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1. 发明专利

JP2005068088A Seven-membered ring ketimine borate, method for producing the same and curing agent for epoxy resin containing the same 审中-公开
标题翻译：七孔环硼酸钾，其制备方法及其含有环氧树脂的固化剂
公开(公告)号：JP2005068088A
公开(公告)日：2005-03-17
申请号：JP2003301173
申请日：2003-08-26
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res , 大日本インキ化学工業株式会社 , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI , MAKI HIROSHI
IPC分类号： C07D243/08 , C08G59/50
摘要： PROBLEM TO BE SOLVED: To provide a seven-membered ring ketimine borate scarcely having amine irritating smell, having a property which is very soluble in methanol, used as a curing agent for epoxy resin and useful in various industrial fields including a conventional curing for ethylenediamine epoxy resins and to provide a method for producing the seven-membered ring ketimine borate.
SOLUTION: The seven-membered ring ketimine borate is represented by general formula (1) (wherein R1, R2, R3 and R4 are each hydrogen or a 1-6C alkyl group such as methyl or ethyl group). The method for producing the seven-membered ring ketimine borate crystal comprises filtering a precipitate from a reaction solution of acetone with ethylenediamine or its homologue and boric acid and depositing the crystal. The curing agent for epoxy resins comprises the seven-membered ring ketimine borate.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供几乎不具有胺类刺激性气味的七元环酮亚胺硼酸盐，其具有非常易溶于甲醇的性质，用作环氧树脂的固化剂并可用于各种工业领域，包括常规的固化乙二胺环氧树脂，并提供一种生产七元环酮亚胺硼酸盐的方法。解决方案：七元环酮亚胺硼酸盐由通式（1）表示（其中R 1，R 2，R 3和R 4各自为氢或1-6C烷基如甲基或乙基）。制备七元环酮亚胺硼酸盐晶体的方法包括从丙酮与乙二胺或其同系物和硼酸的反应溶液中过滤沉淀物并沉积晶体。环氧树脂固化剂包括七元环酮亚胺硼酸盐。版权所有（C）2005，JPO＆NCIPI

2. 发明专利

JP2005272689A Methylhexamine condensed borate and novolak phenolic resin composition 审中-公开
标题翻译：甲基四氢INE ED ATE ATE TION TION TION TION TION TION TION TION TION TION
公开(公告)号：JP2005272689A
公开(公告)日：2005-10-06
申请号：JP2004089044
申请日：2004-03-25
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res , 大日本インキ化学工業株式会社 , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI , MAKI HIROSHI
IPC分类号： C07D471/22 , C08K3/38 , C08L61/06
摘要： PROBLEM TO BE SOLVED: To obtain a methylhexamine condensed borate useful in various industrial fields including a curing agent for a novolak phenolic resin.
SOLUTION: The methylhexamine condensed borate is expressed by formula (1). Preferably the borate is a crystalline hexamine condensed borate. Especially, the hexamine condensed borate is produced by reacting 1 mol of hexamine with 2-10 mol of an inorganic boric acid compound in terms of boron.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：获得可用于包括酚醛清漆酚醛树脂的固化剂的各种工业领域中的甲基六氢呋喃浓缩的硼酸盐。解决方案：甲基六胺浓缩的硼酸盐由式（1）表示。硼酸盐优选为结晶六胺缩合硼酸盐。特别地，通过使1摩尔六胺与2-10摩尔无机硼酸化合物以硼换算而产生六胺缩合硼酸盐。版权所有（C）2006，JPO＆NCIPI

