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1. 发明专利

JP2014213591A 撥水性透明被膜付基材およびその製造方法有权
标题翻译：具有水透明涂层膜的基材及其制造方法
公开(公告)号：JP2014213591A
公开(公告)日：2014-11-17
申请号：JP2013095279
申请日：2013-04-30
申请人：日揮触媒化成株式会社 , Jgc Catalysts & Chemicals Ltd
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , MURAGUCHI MAKOTO , EGAMI KAZUTAKA , KOYANAGI TSUGUO
IPC分类号： B32B9/00 , B05D7/24 , C03C17/25 , C03C17/30
CPC分类号： B05D7/24 , B32B9/00 , C03C17/25 , C03C17/30
摘要：【課題】撥水性に優れるとともに透明性、ヘーズ、硬度、強度、耐擦傷性、耐摩耗性、密着性等に優れた撥水性透明被膜付基材を提供する。【解決手段】基材、および基材上に形成された撥水性透明被膜からなり、該撥水性透明被膜が、表面処理無機酸化物微粒子からなる無機酸化物微粒子層からなり、撥水性透明被膜表面が凹凸構造を有し、該凹凸の凸部の平均高さ(TF)が30〜500nmの範囲にあり、平均凸部間距離(ピッチ幅)(WF)が50〜1000nmの範囲にあり、水との接触角が130〜180?の範囲にあることを特徴とする撥水性透明被膜付基材。【選択図】なし
摘要翻译：要解决的问题：为了提供具有优异的防水性和优异的透明性，雾度，硬度，强度，耐擦伤性，耐磨性，粘附性等的防水透明涂膜的基材。溶液：提供了具有防水透明涂膜，其包含在基板上形成的基板和防水透明涂膜，其中所述防水透明涂膜由包含经表面处理的无机氧化物细颗粒的无机氧化物细颗粒层组成，防水透明涂膜表面具有不规则结构，不规则结构的突出部分的平均高度（T）在30至500nm的范围内，突出部分之间的平均距离（间距宽度）（W ）在50〜1000nm的范围内，与水的接触角在130〜180°的范围内。

2. 发明专利

JP2014129480A Case comprising hard coat film, coating liquid for hard coat, silica sol used for coating liquid and method for producing silica sol 有权
标题翻译：包括硬包装薄膜，用于硬质涂层的涂覆液体，用于涂覆液体的二氧化硅溶液和用于生产硅胶的方法
公开(公告)号：JP2014129480A
公开(公告)日：2014-07-10
申请号：JP2012288173
申请日：2012-12-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： FUTAGAMI WATARU , MURAGUCHI MAKOTO , MATSUDA MASAYUKI
IPC分类号： C09C1/28 , B32B27/20 , C09C3/08 , C09D7/12 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a hard coat film capable of achieving both high hardness and prevention of whitening.SOLUTION: A hard coat film formed by using a silica sol containing silica fine particles to which surface a first organosilicon compound having a first functional group is bonded and silica fine particles to which surface a second organosilicon compound having a second functional group is bonded. The first functional group is a functional group which is bonded to a matrix component and the second functional group is a functional group which is not bonded to a matrix component. Further, the molar ratio a/b between the first organosilicon compound and the second organosilicon compound is preferably set in the range of 9:1 to 5:5.
摘要翻译：要解决的问题：提供能够实现高硬度和防止增白的硬涂膜。溶液：使用含有二氧化硅微粒的二氧化硅溶胶形成的硬涂膜，表面具有第一官能团的第一有机硅化合物与表面具有第二官能团的第二有机硅化合物接合的二氧化硅微粒。第一官能团是与基质成分结合的官能团，第二官能团是不与基质成分结合的官能团。此外，第一有机硅化合物和第二有机硅化合物之间的摩尔比a / b优选设定在9:1至5:5的范围内。

