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31. 发明专利

JP2014196215A 改質金属酸化物微粒子粉末およびその製造方法审中-公开
标题翻译：改性金属氧化物颗粒状粉末及其制造方法
公开(公告)号：JP2014196215A
公开(公告)日：2014-10-16
申请号：JP2013072919
申请日：2013-03-29
申请人：日揮触媒化成株式会社 , Jgc Catalysts & Chemicals Ltd
发明人： YAMAGUCHI JUN , MATSUDA MASAYUKI , MURAGUCHI MAKOTO
IPC分类号： C01B13/14 , C01B33/149 , C01G23/053 , C01G25/02 , C01G30/00
摘要：【課題】分散性、流動性および経済性にも優れた改質金属酸化物微粒子粉末の製造方法を提供する。【解決手段】(a)金属酸化物微粒子の水および/または有機溶媒分散液を調製したのち、(b)該分散液に、Rp-MXq-pで表される有機金属化合物を添加し、次いで、(d)分散液を噴霧乾燥することを特徴とする、粉末の平均粒子径(DMP)が1〜200μmの範囲にあり、一次粒子および二次粒子の集合体から構成されてなり、二次粒子のレーザー法で測定した平均二次粒子径(DM2)が5〜500nmの範囲にあり、一次粒子のTEM法で観察して測定した平均一次粒子径(DM1)が5〜500nmの範囲にあり、平均二次粒子径(DM2)と平均一次粒子径(DM1)との比(DM2)/(DM1)が1〜10の範囲にあり、安息角が40?以下である、改質金属酸化物微粒子粉末の製造方法。【選択図】なし
摘要翻译：要解决的问题：提供一种生产分散性，流动性和经济效率优异的改性金属氧化物颗粒粉末的方法。提供一种制备改性金属氧化物颗粒粉末的方法，所述改性金属氧化物颗粒粉末的平均粒径（D）在 1〜200μm的范围，其由初级粒子和二次粒子的聚集体构成，其通过激光法测定的二次粒子的平均二次粒径（D）在5〜500nm的范围内，平均一次粒子通过TEM法观察的一次粒子的直径（D）在5〜500nm的范围内，平均二次粒径（D）与平均一次粒径（D）的比（D）/（D）在1〜10的范围内，休止角为40°以下。制备改性金属氧化物颗粒粉末的方法包括：（a）在水和/或有机溶剂中制备金属氧化物颗粒的流体分散体，然后（b）将由R-MX表示的有机金属化合物加入到流体分散体中; 然后（d）雾化和干燥流体分散体。

