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1. 发明专利

JPS5910529A Production of norbornadiene derivative 失效
标题翻译：生产异丙苯衍生物
公开(公告)号：JPS5910529A
公开(公告)日：1984-01-20
申请号：JP11784682
申请日：1982-07-08
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res
发明人： OGAWA HIROSHI , ISHIZUKA MANABU , NAKANO HIROSHI , ONODERA NORIO
IPC分类号： C07C69/753 , C07C1/00 , C07C2/50 , C07C13/39 , C07C17/00 , C07C17/272 , C07C17/30 , C07C22/02 , C07C23/18 , C07C23/20 , C07C41/00 , C07C43/18 , C07C43/188 , C07C43/192 , C07C51/00 , C07C61/29 , C07C67/00 , C07C201/00 , C07C253/00 , C07C255/46 , C09K5/00 , C09K5/08 , F24J2/46
CPC分类号： F24J2/4649 , Y02E10/40
摘要： PURPOSE: The dehydration of a cyclopentenol derivative is carried out in the presence of an acidic substance at lower temperatures in the system to form a cyclopentadiene derivative and the product is made to react with an acetylene derivative to give the titled compound used as a substance for absorbing and storing solar energy.
CONSTITUTION: The reaction between a cyclopentenol derivative of formula I (R
1 WR
4 are electron-donating substituents such as 2,3-dimethylcyclopenta-2-ene- 1-ol and an acethylene derivative of formula II (R
5 , R
6 are electron-attracting substituents such as 1,1,1,4,4,4-hexafluorobutyne-2 is carried out in the presence of an acidic substance such as sulfuric or phosphoric acid in a solvent such as ether or chloroform at -50W50°C, preferably lower than 0°C to give a norbornadiene derivative such as 2,3-bis(trifluoromethyl)-5,6-dimethylnorbornadiene.
EFFECT: The process is operated at lower temperatures to cause scarce contamination of isomers.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：环戊烯醇衍生物的脱水在系统中在较低温度下在酸性物质存在下进行，形成环戊二烯衍生物，使产物与乙炔衍生物反应，得到标题化合物，用作物质吸收和储存太阳能。构型：式Ⅰ的环戊烯醇衍生物（R 1 -R 4为2,3-二甲基环戊-2-烯-1-醇和式Ⅱ的亚乙基衍生物（R5，R6）是给电子取代基的电子吸引取代基如1,1,1,4,4,4-六氟丁烯-2在酸性物质例如硫酸或磷酸的存在下，在溶剂如乙醚或氯仿中，-50-50℃下进行，优选低于0℃，得到降冰片二烯衍生物如2,3-双（三氟甲基）-5,6-二甲基降冰片二烯。效果：该方法在较低温度下操作，引起异味物的稀少污染。

2. 发明专利

JPS59206052A Isomerization catalyst 失效
标题翻译：异构催化剂
公开(公告)号：JPS59206052A
公开(公告)日：1984-11-21
申请号：JP8128583
申请日：1983-05-10
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res
发明人： NAKANO HIROSHI , OOAKU KENICHI
IPC分类号： C07C69/753 , B01J31/22 , C07B61/00 , C07C1/00 , C07C5/31 , C07C13/61 , C07C17/00 , C07C17/358 , C07C22/00 , C07C45/00 , C07C49/553 , C07C51/00 , C07C61/28 , C07C67/00 , C07C253/00 , C07C255/46
CPC分类号： Y02P20/52
摘要： PURPOSE: To improve catalytic activity by mixing powder of carbon, silica, alumina, etc. with insolubilized polystyrene and metallophthalocyanine polymer.
CONSTITUTION: Metallophthalocyanine polymer is obtd. by heating, for example, 1,2,4,5-tetracyanobenzene and anhydrous metallic chloride at 200°C for 1W2hr in formamide/glycol solvent. Active carbon, alumina sol, or silica sol is mixed with said metallophthalocyanine polymer, and the mixture is molded to an optional shape.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过将碳，二氧化硅，氧化铝等粉末与不溶性聚苯乙烯和金属酞菁聚合物混合来提高催化活性。构成：金属酞菁聚合物是有效的。例如通过在甲酰胺/乙二醇溶剂中在200℃下加热例如1,2,4,5-四氰基苯和无水金属氯化物1-2小时。将活性炭，氧化铝溶胶或二氧化硅溶胶与所述金属酞菁聚合物混合，并将混合物模塑成任意形状。