3. 发明专利

JP2014058652A Transparent film-forming coating liquid and substrate with transparent film 有权
标题翻译：透明薄膜成型液体和透明薄膜基材
公开(公告)号：JP2014058652A
公开(公告)日：2014-04-03
申请号：JP2012206118
申请日：2012-09-19
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , MURAGUCHI MAKOTO
IPC分类号： C09D201/00 , B32B27/18 , C09C1/00 , C09C1/28 , C09C3/12 , C09D5/24 , C09D7/12 , G02B1/10 , G02B1/11
摘要： PROBLEM TO BE SOLVED: To provide a transparent film-forming coating liquid for forming a transparent film having refraction index which decreases gradually from a lower layer to an upper layer, excellent in light transmissivity, transparency, and having antistatic and antireflection performances.SOLUTION: A transparent film-forming coating liquid contains a surface finishing silica-based fine particle (A), surface finishing chain conductive metal oxide particles (B), a matrix forming component and a solvent. The average particle diameter of the surface finishing silica-based fine particle (A), (D) is in the range of 10 to 200 nm. The surface finishing chain conductive metal oxide particles (B) are chain conductive particles in which 2 to 30 metal oxide particles having an average particle diameter (D) in the range of 5 to 20 nm are connected in a chain, where the metal oxide particles have a volume resistivity value in the range of 10to 10Ω cm. The concentration of the surface finishing silica-based fine particle (A) is in the range of 0.05 to 35 wt.% as a solid content, the concentration of the surface finishing chain conductive metal oxide particles (B) is in the range of 0.025 to 25 wt.% as a solid content, the concentration of the matrix forming component is in the range of 0.1 to 42.5 wt.% as a solid content and the total solid content concentration is in the range of 0.5 to 50 wt.%.
摘要翻译：要解决的问题：提供一种用于形成透明膜的透明成膜涂布液，其具有从下层到上层逐渐降低的折射率，透光性，透明性优异，并且具有抗静电和抗反射性能。解决方案：透明成膜用涂布液含有表面处理用二氧化硅系微粒（A），表面精整链导电性金属氧化物粒子（B），基质形成成分和溶剂。表面处理二氧化硅系微粒（A），（D）的平均粒径在10〜200nm的范围内。表面处理链导电性金属氧化物粒子（B）是链状导电粒子，其中平均粒径（D）在5〜20nm范围内的2〜30个金属氧化物粒子连接在金属氧化物粒子体积电阻率值范围为10〜10＆OHgr; 厘米。表面处理二氧化硅系微粒（A）的浓度为固体成分的0.05〜35重量％，表面精整链导电性金属氧化物粒子（B）的浓度为0.025 至25重量％的固体成分，基质形成成分的浓度为固体成分的0.1〜42.5重量％，总固体成分浓度为0.5〜50重量％。

4. 发明专利

JP2014006443A Manufacturing method for substrate with anti-reflection film and photoelectric cell 有权
标题翻译：具有抗反射膜和光电池的衬底的制造方法
公开(公告)号：JP2014006443A
公开(公告)日：2014-01-16
申请号：JP2012143396
申请日：2012-06-26
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , MURAGUCHI MAKOTO
IPC分类号： G02B1/11 , G02B1/111 , H01G9/20 , H01L31/04 , H01M14/00
CPC分类号： Y02E10/542 , Y02P70/521
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method for a substrate with anti-reflection film with high rigidity and suppressing occurence of such as cracks and scratches.SOLUTION: A manufacturing method for a substrate with an antireflection film is composed of a high refractive index layer formed on the substrate and a low refractive index layer formed on the high refractive index layer includes the steps (a) to (e) below. (a)Dispersion liquid of high refractive index metallic oxide including 1 to 1,000 ppm of basic nitrogen compound is coated on the substrate, with a refractive index in a range from 1.50 to 2.40, (b)removing the dispersion medium at a temperature which is less than boiling point of the basic nitrogen compound, (c)coating dispersion liquid of low refractive index layer forming components, (d)removing the dispersion medium, and then (e) heat treating at 120 to 700°C.
摘要翻译：要解决的问题：提供具有高刚性的抗反射膜的基板的制造方法，并且抑制诸如裂纹和划痕的发生。解决方案：具有抗反射膜的基板的制造方法由高折射率形成在基板上的低折射率层和形成在高折射率层上的低折射率层包括以下步骤（a）至（e）。（a）包含1〜1000ppm碱性氮化合物的高折射率金属氧化物的分散液涂布在基材上，折射率在1.50〜2.40的范围内，（b）在温度为低于碱性氮化合物的沸点，（c）低折射率层形成组分的涂布分散液，（d）除去分散介质，然后（e）在120-700℃进行热处理。