32. 发明专利

JP2014124913A Water-repellent transparent coating film-fitted substrate and method for manufacturing the same 有权
标题翻译：透明透明涂料薄膜基材及其制造方法
公开(公告)号：JP2014124913A
公开(公告)日：2014-07-07
申请号：JP2012285398
申请日：2012-12-27
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , MURAGUCHI MAKOTO , EGAMI KAZUTAKA , KOYANAGI TSUGUO
IPC分类号： B32B9/00 , B05D5/00 , B05D5/06 , B32B3/30 , C03C17/34 , C09D1/00 , C09D5/00 , C09K3/18
CPC分类号： C09K3/18 , B05D7/50 , B32B3/30 , B32B9/00 , B32B2307/412 , B32B2307/73 , B32B2605/00 , C03C17/3411 , C03C2217/42 , C03C2217/76 , Y10T428/24364
摘要： PROBLEM TO BE SOLVED: To provide a water-repellent transparent coating film having a high water repellency as well as improved adhesiveness to a substrate, abrasion resistance, scratch resistance, etc.SOLUTION: The provided water-repellent transparent coating film-fitted substrate comprises: a substrate; and a water-repellent transparent coating film formed on the surface of the substrate. The water-repellent transparent coating film consists of an inorganic oxide particulate layer including inorganic oxide particulates and an overcoat layer formed atop the inorganic oxide particulate layer. The water-repellent transparent coating film surface has an uneven structure. The average height (T) of peak portions thereof is confined to a range of 30-500 nm, The average distance between peak portions (pitch width) (W) is confined to a range of 50-1000 nm. The contact angle thereof with water is confined to a range of 130-180°. The ratio of the average height (T) with respect to the average distance between peak portions (W), namely (T)/( W), is confined to a range of 0.1-10. Surfaces of peak portions of the uneven structure further possesses fine valleys and peaks. The average height of the fine peak portions (T) is confined to a range of 3-50 nm. The average distance between these peak portions (W) is less than the average inter-peak distance of the former peak portions (W) and is confined to a range of 3-50 nm.
摘要翻译：要解决的问题：提供具有高斥水性以及改善与基材的粘合性，耐磨性，耐划伤性等的拒水透明涂膜。溶液：所提供的防水透明涂膜敷设基材包括：底物以及形成在基板的表面上的防水透明涂膜。防水透明涂膜由无机氧化物颗粒层组成，无机氧化物颗粒层和无机氧化物颗粒层顶上形成的外涂层。防水透明涂膜表面具有不均匀的结构。其峰部的平均高度（T）限制在30〜500nm的范围。峰部（间距宽度）（W）之间的平均距离被限制在50〜1000nm的范围。其与水的接触角限制在130-180°的范围内。平均高度（T）相对于峰值部分之间的平均距离（W）的比例即（T）/（W））限制在0.1-10的范围内。不平坦结构的峰部的表面还具有细小的谷和峰。微细峰部（T）的平均高度被限制在3-50nm的范围。这些峰值部分（W）之间的平均距离小于前一个峰部分（W）的平均峰间距离，并被限制在3-50nm的范围内。

33. 发明专利

JP2014094865A Method of producing silica particle having internal cavity, silica particle having internal cavity and coating liquid for film formation and film-provided substrate containing the silica particle 有权
标题翻译：生产具有内部孔隙的二氧化硅颗粒的方法，具有内部孔的二氧化硅颗粒和用于膜形成的涂层液体和包含二氧化硅颗粒的膜式底物
公开(公告)号：JP2014094865A
公开(公告)日：2014-05-22
申请号：JP2012247969
申请日：2012-11-12
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： FUTAGAMI WATARU , EGAMI KAZUTAKA , MURAGUCHI MAKOTO , KOYANAGI TSUGUO
IPC分类号： C01B33/18 , C09D7/12 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a silica particle which is useful as e.g. a low-refractive-index material, a low-dielectric-constant material, a heat insulation material, an adsorbent, a separation material and a sustained release material and has a cavity inside a polygonal shape having a relatively large particle size and its production method.SOLUTION: A method of producing a silica particle having an internal cavity includes: a step (a) of adding an aqueous solution of a silicate and/or an acidic silicate solution and an aqueous solution of an alkali-soluble inorganic compound other than silica simultaneously to a zeolite particle fluid dispersion in such a manner as to form a complex oxide (hydrate) layer of silica and the inorganic compound on the surface of the zeolite particles having a weight ratio (W)/(W) of the amount (W), by solid contents, of zeolite particles and the amount (W), by solid contents, of the complex oxide (hydrate) layer formed on the surface of the zeolite particles in a range of 0.1 to 5.0 in order to prepare a zeolite-complex oxide particle fluid dispersion; and a step (b) of adding an acid to the zeolite-complex oxide particle fluid dispersion to remove at least a part of the elements constituting the zeolite-complex oxide particles other than silicon.
摘要翻译：要解决的问题：提供可用于例如二氧化硅的二氧化硅颗粒。低折射率材料，低介电常数材料，绝热材料，吸附剂，分离材料和缓释材料，并且具有粒径较大的多边形内的空腔及其制造方法溶液：制备具有内腔的二氧化硅颗粒的方法包括：添加硅酸盐和/或酸性硅酸盐溶液的水溶液和除二氧化硅以外的碱溶性无机化合物的水溶液的步骤（a）同时以沸石颗粒流体分散体的形式，以在二氧化硅和无机化合物的表面上形成重量比（W）/（W）为（W）的沸石颗粒的复合氧化物（水合物）层），沸石粒子的固体成分和形成在沸石粒子的表面上的复合氧化物（水合物）层的含量（W）的固体成分的含量（W）在0.1〜5.0的范围内，复杂的牛颗粒流体分散体; 和向沸石 - 复合氧化物颗粒流体分散体中加入酸以除去构成除了硅以外的沸石复合氧化物颗粒的至少一部分的步骤（b）。

