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    • 4. 发明专利
    • Hydrogen separation and recovery methods and hydrogen separation and recovery equipment
    • JP5344113B2
    • 2013-11-20
    • JP2007276564
    • 2007-10-24
    • 三菱マテリアル株式会社
    • 満敏 生川
    • C01B3/56C01B3/52C01B33/107
    • PROBLEM TO BE SOLVED: To provide a method and a facility for separation/collection of hydrogen, wherein hydrogen contained in a gas generated by a conversion reaction is efficiently separated and collected to be reused by being connected to a conversion facility for producing trichlorosilane. SOLUTION: The hydrogen separation/collection method comprises: [an absorption step] of bringing a mixed gas containing chlorosilanes, hydrogen chloride and hydrogen into contact with an absorption solution consisting mainly of liquid chlorosilanes to absorb the chlorosilanes and hydrogen chloride in the mixed gas into the absorption solution; [a hydrogen chloride separation step] of distillating the absorption solution which has absorbed the chlorosilanes and hydrogen chloride to gasify hydrogen chloride and separating the gasified hydrogen chloride; [an absorption solution circulating step] of collecting the chlorosilanes separated from hydrogen chloride, cooling the collected chlorosilanes, and returning the cooled chlorosilanes to the absorption step; and [a hydrogen purification step] of passing a gas which has passed through the absorption solution and is mainly composed of hydrogen through active carbon to adsorb the chlorosilanes and hydrogen chloride remaining in the gas onto the active carbon, thereby separating hydrogen from the chlorosilanes and hydrogen chloride. The facility for the method is also provided. COPYRIGHT: (C)2008,JPO&INPIT