5. 发明专利

JP2013136710A Substrate with transparent coloring film and coating solution for forming transparent coloring film 有权
标题翻译：具有透明彩色膜和涂层溶液的基底，用于形成透明色彩膜
公开(公告)号：JP2013136710A
公开(公告)日：2013-07-11
申请号：JP2011289345
申请日：2011-12-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MATSUDA MASAYUKI , HAKOJIMA YUKO , MURAGUCHI MAKOTO
IPC分类号： C09D201/00 , C09B67/22 , C09B67/44 , C09C3/08 , C09C3/12 , C09D7/12
摘要： PROBLEM TO BE SOLVED: To provide a substrate with a transparent coloring film that excels in adhesion, scratch resistance, and film hardness or the like, and that excels in light resistance, weatherability, contrast, and display performance or the like.SOLUTION: The substrate with a transparent coloring film includes: a substrate; and a transparent coloring film formed on the substrate, wherein the transparent coloring film includes: a matrix component; an inorganic oxide fine particle subjectd to a surface treatment by an organic silicon compound shown by the following formula (1): R-SiX; and a surfactant treatment organic pigment (A) that absorbs light of at least 580-600 nm of a wavelength range. The average particle size of the surfactant treatment organic pigment (A) is in the range of 5-60 nm, the content in the transparent coloring film is in the range of 0.05-3 wt.% as a solid content, the transparent coloring film has an absorption wavelength in the range of 580-600 cm, and the light transmittance (I) is in the range of 50-90%. In the formula (1), R identically or differently denotes a 1-10C unsubstituted or substituted hydrocarbon group; and X denotes a 1-4C alkoxy group, a silanol group, a halogen or hydrogen; and n denotes an integer of 0-3.
摘要翻译：要解决的问题：提供一种具有优异的粘合性，耐刮擦性和膜硬度等的透明着色膜的基材，并且耐光性，耐候性，对比度和显示性能等优异。解决方案：具有透明着色膜的基板包括：基板; 以及形成在所述基板上的透明着色膜，其中所述透明着色膜包括：基体成分; 通过下式（1）表示的有机硅化合物进行表面处理的无机氧化物微粒：R-SiX; 和吸收波长范围至少为580-600nm的光的表面活性剂处理有机颜料（A）。表面活性剂处理有机颜料（A）的平均粒径在5-60nm的范围内，透明着色膜的含量作为固体成分在0.05-3重量％的范围内，透明着色膜具有在580-600cm范围内的吸收波长，透光率（I）在50-90％的范围内。在式（1）中，R相同或不同地表示1-10C未取代或取代的烃基; X表示1-4C烷氧基，硅烷醇基，卤素或氢; n表示0〜3的整数。

6. 发明专利

JP2013133444A Coating material for transparent film formation and substrate with transparent film 有权
标题翻译：透明膜成膜用涂料和透明膜
公开(公告)号：JP2013133444A
公开(公告)日：2013-07-08
申请号：JP2011286073
申请日：2011-12-27
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , HAKOJIMA YUKO , MATSUDA MASAYUKI
IPC分类号： C09D4/00 , B32B23/08 , C09D7/12 , C09D175/14
摘要： PROBLEM TO BE SOLVED: To provide a coating material for transparent film formation used for forming a transparent film, wherein curling (curvature) is controlled even a thin substrate is used, and adhesion to the substrate, hardness, scratch resistance, transparency, etc. are excellent.SOLUTION: The coating material for transparent film formation includes an acrylate resin (A) with a number of functional group of at least 4, an acrylate resin (B) with a number of functional group of 2 and/or 3, an irregular-shaped metal oxide fine particle (C), and an organic solvent (D), wherein a concentration ratio (C)/(C) of the concentration (C) of the acrylate resin (B) to the concentration (C) of the acrylate resin (A) is in the range of 0.05-0.5.
摘要翻译：要解决的问题：为了提供用于形成透明膜的透明成膜用涂料，即使使用薄的基板也能够控制卷曲（曲率），并且与基板的粘合性，硬度，耐刮擦性，透明性等。透明膜形成用涂料包括具有至少4个官能团数的丙烯酸酯树脂（A），具有2个和/或3个官能团数的丙烯酸酯树脂（B），和/或3 不规则形状的金属氧化物微粒（C）和有机溶剂（D），其中丙烯酸酯类树脂（B）的浓度（C）与（C）的浓度（C）的浓度比（C）/（℃）丙烯酸酯树脂（A）在0.05-0.5的范围内。

