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1. 发明专利

JP2012195134A Positive electrode active material substance based on lithium transition metal silicate, and method for manufacturing positive electrode for nonaqueous electrolyte secondary battery 有权
标题翻译：基于钛酸转移金属硅酸盐的正极活性物质物质，以及用于制造非电解电解质二次电池正极的方法
公开(公告)号：JP2012195134A
公开(公告)日：2012-10-11
申请号：JP2011057575
申请日：2011-03-16
申请人： Furukawa Electric Co Ltd:The , Furukawa Battery Co Ltd:The , 古河電気工業株式会社 , 古河電池株式会社
发明人： HIRAYAMA YOSUKE , OKUBO NORIO , ABE HIDETOSHI , NEMOTO MIYU
IPC分类号： H01M4/58 , C01B33/20 , H01M4/1397
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a positive electrode active material substance based on lithium transition metal silicate where the oxidation of a transition metal element is inhibited.SOLUTION: The method for manufacturing a positive electrode active material substance based on lithium transition metal silicate comprises the steps of (a) synthesizing a particle mixture from a lithium source, a transition metal source, and a silicon source, (b) mixing a carbon source into the particle mixture, (c) making a green compact by charging the particle mixture mixed with the carbon source into a mold and applying pressure, (d) burning the green compact in a filling atmosphere of an inert gas, and (e) pulverizing the green compact. More particularly, the particle mixture is preferably synthesized, in the step (a), by adopting an atomization firing method, where the lithium source, the transition metal source, and the silicon source are supplied to a flame with a flame-enhancing gas and a flammable gas.
摘要翻译：解决的问题：提供一种制造基于锂过渡金属硅酸盐的正极活性物质物质的方法，其中过渡金属元素的氧化被抑制。解决方案：制造基于锂过渡金属硅酸盐的正极活性物质物质的方法包括以下步骤：（a）从锂源，过渡金属源和硅源合成颗粒混合物，（b）将碳源混合到颗粒混合物中，（c）通过将与碳源混合的颗粒混合物装入模具中并施加压力来制备生坯，（d）在惰性气体的填充气氛中燃烧生坯，以及（e）粉碎生坯。更具体地说，在步骤（a）中，优选通过采用雾化燃烧法合成颗粒混合物，其中将锂源，过渡金属源和硅源用火焰增强气体供给火焰，易燃气体。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP2011181331A Cathode active material substance, cathode, secondary battery and manufacturing methods for same positive electrode active material, positive electrode, secondary battery and manufacturing methods for them 有权
标题翻译：阴极活性物质，阴极，二次电池和制造方法，用于同位素电极活性材料，阳极电极，二次电池及其制造方法
公开(公告)号：JP2011181331A
公开(公告)日：2011-09-15
申请号：JP2010044185
申请日：2010-03-01
申请人： Furukawa Battery Co Ltd:The , Furukawa Electric Co Ltd:The , 古河電気工業株式会社 , 古河電池株式会社
发明人： OKUBO NORIO , SHIMADA MICHIHIRO , UNO NAOKI , HIRAYAMA YOSUKE , TANI TOSHIO , ABE HIDETOSHI , AIDA MIYU
IPC分类号： H01M4/58 , H01M4/136 , H01M4/1397 , H01M4/36 , H01M4/66 , H01M4/70 , H01M10/052 , H01M10/0569
CPC分类号： H01M4/5825 , C01B33/021 , H01M10/052 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： PROBLEM TO BE SOLVED: To provide a lithium transition metal silicate having a small-particle diameter and low crystallinity, which can carry out charge/discharge reaction in an environment of room temperature, as a positive electrode active substance for nonaqueous electrolyte secondary battery, and to provide a manufacturing method for the metal silicate. SOLUTION: The lithium transition metal silicate is a material whose diffraction-peak half width value obtained as a result of analysis of the range of 2θ=5 to 50° by a powder X-ray diffraction method lies within the range of 0.175 to 0.6°, and in a microcrystal condition having crystals, with at least one portion of the same covered by an amorphous component; and a portion of the silicate is replaced by metal acid which does not emit oxygen, a phosphoric acid source or a boric acid source. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供在室温环境下进行充放电反应的具有小粒径和低结晶度的锂过渡金属硅酸盐作为非水电解质二次的正极活性物质电池，并提供金属硅酸盐的制造方法。解决方案：锂过渡金属硅酸盐是通过粉末X射线衍射法分析2θ= 5〜50°的范围而得到的衍射峰值半值值的材料在0.175的范围内至0.6°，并且在具有晶体的微晶状态下，其至少一部分被无定形成分覆盖; 并且一部分硅酸盐被不发射氧的金属酸，磷酸源或硼酸源代替。版权所有（C）2011，JPO＆INPIT

