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1. 发明专利

JP2006022009A METHOD FOR PRODUCING 3-FLUORO-2,3-DIDEOXY-β-D-RIBOFURANOSYL-TYPE NUCLEOSIDE DERIVATIVE 审中-公开
标题翻译：生产3-氟-2,3-二脱氧-β-D-吡喃木糖型核苷衍生物的方法
公开(公告)号：JP2006022009A
公开(公告)日：2006-01-26
申请号：JP2004198851
申请日：2004-07-06
申请人： Ajinomoto Co Inc , Central Glass Co Ltd , セントラル硝子株式会社 , 味の素株式会社
发明人： ISHII AKIHISA , OTSUKA TAKASHI , KUME KOJI , KURIYAMA KATSU , TORII TAKAYOSHI , ONISHI TOMOYUKI , IZAWA KUNISUKE
IPC分类号： C07H1/00 , C07H19/16
CPC分类号： Y02P20/55
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a 3-fluoro-2,3-dideoxy-β-D-ribofuranosyl-type nucleoside derivative, capable of industrially producing the derivative, especially 3'-fluoro-2',3'-dideoxyguanosine, at a low cost. SOLUTION: This 3-fluoro-2,3-dideoxy-β-D-ribofuranosyl-type nucleoside derivative is produced by reacting a 3-halogeno-3-dideoxy-β-D-xylofuranosyl-type nucleoside derivative with sulfur tetrafluoride (SF 4 ), so as to convert the xylofuranosyl-type derivative into a 2-halogeno-2,3-dideoxy-3-fluoro-β-D-arabinofuranosyl-type nucleoside derivative with high regioselectivity, and then conducting, irrespective of order, a process (1) for subjecting a halogen atom at the 2'-position to dehalogenation, a process (2) for subjecting a protective group for a hydroxy group at the 5'-position to deprotection, and, if necessary, a process (3) for conducting at least any one of protection, deprotection, and modification of a nucleic-acid base or its derivative. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种能够在工业上生产该衍生物的3-氟-2,3-二脱氧-β-D-呋喃核糖型核苷衍生物的制备方法，特别是3'-氟-2' ，3'-二脱氧鸟苷，成本低廉。解决方案：3-氟-2,3-二脱氧-β-D-呋喃核糖基型核苷衍生物通过3-卤代-3-二脱氧-β-D-木糖呋喃糖基型核苷衍生物与四氟化硫（SF 4 ），将该恶二糖基型衍生物转化为具有高区域选择性的2-卤代-2,3-二脱氧-3-氟-β-D-阿拉伯呋喃糖基型核苷衍生物，然后进行将2位的卤原子进行脱卤的步骤（1），不管其顺序如何，将在5'-位保护基进行羟基保护基脱保护的方法（2）如果需要，可以进行核酸碱基或其衍生物的保护，脱保护和修饰中的至少任一种的方法（3）。版权所有（C）2006，JPO＆NCIPI

2. 发明专利

JP2010018785A Fluorine-containing polymer and antistatic agent wherein the same is used 有权
标题翻译：使用含氟聚合物和抗静电剂
公开(公告)号：JP2010018785A
公开(公告)日：2010-01-28
申请号：JP2009132603
申请日：2009-06-01
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： TERUI TAKAAKI , KOMORIYA HARUHIKO , INOUE SUSUMU , KUME KOJI
IPC分类号： C08F20/38 , C08F16/16 , C08F32/08 , C09K3/16
CPC分类号： C09K3/16 , C08F20/24 , C08F20/38 , C08F212/14 , C08F220/38 , C08L33/16 , Y10T428/3154 , Y10T428/31649
摘要： PROBLEM TO BE SOLVED: To provide a synthetic resin composition having excellent weather resistance, antistatic properties and excellent transparency.
SOLUTION: A fluorine-containing polymer contains a repeating unit shown by general formula (2) (wherein W represents a linking group; R
1 s each independently represents a perfluoroalkyl group; Q represents a unit structure formed by cleaving the double bond of a polymerizable double-bond-containing group; M
+ represents a hydrogen cation, a metal ion or the quaternary ammonium cation shown by general formula (15) (wherein R
11 to R
14 are each a 1-20C alkyl or aryl group having or not having a substituent group, independently)).
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供具有优异的耐候性，抗静电性和优异的透明性的合成树脂组合物。解决方案：含氟聚合物含有通式（2）所示的重复单元（其中W表示连接基团; R“SP”1各自独立地表示全氟烷基; Q表示单元通过切断含有可聚合双键的基团的双键形成的结构; M

