-dihydroxyalkanes.

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