3. 发明专利

JP2011074476A Method for producing copper nanoparticle 有权
标题翻译：生产铜纳米微粒的方法
公开(公告)号：JP2011074476A
公开(公告)日：2011-04-14
申请号：JP2009229482
申请日：2009-10-01
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： HIRAYAMA YOSUKE
IPC分类号： B22F9/24 , B22F1/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing copper nanoparticles in which particle diameter is the nanosize of ≤10 nm, and also, a particle size distribution width is narrow.
SOLUTION: In the method for producing copper nanoparticles, cupic hydroxide (Cu(OH)
2 ) in a reduction reaction aqueous solution is brought into reduction reaction with an organic dispersant (D) in the presence of sodium borohydride (NaBH
4 ) as a reducing agent while stirring, copper ions formed by the dissolution of the cupic hydroxide and undissolved cupic hydroxide are coexistent in the aqueous solution during the reduction reaction, the copper ions in the aqueous solution are reduced so as to produce copper atoms and copper nanoparticles by the progression of the reduction reaction, in accordance with the same, the undissolved cupic hydroxide is continuously dissolved into the aqueous solution so as to produce copper ions, and the reduction reaction is performed at the saturated solubility of the cupic hydroxide or at a concentration less than that in the aqueous solution.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供粒径为≤10nm的纳米尺寸的纳米粒子的制造方法，粒径分布宽度窄。解决方案：在制备铜纳米颗粒的方法中，还原反应水溶液中的氢氧化铜（Cu（OH）2 SBB））在有机分散剂（D）的存在下进行还原反应的硼氢化钠（NaBH·SB> 4 ）作为还原剂，同时搅拌，通过氢氧化铜溶解和未溶解的氢氧化铜形成的铜离子在还原反应中在水溶液中共存，铜离子通过还原反应的进行，水溶液被还原以产生铜原子和铜纳米颗粒，根据相同的原理，将未溶解的氢氧化铜连续地溶解到水溶液中以产生铜离子，还原反应以氢氧化铜的饱和溶解度或低于水溶液中的浓度进行。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2011178601A Fine particle mixture, active material aggregate, positive electrode active material, positive electrode, secondary battery and method for producing these 有权
标题翻译：精细颗粒混合物，活性材料聚集体，阳极电极活性材料，阳极电极，二次电池及其生产方法
公开(公告)号：JP2011178601A
公开(公告)日：2011-09-15
申请号：JP2010044202
申请日：2010-03-01
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： OKUBO NORIO , YAGI TAKESHI , SHIMADA MICHIHIRO , UNO NAOKI , HIRAYAMA YOSUKE , NISHIMURA TAKESHI , TANI TOSHIO
IPC分类号： C01B33/12 , H01M4/134 , H01M4/36 , H01M4/58
CPC分类号： C01B33/32 , B82Y30/00 , C01B33/12 , C01B33/18 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C01P2004/62 , C01P2004/64 , H01M4/5825 , H01M10/052 , Y02T10/7011
摘要： PROBLEM TO BE SOLVED: To provide a fine particle mixture which can be converted to a precursor of a lithium transition metal silicate-based compound with a small particle size and low crystallinity, and to provide a positive electrode active material containing a lithium transition metal silicate-based compound and performing charge and discharge reactions in a room-temperature environment.
SOLUTION: The fine particle mixture is a mixture of silicon oxide fine particles, transition metal oxide fine particles and lithium transition metal silicate fine particles, and has diffraction peaks near 2θ=33.1° and near 2θ=35.7° in a powder X-ray diffraction measurement, wherein the silicon oxide fine particles and the transition metal oxide fine particles are amorphous and the lithium transition metal silicate fine particles are microcrystalline or amorphous. The positive electrode active material is obtained by pulverizing an active material aggregate obtained by heat treating the fine particle mixture.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供可以转化为具有小粒径和低结晶度的锂过渡金属硅酸盐系化合物的前体的微粒混合物，并提供含有锂的正极活性物质过渡金属硅酸盐基化合物，并在室温环境中进行充放电反应。解决方案：微粒混合物是氧化硅细颗粒，过渡金属氧化物微粒和锂过渡金属硅酸盐细颗粒的混合物，并且在粉末X中具有接近2θ= 33.1°和接近2θ= 35.7°的衍射峰射线衍射测量，其中氧化硅细颗粒和过渡金属氧化物细颗粒是无定形的，并且锂过渡金属硅酸盐细颗粒是微晶或无定形的。正极活性物质是通过粉碎通过热处理微粒子混合物得到的活性物质聚集体得到的。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2009242824A Manufacturing method of copper particulate dispersion liquid, and copper particulate dispersion liquid 有权