3. 发明专利

JP2008255100A Method for producing trifluoromethanesulfonyl fluoride 审中-公开
标题翻译：生产三氟甲磺酰氟的方法
公开(公告)号：JP2008255100A
公开(公告)日：2008-10-23
申请号：JP2008048951
申请日：2008-02-29
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： SAKAI SHIGENORI , MORINAKA TAKAYOSHI , MINAMIMEI TSUTOMU , KUME KOJI
IPC分类号： C07C303/02 , C07C309/80
摘要： PROBLEM TO BE SOLVED: To provide a method for producing trifluoromethanesulfonyl fluoride, which method, as compared with a conventional production method, can be carried out in fewer steps, in higher yields, and with higher purity.
SOLUTION: The method for producing trifluoromethanesulfonyl fluoride (CF
3 SO
2 F) is a method for producing trifluoromethanesulfonyl fluoride (CF
3 SO
2 F) by reacting trifluoromethanesulfonyl chloride (CF
3 SO
2 Cl) with a metal fluoride in the presence of water, wherein a halogenated quaternary salt is present combinedly.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供一种三氟甲磺酰氟的制备方法，与常规生产方法相比，该方法可以较少的步骤，更高的产率和更高的纯度进行。解决方案：三氟甲磺酰氟（CF 3 SB 3 SO 2）的制备方法是制备三氟甲磺酰氟（CF 3 SBSO 3 通过在水存在下使三氟甲磺酰氯（CF 3 SB 3 SO 2）与金属氟化物反应，其中卤化季盐结合在一起。版权所有（C）2009，JPO＆INPIT

