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21. 发明专利

JPH0357900B2 失效
公开(公告)号：JPH0357900B2
公开(公告)日：1991-09-03
申请号：JP17676282
申请日：1982-10-05
申请人： SHIONOGI & CO
发明人： MAKIKADO TOKUO , MURABAYASHI AKIRA , TAWARA KATSUYA , WATANABE YOSHA , TAKAHASHI TOSHIO , KONISHI TAKAO
IPC分类号： A01N43/80 , A61K31/42 , A61P31/04 , A61P31/10 , A61P33/02 , C07D261/14 , C07D413/04 , C07D413/06 , C07D413/12 , C07D521/00

22. 发明专利

JPH03178983A ORGANIC TIN COMPOUND AND ACARICIDE AND INSECTICIDE CONTAINING SAME COMPOUND 失效
公开(公告)号：JPH03178983A
公开(公告)日：1991-08-02
申请号：JP29865390
申请日：1990-11-01
申请人： NITTO KASEI CO LTD , SHIONOGI & CO
发明人： IMAZAKI HIDEYUKI , FUJIKAWA MASAZUMI , OBA KATSUAKI , KUMAYAMA FUSAJI , TAKAHASHI TOSHIO
IPC分类号： A01N55/04 , C07F7/22
摘要： NEW MATERIAL:A compound expressed by formula I [R is alkyl, cycloalkyl or aralkyl: R* is fluorophenyl or trifluoromethylphenyl when R is alkyl and R* is formula II (R is halogen, trifluoromethyl, etc.), dichlorophenyl, etc., when R is cycloalkyl and R* is formula III (R to R are H, halogen, lower alkyl, etc.), 2 thienyl, etc., when R is aralkyl; m is 1 or 2; X is halogen when m is 1 and X is O, S, etc., when m is 2]. EXAMPLE:Dineophylmetatrifluoromethylphenyltin fluoride. USE:An acaricide and insecticide. PREPARATION:A compound expressed by the formula nR*MgY is reacted with a compound expressed by formula IV (Y and Y are Cl, Br or I; n is 1 or 2) at 5-100 deg.C to afford an asymmetric tetraorganotin expressed by formula V, which is then reacted with a halogen.

23. 发明专利

JPS62298575A 7-(PYRIDYLOXY)-2-NAPHTHYLOXYMALONIC ACID DERIVATIVE, PRODUCTION THEREOF AND HERBICIDE CONTAINING SAME 失效
公开(公告)号：JPS62298575A
公开(公告)日：1987-12-25
申请号：JP14429786
申请日：1986-06-19
申请人： SHIONOGI & CO
发明人： HAYASE YOSHIO , MORITA KOICHI , IWAKURA TADAYUKI , IDE KINYA , TAKAHASHI TOSHIO
IPC分类号： A01N43/40 , C07D213/64
摘要： NEW MATERIAL:The 7-(pyridyloxy)-2-naphthyloxymalonic acid derivative of formula I [R and R are H, halogen, trifluoromethyl or nitro; R and R are hydroxy, alkoxy, alkoxyalkoxy, alkylthioalkoxy or group of formula II (R and R are H, alkyl or phenyl)]. EXAMPLE:alpha-[7-(3,5-Dichloro-2-pyridyloxy)-2-naphthyloxy]-alpha-meth ylmalonic acid diethyl ester. USE:Useful as a herbicide. It has excellent selectivity and scarcely gives phytotoxicity to useful plants. PREPARATION:The compound of formula I can be produced e.g. by reacting the compound of formula III with the compound of formula IV (X is halogen) in a solvent such as acetone in the presence of a basic substance at 40-120 deg.C, preferably 60-100 deg.C.