标题翻译：铜颗粒分散液和铜颗粒分散液的制造方法
公开(公告)号：JP2009242824A
公开(公告)日：2009-10-22
申请号：JP2008087945
申请日：2008-03-28
申请人： Furukawa Electric Co Ltd:The , Japan Advanced Institute Of Science & Technology Hokuriku , 古河電気工業株式会社 , 国立大学法人北陸先端科学技術大学院大学
发明人： HIRAYAMA YOSUKE , MAENOZONO SHINYA
IPC分类号： B22F9/00 , B01D21/01 , B01F17/16 , B01F17/22 , B01F17/38 , B01F17/42 , B01F17/52 , B01J13/00 , B22F9/24
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a copper particulate dispersion liquid in which the copper particulates modified by an aliphatic amine is dispersible in a high concentration in a specific dispersion liquid and which is excellent in dispersion stability for a long period of time, and a copper particulate dispersion liquid. SOLUTION: The method includes: (i) a step of adding a flocculation agent to an aqueous copper particulate dispersion liquid in which portions of copper particulates of a mean grain size 1 to 150 nm of primary particles are covered with a dispersant and are dispersed in the aqueous liquid and recovering the copper particulates; (ii) a step of adding the copper particulates into an aliphatic amine or a modification agent liquid composed of a liquid dissolved with the aliphatic amine in an organic liquid to obtain a dispersion liquid of the copper particulates in which the surfaces of the copper particulates are modified by the aliphatic amine under stirring; (iii) a step of adding the flocculation agent to the dispersion liquid, and recovering the modified copper particulate; and (iv) a step of obtaining the copper particulate by redispersing the modified copper particulates into the one or two or more dispersion liquids selected from chloroform. Limonene, and diol. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种铜颗粒分散液的制造方法，其中通过脂肪族胺改性的铜微粒在特定分散液中以高浓度分散，并且对于长的分散稳定性优异一段时间，和一个铜颗粒分散液。解决方案：该方法包括：（i）向铜颗粒分散液中加入絮凝剂的步骤，其中一次颗粒的平均粒径为1至150nm的铜颗粒的一部分被分散剂覆盖，分散在水性液体中并回收铜微粒; （ii）将铜微粒添加到有机液体中的脂肪族胺或由与脂肪族胺溶解的液体组成的改性剂液体的步骤，得到铜微粒表面的铜微粒的分散液，在脂肪胺搅拌下改性; （iii）将絮凝剂添加到分散液中并回收改性铜颗粒的步骤; 和（iv）通过将改性铜颗粒再分散到选自氯仿中的一种或两种或更多种分散液中来获得铜颗粒的步骤。柠檬烯和二醇。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2013211209A Positive electrode active material, production method thereof, and negative electrode and nonaqueous electrolyte secondary battery 有权
标题翻译：正极电极活性材料，其制造方法，负极和非电解电解质二次电池
公开(公告)号：JP2013211209A
公开(公告)日：2013-10-10
申请号：JP2012081801
申请日：2012-03-30
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： KAZAMA YOSHINORI , HIRAYAMA YOSUKE , OKUBO NORIO
IPC分类号： H01M4/58 , H01M4/13 , H01M4/36
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a positive electrode active material for coating positive electrode active material precursor particles with carbon while reducing the positive electrode active material precursor particles.SOLUTION: A method for producing a positive electrode active material includes a step of calcining positive electrode active material precursor particles while exposing to a reducing gas and a hydrocarbon gas. Another method for producing a positive electrode active material includes the steps of: adding a reducing agent to the positive electrode active material precursor particles, and calcining the positive electrode active material precursor particles while exposing the positive electrode active material precursor particles to a hydrocarbon gas.
摘要翻译：要解决的问题：提供一种用于在还原正极活性物质前体颗粒的同时还原正极活性物质前体颗粒的同时生产正极活性物质的正极活性物质的制造方法。解决方案：正极活性物质的制造方法包括：在暴露于还原气体和烃气体的同时煅烧正极活性物质前体颗粒。制造正极活性物质的另一种方法包括以下步骤：向正极活性物质前体颗粒中加入还原剂，并将正极活性物质前体颗粒暴露于烃气体同时煅烧正极活性物质前体颗粒。