3. 发明专利

JP2005089317A Piperidine condensed borate, epoxy resin curing agent and epoxy resin composition 审中-公开
标题翻译：哌嗪稠合硼酸酯，环氧树脂固化剂和环氧树脂组合物
公开(公告)号：JP2005089317A
公开(公告)日：2005-04-07
申请号：JP2003321197
申请日：2003-09-12
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res , 大日本インキ化学工業株式会社 , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI , MAKI HIROSHI
IPC分类号： C07D295/02 , C07F5/05 , C08G59/50
摘要： PROBLEM TO BE SOLVED: To provide a piperidine condensed borate which is useful in various fields, particularly as an epoxy resin curing agent by reacting piperidine with boric acid, that is, hardly has an amine irritating odor, has the property of easily dissolving in water and an organic solvent such as methanol and dimethyl sulfoxide (DMSO), can increase a boron content compared to the conventional boric acid compound added as a regulator of curing characteristics when used as an epoxy resin curing agent, accordingly gives a cured product having an extremely high glass transition temperature and exhibiting an effect of improving flame retardance.
SOLUTION: The piperidine condensed borate is represented by chemical formula (1). The piperidine condensed borate is particularly useful as an epoxy resin curing agent.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供可用于各种领域的哌啶稠合的硼酸盐，特别是作为环氧树脂固化剂，通过使哌啶与硼酸反应，即几乎不具有胺刺激性气味，具有容易的性质溶解在水和有机溶剂如甲醇和二甲基亚砜（DMSO）中时，与用作环氧树脂固化剂的固化特性调节剂相比，常规硼酸化合物可以增加硼含量，从而得到固化产物具有非常高的玻璃化转变温度并具有改善阻燃性的作用。解决方案：哌啶稠合的硼酸盐由化学式（1）表示。哌啶稠合的硼酸盐特别可用作环氧树脂固化剂。版权所有（C）2005，JPO＆NCIPI

4. 发明专利

JP2006045546A Thermosetting resin composition, boric acid-modified triazine structure-containing novolac resin and their preparation processes 审中-公开
标题翻译：热固性树脂组合物，含硼酸改性TRIAZINE结构的NOVOLAC树脂及其制备方法
公开(公告)号：JP2006045546A
公开(公告)日：2006-02-16
申请号：JP2005194933
申请日：2005-07-04
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res , 大日本インキ化学工業株式会社 , 財団法人川村理化学研究所
发明人： NAKAJIMA YASUTOSHI , YOSHIZAWA MASAKAZU , MIYAZAWA MASASHI , HARAGUCHI KAZUTOSHI , OBAYASHI AKIRA
IPC分类号： C08G59/62 , C08G8/28 , C08G59/20
摘要： PROBLEM TO BE SOLVED: To improve moisture and solder resistances which are required in the electric part fields and the electronic part field by giving an excellent heat resistance and an extremely good water resistance. SOLUTION: This resin composition contains, as its essential components, an epoxy resin and a phenol resin having a structure in which two or more aromatic rings in a molecule are connected with boric acid ester links by reacting a phenol resin containing a triazine structure such as a polycondensate of melamine, formalin, and phenol and the like with boric acid or a boric ester while removing water content in the system. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：通过提供优异的耐热性和极好的耐水性来改善电气部件领域和电子部件领域所需的耐湿性和焊料电阻。解决方案：该树脂组合物含有作为其主要成分的环氧树脂和酚醛树脂，其具有通过使含有三嗪的酚醛树脂反应而使分子中的两个以上的芳香环与硼酸酯连接物连接的结构结构如三聚氰胺，福尔马林和苯酚等的缩聚物与硼酸或硼酸酯同时除去体系中的水分含量。版权所有（C）2006，JPO＆NCIPI

5. 发明专利

JP2009149759A Preparation of cationic organic-inorganic composite hydrogel 有权
标题翻译：阳离子有机无机复合水凝胶的制备
公开(公告)号：JP2009149759A
公开(公告)日：2009-07-09
申请号：JP2007328519
申请日：2007-12-20
申请人： Kawamura Inst Of Chem Res , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI
IPC分类号： C08F2/44 , C08F292/00
摘要： PROBLEM TO BE SOLVED: To provide a preparation of a novel organic-inorganic composite hydrogel having not only high dynamic physical properties but also low water swellable properties. SOLUTION: The preparation of an organic-inorganic composite hydrogel with a three-dimensional network of the sodium pyrophosphate-containing water swellable clay mineral (B) and an organic polymer (A) obtained by copolymerization of a (meth)acrylamide or a derivative thereof and a polymerizable monomer having a quaternary ammonium base, comprises a step of preparing a homogeneous solution containing a (meth)acrylamide or a derivative thereof, a sodium pyrophosphate-containing water swellable clay mineral (B) and water (C), and adding a polymerizable monomer having a quaternary ammonium base simultaneously with a polymerization initiator or after addition of a polymerization initiator. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供不仅具有高动态物理性能，而且具有低水膨胀性能的新型有机 - 无机复合水凝胶的制备。解决方案：制备具有含焦磷酸钠的水可溶胀粘土矿物（B）和通过（甲基）丙烯酰胺或（甲基）丙烯酰胺共聚合获得的有机聚合物（A））的三维网络的有机 - 无机复合水凝胶其衍生物和具有季铵碱的可聚合单体包括制备含有（甲基）丙烯酰胺或其衍生物，含焦磷酸钠的水可溶胀粘土矿物（B）和水（C）的均匀溶液的步骤，并在聚合引发剂中加入具有季铵碱的可聚合单体，或加入聚合引发剂。版权所有（C）2009，JPO＆INPIT