3. 发明专利

JPS61124951A Electrophotographic sensitive body 失效
标题翻译：电子感应敏感体
公开(公告)号：JPS61124951A
公开(公告)日：1986-06-12
申请号：JP24617784
申请日：1984-11-22
申请人： Dainippon Ink & Chem Inc
发明人： OAKU KENICHI , GUEN CHIYAN KEE , AIZAWA MASAO , NAKANO HIROSHI
IPC分类号： G03G5/043 , G03G5/06 , H01L51/42
CPC分类号： G03G5/0696
摘要： PURPOSE:To obtain an electrophotographic sensitive body having relatively high photosensitivity in a specified wavelength range and causing no problem on environmental safety by using a halogenated indium phthalocyanine compound having intensity peaks at 60 deg., 124 deg., 25.4 deg. and 27.8 deg. Bragg angles in its X-ray diffraction diagram and by forming a photosensitive layer contg. the compound dispersed in a binder. CONSTITUTION:A halogenated indium phthalocyanine compound is uniformly dispersed in a soln. of resin in an org. solvent with a dispersing machine, and the resulting dispersion is applied to a substrate and dried to manufacture an electrophotographic sensitive body. Any of various structures may be provided to the sensitive body. For example, a photosensitive layer contg. a halogenated indium phthalocyanine compound 2 dispersed in a binder 3 is formed on an electrically conductive support 1, a photosensitive layer contg. halogenated indium phthalocyanine compound 2 dispersed in a charge transferring medium consisting of a positive hole transferring substance 4, an electron transferring substance 5 and a binder 3 is formed on an electrically conductive support 1, or a photosensitive layer composed of a charge carrier generating layer B consisting of a halogenated indium phthalocyanine compound 2 and a binder 3 and a charge carrier transferring layer A consisting of a positive hole transferring substance 4, an electron transferring substance 5 and a binder 3 is formed on an electrically conductive support 1.
摘要翻译：目的：通过使用在60度，124度，25.4度的强度峰值的卤化铟酞菁化合物，在特定的波长范围内获得具有较高光敏性的电子照相感光体，并且对环境安全没有问题。和27.8度布拉格角在其X射线衍射图中并通过形成光敏层。该化合物分散在粘合剂中。构成：卤化铟酞菁化合物均匀地分散在溶胶中。的树脂在组织。溶剂，并将所得分散体施加到基材上并干燥以制造电子照相感光体。可以将任何各种结构提供给敏感体。例如，感光层分散在粘合剂3中的卤化铟酞菁化合物2形成在导电性载体1上，分散在由空穴转移物质4，电子转移物质5和粘合剂3组成的电荷转移介质中的卤化铟酞菁化合物2形成在导电载体1或由电荷载体产生层B组成的感光层在导电性支撑体1上形成由卤化铟酞菁化合物2和粘合剂3构成的电荷载体转印层A和由空穴转移物质4，电子转移物质5和粘合剂3构成的载流子转移层A.

4. 发明专利

JPS6145249A Laminate type electrophotographic sensitive body and its manufacture 失效
标题翻译：层压型电感敏感体及其制造
公开(公告)号：JPS6145249A
公开(公告)日：1986-03-05
申请号：JP16659184
申请日：1984-08-10
申请人： Dainippon Ink & Chem Inc
发明人： OAKU KENICHI , NAKANO HIROSHI , GUEN CHIYAN KEE , AIZAWA MASAO
IPC分类号： G03G5/043 , G03G5/06 , H01L51/42
CPC分类号： G03G5/0696
摘要： PURPOSE:To obtain superior photosensitivity and stability by forming an electrostatic charge generating layer made of a specified phthalocyanine vapor deposition layer. CONSTITUTION:The charge generating layer of a vapor deposition layer of chloroindium-phthalocyanine (Cl.InPc) heat treated so as to have the max. absorption wavelength in the range of 780-850nm at the time of its vapor deposition and/or after that to enhance its crystallinity and to ramarkably reduce the carrier traps due to nonuniformity of the crystal faces, thus permitting sufficient spectral sensitivity in the 800-850nm long wavelength region to be given and the obtained electrophotographic sensitive body to have especially superior aptitude for use in a laser beam printer using 750-850nm wavelength light source.
摘要翻译：目的：通过形成由特定酞菁蒸镀层制成的静电电荷产生层，以获得优异的光敏性和稳定性。构成：热处理氯阴离子（Cl.InPc）的蒸镀层的电荷产生层，吸收波长在780-850nm的范围内，和/或之后，以增强其结晶度，并由于晶面不均匀而明显地减少载流子阱，从而在800-850nm中具有足够的光谱灵敏度长波长区域和获得的电子照相感光体，以使用750-850nm波长光源的激光束打印机具有特别优异的性能。