7. 发明专利

JP2011098849A Oxide nanoparticle, oxide nanoparticle dispersed colloidal liquid and method for producing those 有权
标题翻译：氧化物纳米颗粒，氧化物纳米颗粒分散的胶体液体及其生产方法
公开(公告)号：JP2011098849A
公开(公告)日：2011-05-19
申请号：JP2009253488
申请日：2009-11-04
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： HIRAYAMA YOSUKE , YAGI TAKESHI , OKUBO NORIO
IPC分类号： C01B13/20 , C01B33/18
摘要： PROBLEM TO BE SOLVED: To provide a method for producing oxide nanoparticles, which can produce oxide nanoparticles having higher hydrophilicity in large quantities as compared with other gas phase methods, at a low cost.
SOLUTION: The method for producing oxide nanoparticles includes blowing a vaporized raw material on a core rod to form an oxide in a particle form on the core rod surface and to deposit the particles; and then, pulverizing the aggregate of the deposited particles.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种生产氧化物纳米颗粒的方法，其可以以低成本生产与其它气相方法相比大量生产具有较高亲水性的氧化物纳米颗粒。解决方案：制备氧化物纳米颗粒的方法包括在核棒上吹入气化的原料，以在芯棒表面上形成颗粒形式的氧化物并沉积颗粒; 然后粉碎沉积的颗粒的聚集体。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2013196934A Method for producing fine particle mixture, fine particle mixture, lithium ion secondary battery positive electrode active material, lithium ion secondary battery, and aqueous solution used in method for producing fine particle mixture 审中-公开
标题翻译：生产细颗粒混合物的方法，微粒混合物，锂离子二次电池正极电极活性材料，锂离子二次电池和用于生产细颗粒混合物的方法中使用的水溶液
公开(公告)号：JP2013196934A
公开(公告)日：2013-09-30
申请号：JP2012063418
申请日：2012-03-21
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： HIRAYAMA YOSUKE , KAZAMA YOSHINORI , OKUBO NORIO
IPC分类号： H01M4/58 , C01B33/32
CPC分类号： Y02E60/12
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fine particle mixture, and the like, the method being capable of continuously synthesizing lithium iron silicate having a small particle diameter and a uniform element distribution at low cost.SOLUTION: A silicon dioxide fine particle is used as a silicon source. Silicon dioxide dissolves in a strong base solution. Lithium hydroxide is therefor used as a lithium source in the present invention. Accordingly, when a silicon dioxide fine particle is mixed into a lithium hydroxide aqueous solution, the silicon dioxide fine particle dissolves into the solution. Divalent iron is preferably used as an iron source.
摘要翻译：要解决的问题：为了提供微粒混合物的制造方法等，该方法能够以低成本连续合成具有小粒径和均匀元素分布的锂铁硅酸盐。解决方案：二氧化硅细粉颗粒被用作硅源。二氧化硅溶解在强碱溶液中。氢氧化锂用作本发明的锂源。因此，当将二氧化硅微粒混入氢氧化锂水溶液中时，二氧化硅微粒溶解于溶液中。优选使用二价铁作为铁源。