6. 发明专利

JP2007177014A Borate group-containing allylamine polymer 审中-公开
标题翻译：含硼酸基的聚氨酯聚合物
公开(公告)号：JP2007177014A
公开(公告)日：2007-07-12
申请号：JP2005374741
申请日：2005-12-27
申请人： Kawamura Inst Of Chem Res , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI
IPC分类号： C08F30/06
摘要： PROBLEM TO BE SOLVED: To provide a polymer having new sugar chain recognition ability which contains allylamine borate units in the polymer skeleton.
SOLUTION: A borate group-containing allyl monomer obtained by reacting allylamine with an inexpensive boric acid is homopolymerized or copolymerized with a different monomer to obtain a borate group-containing allylamine polymer having sugar chain recognition ability which contains a borate group in the molecule and has inherent viscosity of 0.1-6 dL/g. The polymer can be highly biocompatible because it is hydrophilic and is excellent in sugar chain recognition ability. Further, the content of boron can be made higher than that in a conventional hydrophilic copolymer of phenylboric acid.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供在聚合物骨架中含有烯丙胺硼酸酯单元的具有新的糖链识别能力的聚合物。解决方案：将烯丙胺与廉价的硼酸反应得到的含硼酸酯基的烯丙基单体与不同的单体进行均聚或共聚，得到含有硼酸酯基的具有糖链识别能力的含有硼酸酯基的烯丙胺聚合物，其中含有硼酸根基团分子，其特性粘度为0.1-6 dL / g。聚合物由于是亲水性的并且具有优异的糖链识别能力，因此可以具有高生物相容性。此外，硼的含量可以比常规的苯基硼酸的亲水性共聚物的含量高。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2006089551A Method for producing boron-modified resol phenolic resin composition 有权
标题翻译：生产硼改性酚醛酚醛树脂组合物的方法
公开(公告)号：JP2006089551A
公开(公告)日：2006-04-06
申请号：JP2004274910
申请日：2004-09-22
申请人： Kawamura Inst Of Chem Res , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI
IPC分类号： C08G8/28
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a boron-modified resol phenolic resin composition which develops heat resistance and flame retardancy when cured and is excellent in solubility and moldability.
SOLUTION: The method for producing the boron-modified resol phenolic resin composition comprises dissolving in an amide solvent (C) a solid resol phenolic resin (A) obtained by reacting a phenol with an aldehyde in the presence of a basic catalyst and a boric compound (B) represented by the formula: B(OR)
n (OH)
3-n (wherein n is an integer of 0 to 3; R is an alkyl group of C
m H
2m+1 ; and m is an integer of 1 to 10) and reacting them at a temperature at which (A) is not cured.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种在固化时显示耐热性和阻燃性并且溶解性和成型性优异的硼改性甲阶酚醛树脂组合物的制造方法。解决方案：硼改性甲阶酚醛树脂组合物的制备方法包括在酰基溶剂（C）中溶解在碱性催化剂存在下使苯酚与醛反应得到的固体甲阶酚醛树脂（A），和由式（B）表示的硼化合物（B）：其中n为0〜3的整数，R为（A）未固化的温度下进行反应，并且使它们在（A）未固化的温度下反应。版权所有（C）2006，JPO＆NCIPI