4. 发明专利

JP2011037804A Method for producing hexafluoroacetone monohydrate 有权
标题翻译：用于生产十六烷基二醇单硬脂酸酯的方法
公开(公告)号：JP2011037804A
公开(公告)日：2011-02-24
申请号：JP2009189347
申请日：2009-08-18
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： KATSUHARA YUTAKA , HAYASAKA TATSUYA , WATANABE MINEO , KUME KOJI
IPC分类号： C07C45/82 , C07C29/00 , C07C29/82 , C07C31/42 , C07C49/167
CPC分类号： C07C29/82 , C07C31/42
摘要： PROBLEM TO BE SOLVED: To provide a method for producing hexafluoroacetone monohydrate (1,1,1,3,3,3-hexafluoropropane-2-diol), and to provide a hexafluoroacetone monohydrate composition having a form easily handled.
SOLUTION: There is disclosed the method for producing hexafluoroacetone monohydrate by: (1) a hydration method of making hexafluoroacetone absorbed into either water or hexafluoroacetone hydrate in an organic solvent; or (2) a dehydration method of distilling a mixture of hexafluoroacetone hydrate with an organic solvent to thereby remove a mixture of water and the organic solvent as a low-boiling composition in a simple manner and in a high yield, and thus obtaining a mixture of hexafluoroacetone monohydrate with the organic solvent as a high-boiling composition.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供生产六氟丙酮一水合物（1,1,1,3,3,3-六氟丙烷-2-二醇）的方法，并提供易于处理的形式的六氟丙酮一水合物组合物。解决方案：公开了通过以下方法制备六氟丙酮单水合物的方法：（1）在有机溶剂中将六氟丙酮吸收到水或六氟丙酮水合物中的水合方法; 或者（2）将六氟丙酮水合物与有机溶剂的混合物进行蒸馏的脱水方法，从而以简单的方式和高收率地除去作为低沸点组合物的水和有机溶剂的混合物，从而得到混合物的六氟丙酮一水合物与有机溶剂作为高沸点组合物。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2010173959A Method for purifying trifluoromethanesulfonyl fluoride 有权
标题翻译：净化三氟甲磺酰氟的方法
公开(公告)号：JP2010173959A
公开(公告)日：2010-08-12
申请号：JP2009017412
申请日：2009-01-29
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： SAKAI SHIGENORI , MORINAKA TAKAYOSHI , MINAMIMEI TSUTOMU , KUME KOJI
IPC分类号： C07C303/44 , C07C303/22 , C07C309/80
摘要： PROBLEM TO BE SOLVED: To provide a method for producing trifluoromethanesulfonyl fluoride in a higher yield and higher purity as compared with those of the conventional production methods.
SOLUTION: Trifluoromethane sulfonic acid is obtained by reacting a metal hydroxide with trifluoromethanesulfonyl fluoride and then treating with an acid. Then, by reacting phosphorus trichloride and chlorine with the trifluoromethane sulfonic acid, trifluoromethanesulfonyl chloride (CF
3 SO
2 Cl) is obtained. Then, by reacting a metal fluoride with the trifluoromethanesulfonyl chloride in the presence of 0.6 to 10.0 mass% water based on 100 mass% metal fluoride, the trifluoromethane sulfonyl fluoride is obtained. Thereby, the trifluoromethanesulfonyl fluoride produced by electrolytic fluorination can be purified by passing through 3 processes in high selectivity and the high purity. It is a very excellent method for producing the same in an industrial scale.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：与常规生产方法相比，提供一种以高产率和更高纯度生产三氟甲磺酰氟的方法。解决方案：三氟甲磺酸是通过使金属氢氧化物与三氟甲磺酰氟反应，然后用酸处理得到的。然后，通过使三氯化磷和氯与三氟甲磺酸反应，得到三氟甲磺酰氯（CF 3 SB 3 SO 3）。然后，通过使金属氟化物与三氟甲磺酰氯在基于100质量％的金属氟化物的0.6〜10.0质量％的水的存在下反应，得到三氟甲磺酰氟。因此，通过电解氟化生产的三氟甲磺酰氟可以通过高选择性和高纯度的3种方法进行纯化。这是一种非常优秀的工业生产方法。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2009242391A New salt having fluorine-containing carbanion structure, derivative thereof, photoacid generator, resist material using the photoacid generator, and pattern forming method 有权
标题翻译：具有含氟化合物的碳酸盐结构的新盐，其衍生物，光致发电机，光电发生器的耐腐蚀材料和图案形成方法
公开(公告)号：JP2009242391A
公开(公告)日：2009-10-22
申请号：JP2009059003
申请日：2009-03-12
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： NAGAMORI MASASHI , NARIZUKA SATOSHI , INOUE SUSUMU , KUME KOJI
IPC分类号： C07C317/18 , C07C381/12 , C09K3/00 , G03F7/004 , G03F7/039 , G03F7/38
CPC分类号： C07C381/12 , C07C317/18 , C07C2603/74 , C08F220/28 , G03F7/0045 , G03F7/0046 , G03F7/0397 , C08F220/18 , C08F220/24 , C08F232/08
摘要： PROBLEM TO BE SOLVED: To provide a photoacid generator which is highly sensitive to ArF excimer laser light and the like and generates an acid (photoacid) having sufficiently high acidity, exhibits high solubility in resist solvents and excellent compatibility with resins; and to provide a resist material containing such a photoacid generator.
SOLUTION: A photoacid generator for chemically amplified resist materials, which generates an acid having a fluorine-containing carbanion structure represented by general formula (4) is used. In general formula (4), n represents an integer of 1 to 3. R' represents a hydrogen atom or a 1-3C substituted or unsubstituted alkyl group. R represents an adamantyl group or the like, A represents a bivalent functional group such as a carbonyl group, R
F and R
F ' each independently represents a 1-4C perfluoroalkyl group.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：为了提供对ArF准分子激光等高度敏感的光致酸产生剂，并且产生具有足够高酸度的酸（光酸），在抗溶剂溶剂中表现出高溶解性和与树脂的相容性优异; 并提供含有这种光致酸产生剂的抗蚀剂材料。解决方案：使用用于产生具有由通式（4）表示的含氟碳负离子结构的酸的化学放大抗蚀剂材料的光致酸发生器。在通式（4）中，n表示1〜3的整数.R'表示氢原子或1-3C取代或未取代的烷基。 R表示金刚烷基等，A表示二价官能团，例如羰基，R SB，R SB，各自独立地表示1-4C全氟烷基。版权所有（C）2010，JPO＆INPIT