7. 发明专利

JP2012025793A Transparent film-forming coating liquid and substrate with transparent film 有权
标题翻译：透明薄膜成型液体和透明薄膜基材
公开(公告)号：JP2012025793A
公开(公告)日：2012-02-09
申请号：JP2010162710
申请日：2010-07-20
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , MATSUDA MASAYUKI , HIRAI TOSHIHARU , KOMATSU MICHIO , HAKOJIMA YUKO
IPC分类号： C09D201/00 , B32B27/18 , B32B27/30 , C09D5/24 , C09D7/12 , C09D133/00 , C09D133/14 , G02B1/10 , H01B5/14 , H01B13/00
摘要： PROBLEM TO BE SOLVED: To provide a transparent film-forming coating liquid that forms a substrate with a transparent film having high electrical conductivity even with a small amount of fine particles of an electrically conductive inorganic oxide blended, high transparency, suppressed coloration and interference fringes, and also excellent economical efficiency.SOLUTION: In the transparent film-forming coating liquid, the fine particle of the electrically conductive inorganic oxide, which is surface treated with an organosilicon compound represented by the following formula (1) R-SiX, is non-aggregable and highly dispersed and has concentration of 0.01-6 mass% as a solid content. The transparent film-forming coating liquid includes ketones as a dispersion medium and has concentration of 1-60 mass% of the total solid content and concentration of 0.1-59.4 mass% as a solid content of a matrix-forming component. In formula, Rs are each a 1-10C unsubstituted or substituted hydrocarbon group and may be the same or different from each other; X is a 1-4C alkoxy group, a hydroxy group, halogen, or hydrogen; and n is an integer of 0-3.
摘要翻译：要解决的问题：为了提供一种透明的成膜涂布液，其形成具有导电性高的透明膜的透明膜，即使少量的导电性无机氧化物的微粒混合，高透明度，抑制着色干涉条纹，经济效益也很好。解决方案：在透明成膜涂布液中，用下式（1）表示的有机硅化合物进行表面处理的导电无机氧化物的微粒R n -SiX 4-n 是不可聚集且高度分散且浓度为0.01-6质量％的固体含量。作为分散介质的透明成膜用涂布液，以固体成分的固体成分浓度为总固体成分的1-60质量％，浓度为0.1-59.4质量％。在式中，R 5各自为1-10C未取代或取代的烃基，并且可以相同或不同; X是1-4C烷氧基，羟基，卤素或氢; n为0-3的整数。版权所有（C）2012，JPO＆INPIT

