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1. 发明专利

JP2006142628A Method for producing polybenzimidazol molding and mold 审中-公开
标题翻译：生产聚苯二甲酸乙二醇酯和模具的方法
公开(公告)号：JP2006142628A
公开(公告)日：2006-06-08
申请号：JP2004335232
申请日：2004-11-19
申请人： Tokai Denka Kogyo Kk , 東海電化工業株式会社
发明人： IKEBE JUICHI , ARAKI MASAO
IPC分类号： B29C43/34 , B29C43/02 , B29C43/14 , B29C43/36 , B29C43/52 , B29C67/04 , B29K79/00
摘要： PROBLEM TO BE SOLVED: To produce a PBI molding which is as excellent as unpretreated PBI powder in moldability and has stable quality.
SOLUTION: A method for producing a polybenzimidazole molding comprises a packing process in which the PBI powder after being neutralized and washed is dried under reduced pressure while being vibrated, and the dried powder is charged into the cavity of a mold heated in advance at room temperature or above, a preheating process in which a primary pressure is applied to the mold to reduce the volume of the packed powder, and the powder is heated at 100°C or above and below the secondary transition point of the resin, a heating process in which the temperature of the powder is kept, a secondary pressure equal to or greater than the primary pressure is applied for a prescribed time, and the powder is heated at the secondary transition point of the PBI resin or above under the primary pressure, a heating pressurization process in which a ternary pressure is applied for a prescribed time while the temperature of the heating process is kept, and a temperature and pressure decreasing process in which the temperature of the cavity of the mold is decreased continuously, and the ternary pressure is decreased stepwise after the temperature decrease is started.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：制造与未经处理的PBI粉末一样优异的PBI模塑成型性，并且质量稳定。解决方案：聚苯并咪唑成型体的制造方法包括将中和洗涤后的PBI粉末振动干燥的包装方法，将干燥的粉末装入预先加热的模具的空腔内在室温以上的情况下，对模具施加一次压力以减小填充粉末的体积的预热过程，并且将粉末在树脂的二次转变点的100℃以上加热，在其中保持粉末温度的加热过程，等于或大于初级压力的二次压力施加规定时间，并且在主要压力下在PBI树脂或以上的二次转变点加热粉末，加热加压过程，其中在保持加热过程的温度的同时施加三次压力达规定时间，并且温度和压力降低程序 ss，其中模具的空腔的温度连续降低，并且在开始温度降低之后三元压力逐步降低。版权所有（C）2006，JPO＆NCIPI

2. 发明专利

JP2984940B2 失效
公开(公告)号：JP2984940B2
公开(公告)日：1999-11-29
申请号：JP26641990
申请日：1990-10-05
申请人： TOKAI DENKA KOGYO KK
发明人： SUGIMURA TOSHIO , WATANABE SATORU , SANO JUJIRO , YAMAMOTO SHINJI
IPC分类号： C07C381/14

3. 发明专利

JP2858254B2 失效
公开(公告)号：JP2858254B2
公开(公告)日：1999-02-17
申请号：JP16264789
申请日：1989-06-27
申请人： TOKAI DENKA KOGYO KK
发明人： SATO KANJI , KONDO TOMOMASA
IPC分类号： C01B15/10 , C11D3/39

4. 发明专利

JPS5735559A Preparation of dihydroxydiphenylsulfone 失效
标题翻译：二氢二硅氧烷的制备
公开(公告)号：JPS5735559A
公开(公告)日：1982-02-26
申请号：JP11039380
申请日：1980-08-13
申请人： Tokai Denka Kogyo Kk
发明人： OOURA OSAMI , SHIMIZU YASUO , FUKAZAWA TSUNEO , KITAMURA KOUJI
IPC分类号： C07B61/00 , B01J21/00 , B01J21/02 , B01J21/10 , B01J23/00 , B01J23/06 , B01J23/74 , B01J27/00 , B01J27/04 , B01J27/08 , B01J27/16 , C07C67/00 , C07C313/00 , C07C315/00 , C07C317/22
CPC分类号： Y02P20/52
摘要： PURPOSE: To obtain a compound useful as a substitute for bisphenol A in a short time in high yield, by reacting phenol with a sulfonating agent in the presence of a compound selected from Zn compound, Fe compound and Mg compound.
CONSTITUTION: Phenol is reacted with a sulfonating agent (e.g., conc. sulfuric acid, fuming sulfuric acid, sulfuric anhydride, etc.) or phenolsulfonic acid, to give dihydroxydiphenylsulfone. In the reaction, at least one compound selected from the group consisting of zinc compound, iron compound, magnesium compound, boron compound, and phosphorus compound (e.g., halide, sulfide, oxide, hydroxide, etc. of Zn) as a catalyst is added to the reaction system. A condensation reaction through dehydration is not preceded substantially when the reaction temperature is below 140°C, and side reactions occur actively when the reaction temperature is ≥250°C. The use of the catalyst reduces the content of by-products and precedes the condensation reaction through dehydration.
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：目的：在选自Zn化合物，Fe化合物和Mg化合物的化合物的存在下，通过苯酚与磺化剂反应获得可用于短时间高收率的双酚A的替代物。构成：使苯酚与磺化剂（例如浓硫酸，发烟硫酸，硫酸酐等）或苯酚磺酸反应，得到二羟基二苯砜。在反应中，添加选自锌化合物，铁化合物，镁化合物，硼化合物和磷化合物（例如Zn的卤化物，硫化物，氧化物，氢氧化物等）中的至少一种化合物作为催化剂到反应体系。当反应温度低于140℃时，通过脱水的缩合反应基本上不存在，当反应温度> 250℃时副反应主要发生。催化剂的使用降低了副产物的含量，并在缩合反应之前脱水。