9. 发明专利

JP2013193927A Method of producing particulate mixture, particulate mixture, lithium ion secondary battery positive electrode active material, lithium ion secondary battery, and aqueous solution used in method of producing the particulate mixture 有权
标题翻译：生产颗粒混合物，颗粒混合物，锂离子二次电池正极电极活性材料，锂离子二次电池和用于生产颗粒混合物的方法中使用的水溶液的方法
公开(公告)号：JP2013193927A
公开(公告)日：2013-09-30
申请号：JP2012063414
申请日：2012-03-21
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： HIRAYAMA YOSUKE , KAZAMA YOSHINORI , OKUBO NORIO
IPC分类号： C01B25/45 , H01M4/36 , H01M4/58
CPC分类号： Y02E60/12
摘要： PROBLEM TO BE SOLVED: To provide a method and the like of producing a particulate mixture capable of continuously synthesizing lithium iron phosphate having small particle diameter and uniform element distribution at low cost.SOLUTION: Preferably, a divalent iron chloride, which is a divalent iron, is used for an iron source. A phosphorous acid is used for a phosphorus source. The phosphorous acid has strong reduction characteristics. When a divalent iron is oxidized to a trivalent iron, it might precipitate hydroxides. Therefore, the phosphorous acid is applied to control progress of oxidation of iron. That is, the phosphorous acid serves as the phosphorus source and functions as an antioxidant for iron. For a lithium source, a lithium hydroxide is desirable because it is inexpensive and includes no corrosive substance such as chlorides.
摘要翻译：要解决的问题：提供一种能够以低成本生产能够连续合成小粒径和均匀元素分布的磷酸铁锂的颗粒混合物的方法等。解决方案：优选地，二价的氯化铁是二价铁，用于铁源。磷源用于磷源。亚磷酸具有很强的还原特性。当二价铁被氧化成三价铁时，可能沉淀出氢氧化物。因此，应用磷酸来控制铁的氧化进程。也就是说，磷酸作为磷源，作为铁的抗氧化剂起作用。对于锂源，氢氧化锂是优选的，因为它是便宜的，并且不包括腐蚀性物质如氯化物。

10. 发明专利

JP2012122135A Plating assistant, plating liquid, and plating material 审中-公开
标题翻译：涂层助剂，镀液和镀层材料
公开(公告)号：JP2012122135A
公开(公告)日：2012-06-28
申请号：JP2011252067
申请日：2011-11-17
申请人： Furukawa Electric Co Ltd:The , 古河電気工業株式会社
发明人： KITAGAWA SHUICHI , FUJII SHIGETO , HIRAYAMA YOSUKE , ITAGAKI MASAYUKI , SHITANDA ISAO
IPC分类号： C25D15/02 , C10M101/02 , C10M169/04 , C10N20/02 , C10N20/06 , C10N30/06 , C25D7/00 , H01H1/04
摘要： PROBLEM TO BE SOLVED: To provide a plating material whose slidability is enhanced by imparting lubricity to a surface plating film and which has good wear resistance and good contact reliability.SOLUTION: A plating assistant contains a capsule which encloses lubricating oil having a kinematic viscosity, at 40°C, of 100 mm/s or less and which includes an outer wall of a resin or an inorganic material. The capsule has an average particle diameter of 1 μm or less and when the diameter of the capsule is denoted by d and the thickness of the outer wall is denoted by t, the ratio t/d of the wall thickness to the diameter d is not less than 1/100 and less than 1/2.
摘要翻译：解决的问题：提供通过赋予表面电镀膜润滑性而提高滑动性并且具有良好的耐磨性和良好的接触可靠性的电镀材料。解决方案：电镀助剂包含胶囊，该胶囊包含在40℃下运动粘度为100mm /秒以下的运动粘度的润滑油，其包括外部树脂或无机材料的壁。胶囊的平均粒径为1μm以下，当胶囊的直径为d，外壁的厚度为t时，壁厚与直径d的比率t / d为小于1/100，小于1/2。版权所有（C）2012，JPO＆INPIT

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