5. 发明专利

JPS59141526A Quadricyclene derivative and method for storing light energy 失效
标题翻译：四氯化碳衍生物和储存光能的方法
公开(公告)号：JPS59141526A
公开(公告)日：1984-08-14
申请号：JP1503083
申请日：1983-02-01
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res
发明人： OOAKU KENICHI , OGAWA HIROSHI , NAKANO HIROSHI , ONODERA NORIO
IPC分类号： C09K5/00 , C07C17/00 , C07C19/08 , C07C22/04 , C07C67/00 , C09K5/08
摘要： NEW MATERIAL:A trifluoromethyl-substituted quadricyclene derivative of formula I (R
1 and R
2 are H, lower aliphatic group or aromatic hydrocarbon group; R
4 and R
5 are H, trifluoromethyl group or R
4 and R
5 are not H at the same time; R
3 and R
6 are H or lower aliphatic hydrocarbon group).
EXAMPLE: 2,3-Bis(trifluoromethyl)-5,6-dimethylnorbornadiene.
USE: Useful as a storing material for storing solar light energy, and capable of releasing the energy optionally as heat.
PREPARATION: A trifluoromethyl-substituted norbornadiene derivative of formula IIis irradiated with light in the presence or absence of a triplet sensitizer, e.g. acetophenone, and isomerized to give the aimed compound of formula I . The compound of formula I can be converted into the original norbornadiene derivative with a transition metallic compound, e.g. AgBF
4 , and thermal energy is generated at the time.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新物质：式I的三氟甲基取代的四环化合物（R 1和R 2是H，低级脂族基或芳族烃基; R 4和R 5是H，三氟甲基或R 4和R 5不同时为H; R 3和R 6 是H或低级脂族烃基）。实施例：2,3-双（三氟甲基）-5,6- dimethylnorbornadiene。用途：用作储存太阳光能的储存材料，并且能够任选地作为热释放能量。制备：在存在或不存在三联体敏化剂的情况下，用光照射式III的三氟甲基取代的降冰片二烯衍生物。苯乙酮，并异构化得到目标式I化合物。式I的化合物可以用过渡金属化合物例如四氢呋喃转化成原始的降冰片二烯衍生物。 AgBF4，当时产生热能。

6. 发明专利

JPS5915763A Lighting apparatus for collecting solar energy 失效
标题翻译：用于收集太阳能的照明装置
公开(公告)号：JPS5915763A
公开(公告)日：1984-01-26
申请号：JP12549582
申请日：1982-07-19
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res , Takenaka Komuten Co Ltd
发明人： ISHIZUKA MANABU , OGAWA HIROSHI , NAKANO HIROSHI , MIKAMI TADAO , SUZUKI SHIYOUICHI , KIMURA KOUZOU
IPC分类号： F24J2/42 , F24J2/04 , F24J2/34
CPC分类号： F24J2/0433 , F24J2/34 , Y02B10/20 , Y02E10/44
摘要： PURPOSE:To enable to absorb the solar energy efficiently, by utilizing the hollow space formed between a pair of plate member as a region for passing a light energy storing compound, and disposing a fibrous structural member in said region to serve as a guide for the energy storing compound. CONSTITUTION:A window frame 12 is shaped to have a rectangular cross section and an opening 18 is formed at a portion of the window frame 12. An outside glass 14 and an inside glass 16 are fixed to the window frame 12 near the opening 18 by the intermediary of sealers 20, and the hollow space formed between these two glasses 14 and 16 is utilized as a region 22 for passing a light energy storing compound. Further, a partition plate 24 is disposed at the middle portion of the window frame 12 so as to divide the inner space of the window frame 12 into an outer chamber 26 and an inner chamber 28. Since a fibrous structural member 36 is disposed in said region 22 to serve as a guide member for the light energy storing compound, it is enables to control the light intercepting rate.
摘要翻译：目的：为了能够有效地吸收太阳能，通过利用形成在一对板构件之间的中空空间作为通过光能储存化合物的区域，并且在所述区域中设置纤维结构构件以用作引导储能复合物。构成：窗框12被成形为具有矩形横截面，并且在窗框12的一部分处形成开口18.外玻璃14和内玻璃16通过开口18附近的窗框12固定到窗框12上密封件20的中间部分和这两个玻璃14和16之间形成的中空空间被用作通过光能储存化合物的区域22。此外，隔板24设置在窗框12的中间部分，以将窗框12的内部空间分成外室26和内室28.由于纤维结构构件36设置在所述区域22用作光能储存化合物的引导构件，能够控制遮光率。