7. 发明专利

JP2009242270A Method for producing 4-perfluoroisopropylaniline 有权
标题翻译：生产4-氟氟草胺的方法
公开(公告)号：JP2009242270A
公开(公告)日：2009-10-22
申请号：JP2008089056
申请日：2008-03-31
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： SASAKI SHINTARO , KUME KOJI
IPC分类号： C07C209/74 , C07C211/52
CPC分类号： C07C209/68 , C07C211/52
摘要： PROBLEM TO BE SOLVED: To provide a method for highly selectively and efficiently producing a 4-perfluoroisopropylaniline from an inexpensive raw material. SOLUTION: Aminoaryl-containing fluoroalcohol is reacted with sulfuryl fluoride (SO 2 F 2 ) in the coexistence of an organic base or "a salt or complex comprising an organic base and hydrogen fluoride" in the presence of an organic solvent. A nitrile is particularly desirable as the organic solvent, and a tertiary amine is particularly desirable as the organic base. It is possible to produce the objective product of the formula while markedly suppressing the formation of by-producs. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供从廉价原料高度选择性和有效地制备4-全氟异丙基苯胺的方法。解决方案：将含氨基芳基的氟代醇与硫酰氟（SO 2 SB 2 F SB 2）在有机碱或“包含有机基团的盐或络合物”共同存在下反应碱和氟化氢“在有机溶剂的存在下进行。作为有机溶剂，腈是特别理想的，特别优选叔胺作为有机碱。可以生产下式的目标产物，同时显着抑制副产物的形成。版权所有（C）2010，JPO＆INPIT

8. 发明专利

JP2004002337A Method for producing methyltrifluoromethylbenzoic acid 有权
公开(公告)号：JP2004002337A
公开(公告)日：2004-01-08
申请号：JP2003079658
申请日：2003-03-24
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： NARIZUKA SATOSHI , KUME KOJI
IPC分类号： C07C51/02 , C07B61/00 , C07C51/04 , C07C51/347 , C07C63/70
摘要： PROBLEM TO BE SOLVED: To efficiently synthesize methyltrifluoromethylbenzoic acids useful as a medicinal/agrochemical intermediate by using an industrially easily available derivative of bis(trifluoromethyl)benzoic acid or a salt of the bis(trifluoromethyl)benzoic acid as a starting raw material. SOLUTION: The derivative of the bis(trifluoromethyl)benzoic acid or the salt of the bis(trifluoromethyl)benzoic acid is reacted with hydrogen gas in the presence of a base and a transition metal catalyst. The reaction rate of the reaction is extremely increased in a mixed solvent comprising water and a water-soluble organic solvent. When the amount of the water and the water-soluble organic solvent is not less than a specific amount, the effects are especially remarkable. COPYRIGHT: (C)2004,JPO