8. 发明专利

JP2011137097A Coating liquid for transparent film formation, substrate with transparent film, and method for producing hydrophobic metal oxide particle 有权
标题翻译：用于透明膜形成的涂料液体，具有透明膜的基材和用于生产疏水性金属氧化物颗粒的方法
公开(公告)号：JP2011137097A
公开(公告)日：2011-07-14
申请号：JP2009298218
申请日：2009-12-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： HAKOJIMA YUKO , MATSUDA MASAYUKI , MURAGUCHI MAKOTO
IPC分类号： C09D4/02 , C09C1/00 , C09C1/28 , C09C1/36 , C09C1/40 , C09C3/12 , C09D7/12 , C09D175/14
摘要： PROBLEM TO BE SOLVED: To provide a coating liquid for transparent film formation comprising hydrophobic metal oxide particles and a hydrophobic matrix-forming component, wherein the hydrophobic metal oxide particles are excellent in dispersibility in a resin and are capable of forming a transparent film excellent in haze, transparency, scratch resistance, strength, alkali resistance, etc., and the resultant transparent film does not cause whitening while excellent in surface flatness; a substrate with a transparent film formed by using the coating liquid for transparent film formation; and a method for producing the hydrophobic metal oxide particles. SOLUTION: In the coating liquid for transparent film formation, the hydrophobic metal oxide particle has a monoalkylsilyl group and a trialkylsilyl group on the surface thereof and an average particle size in the range of 5-300 nm. The content of the monoalkylsilyl group as a solid content (R-SiO 3/2 ) is in the range of 1-50 wt.% of the metal oxide particle, and the content of the trialkylsilyl group as a solid content (R 3 -SiO 1/2 ) is in the range of 3-100 wt.% of the metal oxide particle. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种透明膜形成用涂布液，其包含疏水性金属氧化物粒子和疏水性基质形成成分，其中疏水性金属氧化物粒子在树脂中的分散性优异，能够形成透明性雾度，透明度，耐擦伤性，强度，耐碱性等优异的膜，并且所得到的透明膜不会发生白化，同时表面平坦度优异; 通过使用用于透明成膜的涂布液形成透明膜的基板; 以及疏水性金属氧化物粒子的制造方法。解决方案：在用于透明膜形成的涂布液中，疏水性金属氧化物颗粒在其表面上具有单烷基甲硅烷基和三烷基甲硅烷基，平均粒度在5-300nm的范围内。作为固体成分的单烷基甲硅烷基（R-SiO 3 SB 2/2）的含量在金属氧化物粒子的1-50重量％的范围内，三烷基甲硅烷基的含量为固体含量（R SB 3 -SiO SB 1/2 / SB））在金属氧化物颗粒的3-100重量％的范围内。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2011136490A Base with hard coated film and coating liquid for forming hard coated film 有权
标题翻译：具有硬涂膜和涂层液的基底用于形成硬涂膜
公开(公告)号：JP2011136490A
公开(公告)日：2011-07-14
申请号：JP2009298216
申请日：2009-12-28
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , FUTAGAMI WATARU , MATSUDA MASAYUKI
IPC分类号： B32B3/30 , B32B27/18 , C09D4/02 , C09D7/12 , C09D163/10 , C09D175/14 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a base with a hard coated film showing excellent antiblocking properties (hard coated film being free from mutual adhesion).
SOLUTION: This base with a hard coated film is composed of a base and a hard coated film including a hydrophilic metallic oxide particle (A) and a hyrophobic matrix component (M), formed on the base. In addition, the refractive index (n
PA ) of the hydrophilic metallic oxide particle (A) is within the range of 1.45 to 1.70, and the refractive index (n
M ) of the hydrophobic matrix component (M) is within the range of 1.45 to 1.70. Further, the refractive index difference between the refractive index (n
PA ) and the refractive index (n
M ) is not more than 0.02. At least a part of the hydrophilic metallic oxide particle (A) exists forming a projecting part on the surface of the hard coated film, and the height (H convex) of the projecting part is within the range of 50 nm to 1 μm.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供具有优异的防粘连性（硬涂膜没有相互粘附）的硬涂层的基底。解决方案：具有硬涂层的基底由基底和形成在基底上的包含亲水性金属氧化物颗粒（A）和疏水基质组分（M））的硬涂层组成。此外，亲水性金属氧化物粒子（A）的折射率（n SB SB ）在1.45〜1.70的范围内，折射率（n M SB）的疏水性基质成分（M）在1.45〜1.70的范围内。此外，折射率（n PA ）与折射率（n M ）之间的折射率差不大于0.02。亲水性金属氧化物粒子（A）的至少一部分在硬质被膜的表面上形成突出部，凸部的高度（H凸）在50nm〜1μm的范围内。版权所有（C）2011，JPO＆INPIT

10. 发明专利

JP2010138040A Method for producing chain antimony pentoxide fine particle and substrate with film containing the same 有权
标题翻译：用于生产链状抗氧化剂精细颗粒和含有其的膜的基材的方法
公开(公告)号：JP2010138040A
公开(公告)日：2010-06-24
申请号：JP2008316961
申请日：2008-12-12
申请人： Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社
发明人： MURAGUCHI MAKOTO , MATSUDA MASAYUKI
IPC分类号： C01G30/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a chain antimony pentoxide fine particle dispersion economically and high in the yield, which was not good conventionally. SOLUTION: In the method for producing the chain antimony pentoxide fine particle dispersion, (a) after preparing an antimonic acid (gel) dispersion by treating an aqueous solution of an alkali antimonate having a solid concentration in a range of 0.1-5 wt.% with a cation exchange resin, (c) an acid is added to the antimonic acid (gel) dispersion so that a molar ratio (M A )/(M S ) of a molar number of the acid (M A ) and a molar number of the antimony pentoxide (M S ) may be a range of 0.002-0.5. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种经济地生产链式五氧化二锑细粒分散体的方法，其收率高，这是传统上不好的。解决方案：在制备链状五氧化锑细颗粒分散体的方法中，（a）通过处理固体浓度在0.1-5的范围内的碱金属锑酸盐水溶液制备锑酸（凝胶）分散体后，（c）将酸添加到锑酸（凝胶）分散体中，使得摩尔比（M SB> S / SB）/ 的摩尔数（M A ）和五氧化二锑的摩尔数（M SB SB S）可以是0.002-0.5的范围。版权所有（C）2010，JPO＆INPIT

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