5. 发明专利

JP2860798B2 失效
公开(公告)号：JP2860798B2
公开(公告)日：1999-02-24
申请号：JP16264889
申请日：1989-06-27
申请人： TOKAI DENKA KOGYO KK
发明人： SATO KANJI , KONDO TOMOMASA
IPC分类号： C01B15/10 , C11D3/39

6. 发明专利

JP2808489B2 失效
公开(公告)号：JP2808489B2
公开(公告)日：1998-10-08
申请号：JP32543290
申请日：1990-11-29
申请人： TOKAI DENKA KOGYO KK
发明人： SUZUKI MORIO , OORA OSAMI , NITO HIROHISA
IPC分类号： G03C1/09 , C07C381/14

7. 发明专利

JPS5777667A Separating method of 4,4'-dihydroxydiphenyl sulfone from isomeric mixture of dihydroxydiphenyl sulfone 失效
标题翻译： 4,4'-二羟基二苯基硫醚从二羟基二苯甲酮异构体混合物中分离的方法
公开(公告)号：JPS5777667A
公开(公告)日：1982-05-15
申请号：JP15222880
申请日：1980-10-31
申请人： Tokai Denka Kogyo Kk
发明人： OOURA OSAMI , SHIMIZU YASUMASA , KITAMURA KOUJI
IPC分类号： C07C67/00 , C07C313/00 , C07C315/06 , C07C317/22
CPC分类号： C07C315/06 , C07C317/22
摘要： PURPOSE: To separate 4,4'-dihydroxydiphenyl sulfone useful as a raw material for a synthetic resin in high purity by an easy operation, by treating an isomeric mixture of dihydroxydiphenyl sulfones inexpensive phenol.
CONSTITUTION: An isomeric mixture of 4,4'-dihydroxydiphenyl sulfone with 2,4'- dihydroxydiphenyl sulfone is wholly dissolved in phenol, and the resultant solution is then cooled to crystallize only the 4,4'-dihydroxydiphenyl sulfone as its adduct with the phenol, which is then separated by the filtration, etc. The resultant adduct directly or in an aqueous solution is heat-treated to give the aimed 4,4'-dihydroxydiphenyl sulfone of high purity easily. The phenol used for the separation is directly usable as a reaction raw material for the dihydroxydiphenyl sulfone.
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：目的：通过简单的操作分离出高纯度合成树脂原料的4,4'-二羟基二苯砜，通过处理二羟基二苯砜的异构体混合物便宜的苯酚。构成：将4,4'-二羟基二苯基砜与2,4'-二羟基二苯基砜的异构体混合物全部溶解在苯酚中，然后将所得溶液冷却，仅结晶出4,4'-二羟基二苯砜与其加合物苯酚，然后通过过滤分离等。所得加合物直接或在水溶液中进行热处理，得到高纯度的目标4,4'-二羟基二苯基砜。用于分离的苯酚可直接用作二羟基二苯砜的反应原料。

8. 发明专利

JP2909743B2 失效
公开(公告)号：JP2909743B2
公开(公告)日：1999-06-23
申请号：JP5380089
申请日：1989-03-08
申请人： TOYAMA NIPPON DENKI KK , TOKAI DENKA KOGYO KK
发明人： KIMURA TOSHA , OONUKI HIDEFUMI , WAKASHIMA KOICHI , NAKAJIMA SHIGEKI , ITANI KATSUTOSHI , HIRAI AKIRA
IPC分类号： C23F1/18 , C23F3/06 , C23G1/10 , H05K3/26 , H05K3/28

9. 发明专利

JP2893537B2 失效
公开(公告)号：JP2893537B2
公开(公告)日：1999-05-24
申请号：JP18587289
申请日：1989-07-20
申请人： TOKAI DENKA KOGYO KK , TSUJI KUNIO
发明人： TSUJI KUNIO , NUKAYA HARUO , KANETANI YASUHIRO
IPC分类号： C01B15/037 , C07D233/54 , C07D233/64 , D21C9/16

10. 发明专利

JP2779635B2 失效
公开(公告)号：JP2779635B2
公开(公告)日：1998-07-23
申请号：JP2090589
申请日：1989-02-01
申请人： TOKAI DENKA KOGYO KK
发明人： ENOMOTO SABURO , INOE MASAMI , KAMYAMA TSUTOMU , OORA OSAMI , NITO HIROHISA
IPC分类号： C07D301/12 , B01J31/34 , C07B61/00 , C07D303/04

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