34. 发明专利

JP2014086526A Light-emitting diode 审中-公开
标题翻译：发光二极管
公开(公告)号：JP2014086526A
公开(公告)日：2014-05-12
申请号：JP2012233590
申请日：2012-10-23
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： YAMAGUCHI JUN , MATSUDA MASAYUKI , MURAGUCHI MAKOTO
IPC分类号： H01L33/56 , H01L23/29 , H01L23/31
CPC分类号： H01L2224/48091 , H01L2224/8592 , H01L2924/00014
摘要： PROBLEM TO BE SOLVED: To provide a light-emitting diode excellent in sealing performance, heat resistance, light extraction efficiency, emission luminance, and the like.SOLUTION: The light-emitting diode including a die bond, a light-emitting element, and a sealing layer is characterized in that: the sealing layer comprises an organic resin and zirconia fine particles surface-treated with an organosilicon compound; the surface-treated zirconia fine particles have an average secondary particle diameter (D) in the range of 5-50 nm and an average primary particle diameter (D) in the range of 5-50 nm; and the ratio (D)/(D) of the average secondary particle diameter (D) to the average primary particle diameter (D) is in the range of 1-10.
摘要翻译：要解决的问题：提供密封性能，耐热性，光提取效率，发光亮度等优异的发光二极管。解决方案：包括管芯接合，发光元件和发光元件的发光二极管密封层的特征在于：密封层包括有机树脂和用有机硅化合物表面处理的氧化锆微粒; 表面处理的氧化锆微粒的平均二次粒径（D）在5-50nm的范围内，平均一次粒径（D）在5-50nm的范围内; 平均二次粒径（D）与平均一次粒径（D）的比（D）/（D）在1-10的范围内。

35. 发明专利

JP2013136222A Substrate with hard coat film and coating liquid for forming hard coat film 有权
标题翻译：具有硬涂层薄膜和涂层液的基材，用于形成硬涂膜
公开(公告)号：JP2013136222A
公开(公告)日：2013-07-11
申请号：JP2011289346
申请日：2011-12-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , HAKOJIMA YUKO , MATSUDA MASAYUKI
IPC分类号： B32B3/26 , C09C1/30 , C09C1/36 , C09C1/40 , C09C3/08 , C09D4/02 , C09D5/00 , C09D7/12 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a substrate with a hard coat film having superior anti-blocking properties (hard coat films does not adhere each to other).SOLUTION: A substrate with a hard coat film comprises the substrate and the hard coat film formed on the substrate. The hard coat film comprises (i) metal oxide particle (A) processed with surfactant and (ii) hydrophobic matrix component, the average particle size (D) of the metal oxide particle (A) is in the range of 30 to 150 nm, the metal oxide particle (A) is unevenly distributed on the upper part of the hard coat film to form protrusions, the height (H convex) of the protrusion is in the range of 10 to 200 nm.
摘要翻译：要解决的问题：为基材提供具有优异的防粘连性的硬涂膜（硬涂膜不粘附到其它）。溶液：具有硬涂层的基材包括基材和形成的硬涂膜在基板上。硬涂膜包含（i）用表面活性剂处理的金属氧化物颗粒（A）和（ii）疏水基质组分，金属氧化物颗粒（A）的平均粒径（D）在30至150nm的范围内，金属氧化物粒子（A）不均匀地分布在硬涂膜的上部，形成突起，凸部的高度（H凸）在10〜200nm的范围内。