24. 发明专利

JPS6165894A Thiazine phosphonic acid derivative, its preparation and insecticide 失效
标题翻译：噻吩磷酸衍生物，其制备和杀虫剂
公开(公告)号：JPS6165894A
公开(公告)日：1986-04-04
申请号：JP18874484
申请日：1984-09-08
申请人： Nippon Chem Ind Co Ltd:The , Shionogi & Co Ltd
发明人： HAYASE YOSHIO , ICHINARI MITSUHIRO , TAGUCHI JUNJI , ISHIGURO TAKEO , TAKAHASHI TOSHIO
IPC分类号： A01N57/32 , C07D279/06 , C07F9/6544
CPC分类号： C07D279/06 , A01N57/32 , C07F9/6544
摘要： NEW MATERIAL:A compound of formula I (R
1 , R
2 are lower alkoxy, lower alkinyloxy, lower alkylthio, arylthio, lower alkylamino; R
3 , R
4 are H, lower alkyl; R
5 is lower alkyl, lower alkoxy, halogen, trifuoromethyl; X is O, S; m is 0W3).
EXAMPLE: 2-Phenylimino-5,5-dimethyl-3,4,5,6-tetrahydro-2H-1,3-thazine-3-thiol phosphonic acid O-methyl S-sec-butyl ester.
USE: Insecticide.
PREPARATION: The reaction between a compound of formula II and another compound of formula III (Y is eliminating group) is conducted, preferably in an inert solvent in the presence of an acid acceptor such as triethylamine at 20W30°C for 2W8hr.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：新物质：式I化合物（R 1，R 2）为低级烷氧基，低级烷氧基，低级烷硫基，芳硫基，低级烷基氨基; R 3，R 4为H，低级烷基; 低级烷基，低级烷氧基，卤素，三氟甲基; X为O，S; m为0-3）。实施例：2-苯基亚氨基-5,5-二甲基-3,4,5,6-四氢-2H- 1,3-thazine-3-硫醇膦酸O-甲基S-仲丁酯。用途：杀虫剂。制备：式Ⅱ化合物与另一种式III化合物（Y为取代基）的反应优选在惰性溶剂中，在酸受体如三乙胺存在下，于20-30℃进行反应， 8小时

25. 发明专利

JPH01265088A NOVEL QUINOLONE CARBOXYLIC ACID DERIVATIVE AND ANTIBACTERIAL AGENT FOR ANIMAL CONTAINING THE SAME DERIVATIVE AS ACTIVE INGREDIENT 失效
公开(公告)号：JPH01265088A
公开(公告)日：1989-10-23
申请号：JP9237388
申请日：1988-04-14
申请人： SHIONOGI & CO
发明人： HAYASHI KOJI , HAYASE YOSHIO , UEDA KAZUO , TOBITAKA SHIGETADA , TAKAHASHI TOSHIO
IPC分类号： C07D215/56 , A61K31/495 , A61P31/00 , A61P31/04 , C07D401/04
摘要： NEW MATERIAL:A compound expressed by formula I (R -R represent H or lower alkyl) or salt thereof. EXAMPLE:6,8-Dichloro-1-ethyl-7-(3-methyl-1-piperazinyl)-4-oxo-1,4- dihydroquinoline-3-carboxylic acid.hydrochlorate. USE:An antibacterial agent for an animal, especially having an excellent activity as an antimycoplasmic agent. PREPARATION:A compound expressed by formula II (Am represents amino- protecting group) is hydrolyzed by, for example, heating with an aqueous solu tion of an alkali hydroxide such as sodium hydroxide at 60-100 deg.C to afford the compound expressed by formula I wherein group R represents H.

26. 发明专利

JPS63119404A BLENDED HERBICIDE 失效
公开(公告)号：JPS63119404A
公开(公告)日：1988-05-24
申请号：JP26513886
申请日：1986-11-06
申请人： SHIONOGI & CO
发明人： IDE KINYA , KAMIYAMA YOSHITO , HAYASE YOSHIO , MORITA KOICHI , TAKAHASHI TOSHIO
IPC分类号： A01N43/70 , A01N33/18 , A01N47/30
摘要： PURPOSE:To obtain a blended herbicide having increased activity, by combining 2,4-bis(isopropylamino)-6-difluoromethylthio-1,3,5-triazine and a compound selected from linuron, trifluralin and prometryn. CONSTITUTION:A blended herbicide obtained by containing (A) 2,4-bis(isopropylamino)-6-difuoromethylthio-1,3,5-triazine and (B) at least one compound selected from the group of 3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea (linuron), alpha,alpha,alpha-trifluoro-2,6-dinitro-N,N-dipropyl-p-toluidine (trifluralin) and 2,4-bis(isopropylamino)-6-methylthio-1,3,5-triazine (prometryn) at 1:8-8:1, preferably 1:4-4:1 weight ratio.

27. 发明专利

JPS62149689A ORGANIC TIN COMPOUND AND MITICIDAL AND INSECTICIDAL AGENT CONTAINING SAME 失效
公开(公告)号：JPS62149689A
公开(公告)日：1987-07-03
申请号：JP20697486
申请日：1986-09-02
申请人： NITTO KASEI CO LTD , SHIONOGI & CO
发明人： IMAZAKI HIDEYUKI , FUJIKAWA MASAZUMI , OBA KATSUAKI , KUMAYAMA FUSAJI , TAKAHASHI TOSHIO
IPC分类号： A01N55/04 , A01N57/12 , A01N57/14 , C07F7/02 , C07F7/22
摘要： NEW MATERIAL:The compound of formula I [R is alkyl, cycloalkyl, etc.; R* is fluorophenyl, group of formula II (R is halogen, trifluoromethyl or alkoxy), dichlorophenyl, neopentyl, trimethylsilylmethyl, etc.; m is 1 or 2; X is halogen, ester, imidazolyl, etc.]. EXAMPLE:Dineophyl-m-trifluoromethylphenyltin fluoride. USE:A miticidal and insecticidal agent. PREPARATION:The organic fluoride of formula I can be produced e.g. by reacting an organotin halide of formula III (Phe is phenyl; Y is halogen; n is 1 or 2) with a Grignard reagent, reacting the reaction product with halogen and reacting the resultant compound of formula IV (Hal is Cl, Br or I) with KF.