7. 发明专利

JPS5910532A Norbornadiene derivative 失效
标题翻译： NORBORNADIENE DERIVATIVE
公开(公告)号：JPS5910532A
公开(公告)日：1984-01-20
申请号：JP11784782
申请日：1982-07-08
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res
发明人： OGAWA HIROSHI , ISHIZUKA MANABU , NAKANO HIROSHI , ONODERA NORIO
IPC分类号： C09K5/00 , C07C17/00 , C07C17/30 , C07C22/02 , C07C67/00 , C09K5/08
摘要： NEW MATERIAL:A norbornadiene derivative substituted with phenyl and trifluoromethyl of formula I (R
1 WR
4 are H, methyl, phenyl, and at least one of R
2 and R
3 is phenyl; R
5 , R
6 are H, trifluoromethyl and at least one of them is trifluoromethyl).
EXAMPLE: 2,3-Bis(trifluoromethyl)-1-methyl-5,6-diphenyl-norbornadiene.
USE: A substance for storing solar energy. It is solid near room temperature, lower than norbornadiene in flammability, higher in flame retardancy with reduced problems on stability and toxicity.
PREPARATION: The dehydration and Diels-Alder reaction are simultaneously effected between a cyclopentenol derivative of formula II and an acetylene derivative of formula III in a solvent such as ether in the presence of an acidic substance such as p-toluenesulfonic acid at -50W40°C to give the compound of formula I .
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：由式I的苯基和三氟甲基取代的降冰片二烯衍生物（R1-R4是H，甲基，苯基，R2和R3中的至少一个是苯基; R5，R6是H，三氟甲基，其中至少一个是三氟甲基）。实施例：2,3-双（三氟甲基）-1-甲基-5,6-二苯基 - 降冰片二烯。用途：用于储存太阳能的物质。在室温附近固体，可燃性低于降冰片二烯，阻燃性更高，稳定性和毒性降低。制备：脱水和Diels-Alder反应在式（Ⅱ）的环戊烯醇衍生物与式III的乙炔衍生物之间，在溶剂如乙醚中，在酸性物质如对甲苯磺酸存在下，在-50-40℃下同时进行得到式I化合物。

8. 发明专利

JPS58200960A Refrigeration system utilizing solar energy 失效
标题翻译：制冷系统利用太阳能
公开(公告)号：JPS58200960A
公开(公告)日：1983-11-22
申请号：JP8444082
申请日：1982-05-19
申请人： Dainippon Ink & Chem Inc , Kawamura Inst Of Chem Res , Takenaka Komuten Co Ltd
发明人： ISHIZUKA MANABU , NAKANO HIROSHI , FUJISAWA NOBURU , SUZUKI SHIYOUICHI , KIMURA KOUZOU , TANAKA YOSHITO
IPC分类号： F24S90/00 , F25B27/00
CPC分类号： F25B27/007 , Y02A30/277 , Y02B30/62
摘要： PURPOSE:To utilize even optical energy in a shortwave region of solar rays effectively, and to store energy for a prolonged term by heating a generator for an absorption type refrigerator by an optical-energy storing compound in a solar energy utilizing device. CONSTITUTION:Hot water mainly heated by the irradiation of long-wave rays in solar rays by a solar-ray collector 10 is stored in a hot-water storage tank 99 through a piping 86, and consumed through a hot-water supply piping 90 as required. On the other hand, a compound circulating collector section 16 receives shortwave rays in solar rays, and changes the optical-energy storing compound into a Q body (quadricyclene). The Q body is stored in a Q-body storage tank 38 through a feed pipe 36, but energy can be conserved for a prolonged term because the Q body does not return singly to an N body (norbornadiene). The Q body in the storage tank 38 is forwarded to the generator 44 for the absorption type refrigerator 12 in a feed piping 40 by a pump 42 as necessary, the generator 44 is heated by the heat of reaction through which the Q body returns to the N body by a catalyst device 54 in the generator, and a cooling piping 76 is cooled through a condenser 60 and an evaporator 56.
摘要翻译：目的：通过在太阳能利用装置中通过光能储存化合物加热用于吸收式冰箱的发生器，能够有效地在太阳光的短波区域中均匀地利用光能并长时间地储存能量。构成：通过太阳光线收集器10在太阳光线中照射长波射线加热的热水通过配管86储存在热水储存箱99中，并通过热水供给管90作为需要。另一方面，复合循环收集部16接收太阳光线中的短波，并将光储能化合物变为Q体（四环）。 Q体通过进料管36储存在Q体储存罐38中，但由于Q体不单独地返回到N体（降冰片二烯），所以能量可以长期保存。存储罐38中的Q体根据需要通过泵42被送到供给管40中的吸收式冷冻机12的发生器44，发生器44被反应热加热，Q通过该反应热Q返回到通过发电机中的催化剂装置54，冷却管道76通过冷凝器60和蒸发器56被冷却。

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