36. 发明专利

JP2013082609A Modified zirconia fine-particle powder, dispersion sol of modified zirconia fine-particle, and method for manufacturing the same powder and dispersion sol 有权
标题翻译：改性的ZIRCONIA微粒粉末，改性ZIRCONIA微粒的分散溶液及其制造相同粉末和分散溶胶的方法
公开(公告)号：JP2013082609A
公开(公告)日：2013-05-09
申请号：JP2012216202
申请日：2012-09-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： YAMAGUCHI JUN , MATSUDA MASAYUKI , MURAGUCHI MAKOTO
IPC分类号： C01G25/02 , C09C1/00 , C09C3/12
摘要： PROBLEM TO BE SOLVED: To provide a modified zirconia fine-particle powder excellent in dispersibility and flowability.SOLUTION: The modified zirconia fine-particle powder is a powder of modified zirconia fine-particles that is surface-treated with an organosilicon compound, has a mean secondary particle diameter in the range of 5-500 nm, has a mean primary particle diameter in the range of 5-500 nm, and the ratio of the mean secondary particle diameter/the mean primary particle diameter is in the range of 1-10. The organosilicon compound, which is represented by formula (1) below, is contained in the fine-particles within the range of 1-50 wt.% as R-SiO(n is an integer of 1-3), and has a half width of the main peak in 29Si MAS NMR spectrum within the range of 3-15 ppm. Formula (1) is represented by R-SiX, wherein R is 1-10C unsubstituted or substituted hydrocarbon groups, each of which may be the same as or different from each other; X is a 1-4C alkoxy group, a hydroxy group, a halogen, or hydrogen; and n is an integer of 1-3.
摘要翻译：要解决的问题：提供分散性和流动性优异的改性氧化锆微粒粉末。解决方案：改性氧化锆微粒粉末是用有机硅化合物表面处理的改性氧化锆微粒的粉末，平均二次粒径在5-500nm的范围内，具有平均初级粒径在5-500nm的范围内，平均二次粒径/平均一次粒径的比在1-10的范围内。由下式（1）表示的有机硅化合物以1-50重量％的范围包含在R -SiO （4-n）/ 2 （n为1-3的整数），并且在29Si MAS NMR光谱中的主峰的半宽度在3-15ppm的范围内。式（1）表示为R 4-n ，其中R为1-10C未取代或取代的烃基各自可以彼此相同或不同; X是1-4C烷氧基，羟基，卤素或氢; n为1-3的整数。版权所有（C）2013，JPO＆INPIT

37. 发明专利

JP2011093754A Antimony pentoxide based complex oxide fine particle, coating liquid for forming transparency coating film containing the fine particle, and base material with transparency coating film 审中-公开
标题翻译：抗氧化剂为基础的复合氧化物微粒，用于形成含有微粒的透明涂层膜的涂布液和具有透明涂层膜的基材
公开(公告)号：JP2011093754A
公开(公告)日：2011-05-12
申请号：JP2009250637
申请日：2009-10-30
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , MIYAMOTO TAKUJI , MURAGUCHI MAKOTO
IPC分类号： C01G30/00 , C09D7/12 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide an antimony pentoxide based complex oxide fine particle which can form a transparency coating film in which there is no interference fringe, which excels in transparency and an antistatic characteristic, and which excels in adhesion with a base material, scratch resistance, scratch strength, pencil hardness or the like.
SOLUTION: The antimony pentoxide based complex oxide fine particle includes: an antimony pentoxide fine particle whose average particle size is in the range of 5-50 nm; and a titanium oxide and/or zirconium oxide layer which has covered the surface of the fine particle. The antimony pentoxide based compound oxide fine particle includes: a chain-like antimony pentoxide fine particle in which an antimony pentoxide fine particle whose average particle size is in the range 5-50 nm connects in the shape of a chain, and an average connectivity number is in the range of 2-30; and a titanium oxide and/or zirconium oxide layer which has covered the surface of the fine particle. The antimony pentoxide fine particle contains a phosphorus oxide in the range of 0.1-15 wt.% as P
2 O
5 .
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种能够形成透明性涂膜的五氧化二锑基复合氧化物细颗粒，其中不存在干涉条纹，其透明性和抗静电特性都优异，并且与基材的粘合性优异材料，耐擦伤性，划痕强度，铅笔硬度等。解决方案：五氧化二锑基复合氧化物微粒包括：平均粒径在5-50nm范围内的五氧化二锑细颗粒; 以及已经覆盖微粒表面的氧化钛和/或氧化锆层。五氧化二锑复合氧化物微粒包括：其平均粒径为5-50nm的五氧化二锑细颗粒以链的形状连接的链状五氧化二锑细颗粒和平均连接数在2-30范围内; 以及已经覆盖微粒表面的氧化钛和/或氧化锆层。五氧化二锑微粒含有氧化磷，为P 2 5 的0.1〜15重量％。版权所有（C）2011，JPO＆INPIT