9. 发明专利

JP2002371028A Method for producing 3,3,3-trifluoro-2-hydroxypropionic acid derivative 有权
标题翻译： 3,3,3-三氟-2-羟基丙酸衍生物的制备方法
公开(公告)号：JP2002371028A
公开(公告)日：2002-12-26
申请号：JP2001180412
申请日：2001-06-14
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： ISHII AKIHISA , KANAI MASATOMI , YASUMOTO MANABU , KURIYAMA KATSU , HAYAMIZU TAKASHI , KUME KOJI , IMURA HIDEAKI
IPC分类号： C07C51/093 , C07B61/00 , C07C51/347 , C07C59/01 , C07C59/125
摘要： PROBLEM TO BE SOLVED: To provide a producing method capable of efficiently obtaining a 3,3,3-trifluoro-2-hydroxypropionic acid derivative which is an important intermediate for medicines and agrochemicals.
SOLUTION: 1,1,1-Trichloro-3,3,3-trifluoro-2-propanol derivative is reacted with a base in methanol to produce a 3,3,3-trifluoro-2-methoxypropionic acid derivative, which is further demethylated to efficiently produce a 3,3,3- trifluoro-2-hydroxypropionic acid derivative.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供能够有效地获得作为药物和农药的重要中间体的3,3,3-三氟-2-羟基丙酸衍生物的制备方法。溶液：将1,1,1-三氯-3,3,3-三氟-2-丙醇衍生物与甲醇中的碱反应生成3,3,3-三氟-2-甲氧基丙酸衍生物，进一步脱甲基化以有效地制备3,3,3-三氟-2-羟基丙酸衍生物。

10. 发明专利

JP2010053124A Method for producing perfluoroalkane sulfinate 有权
标题翻译：生产全氟烷烃磺酸盐的方法
公开(公告)号：JP2010053124A
公开(公告)日：2010-03-11
申请号：JP2009174338
申请日：2009-07-27
申请人： Central Glass Co Ltd , セントラル硝子株式会社
发明人： MINAMIMEI TSUTOMU , KASHIBA TAKASHI , MORINAKA TAKAYOSHI , KAWAMOTO HIROMI , INOUE SUSUMU , KUME KOJI
IPC分类号： C07C313/04
CPC分类号： C07C313/04 , Y02P20/582
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a perfluoroalkane sulfinate useful as an intermediate of medicines and pesticide precursors. SOLUTION: A perfluoroalkane sulfonyl halide is reacted with hydrazine to prepare a hydrazine salt of the perfluoroalkane sulfinic acid (RfSO 2 H N 2 H 4 ). The resultant hydrazine salt is reacted with a base such as a hydroxide of an alkali metal to prepare the perfluoroalkane sulfinate. The resultant sulfinate is reacted with a fluoride of an alkali metal or the like, to crystallize the sulfinate. The resultant sulfinate is added with a halide of an alkali metal or the like to prepare the perfluoroalkane sulfinate of high purity. The production method is very useful because it can produce the perfluoroalkane sulfinate safer and easier on a commercial scale, as compared with conventional technologies, and the method greatly reduce waste products. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供可用作药物和农药前体的中间体的用于制备用于制备全氟烷基亚磺酸盐的方法。解决方案：将全氟烷基磺酰卤与肼反应以制备全氟烷烃亚磺酸的肼盐（RfSO 2 SBH 2 H SB 3 >）。所得的肼盐与碱如碱金属的氢氧化物反应以制备亚烷基全氟烷烃。所得的亚磺酸盐与碱金属等的氟化物反应，使亚磺酸盐结晶。所得的亚磺酸盐加入碱金属的卤化物等以制备高纯度的全氟烷基亚磺酸盐。生产方法是非常有用的，因为与常规技术相比，它可以在商业规模上产生更全面，更容易的全氟烷基亚磺酸盐，并且该方法大大减少了废物。版权所有（C）2010，JPO＆INPIT

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