8. 发明专利

JP2010215784A Organic-inorganic composite hydrogel and method for producing the same 有权
标题翻译：有机无机复合水凝胶及其制造方法
公开(公告)号：JP2010215784A
公开(公告)日：2010-09-30
申请号：JP2009064218
申请日：2009-03-17
申请人： Kawamura Inst Of Chem Res , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI , TAKEHISA KAN , MURATA KAZUTAKA
IPC分类号： C08L33/14 , C08F2/44 , C08K3/34
摘要： PROBLEM TO BE SOLVED: To provide an organic-inorganic composite hydrogel having both excellent mechanical properties and high swellability with a physiological saline, a dried article of the same, and a method for producing the same. SOLUTION: This organic-inorganic composite hydrogel includes a polymer of a water-soluble acrylic monomer and a water-swellable clay mineral. A monomer represented by formula (1) is used as the water-soluble acrylic monomer to provide the organic-inorganic composite hydrogel having both excellent mechanical properties and high swellability with a physiological saline as well as a dried article thereof excellent in flexibility. In formula (1), R 1 is a hydrogen atom or a methyl group, R 2 is a 2-3C alkylene group, n is an integer of 10-99, and Y is a methoxy or hydroxy group. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种具有优异的机械性能和高溶胀性的有机 - 无机复合水凝胶与生理盐水，其干燥制品及其制备方法。该有机 - 无机复合水凝胶包括水溶性丙烯酸类单体和水溶胀性粘土矿物的聚合物。使用由式（1）表示的单体作为水溶性丙烯酸单体，以提供具有优异的机械性能和高溶胀性的有机 - 无机复合水凝胶与生理盐水以及柔软性优异的干燥制品。在式（1）中，R 1 SP 1是氢原子或甲基，R 2是2-3C亚烷基，n是10-99的整数， Y为甲氧基或羟基。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2008074925A Borate group-containing organic inorganic composite hydrogel and method for producing the same 审中-公开
标题翻译：含硼有机无机复合水凝胶及其制造方法
公开(公告)号：JP2008074925A
公开(公告)日：2008-04-03
申请号：JP2006254179
申请日：2006-09-20
申请人： Kawamura Inst Of Chem Res , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI
IPC分类号： C08L101/00 , C08K3/34 , C08K3/38
摘要： PROBLEM TO BE SOLVED: To provide a new borate groups-introduced organic inorganic composite hydrogel having not only high dynamic properties but also hydrophilicity and excellent sugar chain recognizability, and to provide a method for producing the same.
SOLUTION: This borate group-containing organic inorganic composite hydrogel which contains borate groups in the three-dimensional network of an organic inorganic composite hydrogel formed from an amino group-having water-soluble organic polymer (A), a water-swelling clay mineral (B) and water (C) is characterized in that the borate groups are ionically bound to at least one part of amino groups in the amino group-having organic inorganic composite hydrogel.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种新的硼酸酯基导入的有机无机复合水凝胶，其具有不仅高的动态性能，而且具有亲水性和优异的糖链可识别性，并提供其制备方法。解决方案：这种含有硼酸酯基的有机无机复合水凝胶在由具有氨基的水溶性有机聚合物（A）形成的有机无机复合水凝胶的三维网络中含有硼酸酯基，水溶胀粘土矿物（B）和水（C）的特征在于硼酸酯基团与具有氨基的有机无机复合水凝胶中的至少一部分氨基离子结合。版权所有（C）2008，JPO＆INPIT

10. 发明专利

JP2006028246A Method for producing phenolic resin/silica composite spherical fine particle 有权
标题翻译：酚醛树脂/二氧化硅复合球形细颗粒的生产方法
公开(公告)号：JP2006028246A
公开(公告)日：2006-02-02
申请号：JP2004205846
申请日：2004-07-13
申请人： Kawamura Inst Of Chem Res , 財団法人川村理化学研究所
发明人： OBAYASHI AKIRA , HARAGUCHI KAZUTOSHI
IPC分类号： C08J3/12 , C08L61/06 , C09K3/14
摘要： PROBLEM TO BE SOLVED: To provide a method for producing composite spherical fine particles whose structure comprising a phenolic resin and silica is controlled, which have silica layers having proper hardness, and whose silica contents are easily controlled.
SOLUTION: This method for producing the phenolic resin/silica composite spherical fine particles is characterized by adding an aqueous solution containing an emulsion stabilizer (D) to an organic phase comprising a phenolic resin (A), a silicon compound (B) and an organic solvent (C) to invert and emulsify the organic layer phase, and then thermally curing the obtained fine particles.
COPYRIGHT: (C)2006,JPO&NCIPI

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