38. 发明专利

JP2011068087A Substrate with hard coat film and coating liquid for forming hard coat film 有权
标题翻译：具有硬涂层薄膜和涂层液的基材，用于形成硬涂膜
公开(公告)号：JP2011068087A
公开(公告)日：2011-04-07
申请号：JP2009222872
申请日：2009-09-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , MATSUDA MASAYUKI , FUTAGAMI WATARU , HIRAI TOSHIHARU
IPC分类号： B32B27/20 , C09D4/02 , C09D7/12 , C09D175/16 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a substrate with a hard coat film excellent in anti-blocking property and to provide a coating liquid used for forming the hard coat film.
SOLUTION: The substrate with hard coat film includes the substrate and the hard coat film which is formed on the substrate and comprises hydrophilic metal oxide particles and a hydrophobic matrix spherical component, wherein at least a part of the metal oxide particles exist so as to form protrusion parts on the surface of the hard coat film and heights (H protrusion) of the protrusion parts are in the range of 50 nm to 1 μm. The spherical coefficient presented by equation (1): spherical coefficient=(D
S )/(D
L ) of the metal oxide particles is 0.5 or more (wherein (D
L ) is the average particle longest diameter and (D
S ) is the average short diameter vertical to the longest diameter on the middle point of the longest diameter).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供具有优异的防粘连性能的硬涂膜的基材，并提供用于形成硬涂膜的涂布液。解决方案：具有硬涂膜的基材包括基材和形成在基材上的硬涂层，其包含亲水性金属氧化物颗粒和疏水性基质球形组分，其中至少一部分金属氧化物颗粒存在于为了在硬涂膜的表面上形成突起部分，突出部分的高度（H突起）在50nm至1μm的范围内。式（1）给出的球状系数：金属氧化物粒子的球面系数=（D S ）/（D L ）为0.5以上（其中（D < SB> L ）是平均颗粒最长直径，（D S ）是垂直于最长直径中点最长直径的平均短径）。版权所有（C）2011，JPO＆INPIT