28. 发明专利

JPS6230761A 4,5,6,7-TETRAHYDRO-2H-INDAZOLE DERIVATIVE AND HERBICIDE 失效
公开(公告)号：JPS6230761A
公开(公告)日：1987-02-09
申请号：JP7745286
申请日：1986-04-02
申请人： SHIONOGI & CO
发明人： HAYASE YOSHIO , OTSUKA SHUNICHI , IDE KINYA , TAKAHASHI TOSHIO
IPC分类号： A01N43/56 , C07D231/56
摘要： NEW MATERIAL:The 4,5,6,7-tetrahydfro-2H-indazole derivative of formula (X and Y are halogen). EXAMPLE:3-Chloro-2-(2,4-dichloro-5-difluoromethoxyphenyl)-4,5,6,7-tetr ahydro-2H- indazole. USE:A herbicide exhibiting selective herbicidal effect exclusively to weeds and having remarkably low phytotoxicity to useful crops. PREPARATION:The compound of formula I can be produced e.g. by reacting 3-chloro-2-(4-chloro-2-halo-5-hydroxyphenyl)-4,5,6,7-tetrah-ydro-2H-in dazole of formula II with about 1-10 equivalent of the compound of formula III in a proper solvent at room temperature or under heating.

29. 发明专利

JPS6147471A Triazine derivative and herbicide 失效
标题翻译： TRIAZINE衍生物和除草剂
公开(公告)号：JPS6147471A
公开(公告)日：1986-03-07
申请号：JP17013184
申请日：1984-08-15
申请人： Shionogi & Co Ltd
发明人： HAYASE YOSHIO , MORITA KOICHI , IDE KINYA , TAKAHASHI TOSHIO
IPC分类号： C07D251/26 , A01N43/70 , C07D251/52
CPC分类号： C07D251/52 , A01N43/70
摘要： NEW MATERIAL:The triazine derivative of formula I [R
1 , R
2 , R
3 and R
4 are H, aliphatic hydrocarbon residue, lower alkoxy(lower)alkyl, cyano(lower)alkyl, aryl(lower)alkyl, or R
1 and R
2 , or R
3 and R
4 together form a lower alkylene].
EXAMPLE: 2,4-Bis(ethylamino)-6-difluoromethyl-1,3,5-triazine.
USE: Herbicide effective to the weed in cultivated field such as plowed land, paddy field, orchard, tea plantation, mulberry plantation, disused land, etc., and uncultivated land such as railway, road, lawn, industrial site, river bed, building land, etc. It is effective to the weeds in plowed land and paddy field, such as large crab-grass, green foxtail, barnyard grass, wheat, etc. Harmless to man, animal and bird. It has high safety.
PREPARATION: The compound of formula I can be prepared by reacting the compound of formula II (X is eliminable group) with the compound of formula IIIin a solvent preferably in the presence of a base.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：新物质：式I [R 1，R 2，R 3和R 4]的三嗪衍生物是H，脂族烃残基，低级烷氧基（低级）烷基，氰基（低级）烷基，芳基（低级）烷基，或R 1和R 2，或R 3和R 4一起形成低级亚烷基]。实施例：2,4-双（乙基氨基）-6-二氟甲基-1,3,5-三嗪。用途：除草剂，耕地，水田，果园，茶园，桑树种植园，废弃土地等耕地的除草剂，以及铁路，公路，草坪，工地，河床，建筑物等未耕地土地等，对ab草，绿草，稗草，小麦等耕地，水田等杂草有效。对人，动，禽无害。安全性高。制备：式I化合物可以通过使式II化合物（X是可消除基团）与式III化合物在溶剂中，优选在碱存在下反应来制备。

30. 发明专利

JPS6011904B2 失效
公开(公告)号：JPS6011904B2
公开(公告)日：1985-03-28
申请号：JP7195379
申请日：1979-06-07
申请人： SHIONOGI & CO
发明人： OGATA HIDE , MATSUMOTO HIROSHI , TAWARA KATSUYA , WATANABE YOSHA , TAKAHASHI TOSHIO
IPC分类号： C07D233/58 , A01N43/50 , A61K31/415 , A61P31/04 , A61P31/10 , C07D233/60 , C07D233/61 , C07D333/00 , C07D409/12

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