39. 发明专利

JP2011063478A Phosphorus-containing antimony pentoxide microparticle, coating liquid for forming transparent conductive film containing the microparticle, and base material with transparent conductive film 有权
标题翻译：含有PHOSPHORUS的抗氧化剂微生物，用于形成含有微量元素的透明导电膜的涂布液和具有透明导电膜的基材
公开(公告)号：JP2011063478A
公开(公告)日：2011-03-31
申请号：JP2009215538
申请日：2009-09-17
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , ABE YONEJI , MURAGUCHI MAKOTO
IPC分类号： C01G30/00 , B05D5/12 , C09D5/24 , C09D7/12 , C09D201/00 , H01B1/20 , H01B5/00 , H01B5/14
摘要： PROBLEM TO BE SOLVED: To provide an antimony pentoxide microparticle exhibiting conductivity and no coloring and discoloring.
SOLUTION: The phosphorus-containing antimony pentoxide microparticle contains a phosphorus oxide in the range of 0.1 to 15 wt.% in terms of P
2 O
5 . The average particle diameter of the antimony pentoxide microparticle is in the range of 5 to 50 nm. The phosphorus oxide is carried on the antimony pentoxide microparticle. The antimony pentoxide microparticles are linked in a chain form, and the average linking number is in the range of 2 to 30. The phosphorus-containing antimony pentoxide microparticle of claim 4 claims that the volume resistance of the antimony pentoxide microparticle is in the range of 1 to 10
3 Ω cm. After the phosphorus compound is added to an antimony pentoxide microparticle dispersion liquid, the mixture is subjected to a drying and heating treatment at 80 to 250°C for 0.5 to 12 hours to obtain the phosphorus-containing antimony pentoxide microparticle.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供显示导电性且不着色和变色的五氧化二锑微粒。解决方案：含磷的五氧化二锑微粒含有以P 2 5 计为0.1〜15重量％的氧化磷。五氧化二锑微粒的平均粒径在5〜50nm的范围内。氧化磷载体在五氧化二锑微粒上。五氧化二锑微粒以链状形式连接，平均连接数在2〜30的范围内。权利要求4的含磷五氧化二锑微粒，其特征在于，所述五氧化二锑微粒的体积电阻为 1至10 3 Ωcm。在将磷化合物加入到五氧化二锑微粒分散液中之后，将混合物在80-250℃下干燥和加热处理0.5-12小时，得到含磷的五氧化二锑微粒。版权所有（C）2011，JPO＆INPIT

40. 发明专利

JP2010168268A Micro ring-like inorganic oxide particle having through-hole, base material with transparent coating film using the same and coating liquid for forming transparent coating film 有权
标题翻译：具有通孔的微环氧化物颗粒，具有透明涂层膜的基材和使用其的涂层液形成透明涂层膜
公开(公告)号：JP2010168268A
公开(公告)日：2010-08-05
申请号：JP2009228070
申请日：2009-09-30
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , MATSUDA MASAYUKI , MIYAMOTO TAKUJI , HIRAI TOSHIHARU , KOMATSU MICHIO
IPC分类号： C01B33/18 , C09C1/28 , C09C3/12 , C09D7/12 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide new micro ring-like inorganic oxide particles each having a through-hole.
SOLUTION: The micro ring-like inorganic oxide particles are characterized in that the average outer diameter (D
O ) is in the range of 10 nm to 20 μm, the average diameter (D
I ) of through-holes is in the range of 1 nm to 12 μm and the ratio (W
R )/(D
O ) of the ring width (W
R ) to the average outer diameter (D
O ) is in the range of 0.2-0.45. The method for producing the micro ring-like inorganic oxide particles includes subjecting an inorganic oxide sol having an average particle diameter of 3-100 nm to spray drying and then treating the obtained particles with an acid or a base to form the through-hole. The method for producing the micro ring-like inorganic oxide particles includes using multiple oxide fine particles comprising silica and an inorganic oxide other than silica, then removing the inorganic oxide other than silica by using an acid, and treating the resulting particles with an acid or a base or subjecting the resulting particles to a hydrothermal treatment to form the through-hole.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供各自具有通孔的新的微环状无机氧化物颗粒。解决方案：微环状无机氧化物颗粒的特征在于，平均外径（D O ）在10nm至20μm的范围内，平均直径（D I ）在1nm至12μm的范围内，并且环的比（W R SB）/（D O ）宽度（W R ）与平均外径（D O SB）的比值在0.2-0.45的范围内。微环状无机氧化物粒子的制造方法包括使平均粒径为3〜100nm的无机氧化物溶胶进行喷雾干燥，然后用酸或碱处理得到的粒子，形成贯通孔。微环状无机氧化物粒子的制造方法包括使用包含二氧化硅和二氧化硅以外的无机氧化物的多种氧化物微粒，然后使用酸除去二氧化硅以外的无机氧化物，并用酸或碱或使得到的颗粒进行水热处理以形成通孔。版权所有（C）2010，JPO＆INPIT

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