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    • 8. 发明公开
    • Process for recovering group VI-B metals from spent catalysts
    • Verfahren zurRückgewinnungvon Gruppe-VI-B-Mmetallen aus verbrauchten Katalysatoren
    • EP2410066A2
    • 2012-01-25
    • EP11185542.5
    • 2007-09-14
    • Albemarle Netherlands BV
    • Sitters, Johannes CornelisFree, Harmannus Willem HomanOogjen, Bob Gerardus
    • C22B34/34C22B34/36C22B23/00C22B7/00C22B1/02B01J23/888C10G45/08
    • C22B7/009B01J23/28B01J23/30B01J23/85B01J23/883B01J23/8885B01J37/031B01J38/68C10G49/04C10G2300/706C22B23/026C22B34/345C22B34/365Y02P10/214Y02P10/224Y02P10/23Y02P10/234
    • The invention relates to a process for recovering Group VIB metals from a catalyst, in particular a spent bulk catalyst, comprising one or more Group VIB metals and one or more Group VIII metals. Further, the invention relates to a solid Group VIB metal compound obtainable by the process according to the invention having the general formula H 2 XO 4 , wherein X = W 1-y Mo y , wherein y is between 0 and 1 and to its use in a process for the manufacture of a fresh catalyst. The process comprises the steps of: a) oxidizing the one or more Group VIB metals to one or more Group VIB metal oxides; separating the one or more Group VIB metal oxides from the one or more Group VIII metals; dissolving the one or more Group VIB metal oxides in water to produce an aqueous solution of one or more Group VIB metal oxides; d) precipitating the one or more Group VIB metal oxides from the aqueous solution by adding alkaline earth metal (Group IIa) ions to the aqueous solution; e) optionally filtering and washing the precipitate; and f) transforming the precipitate by adding an acid to form a solid metal compound comprising one or more Group VIB metals.
    • 本发明涉及一种从催化剂中回收VIB族金属的方法,特别是废组分催化剂,其包含一种或多种VIB族金属和一种或多种VIII族金属。 此外,本发明涉及通过根据本发明的方法获得的具有通式H 2 XO 4的固体VIB族金属化合物,其中X = W 1-y Mo y,其中y在0和1之间,并且其使用 在制造新鲜催化剂的过程中。 该方法包括以下步骤:a)将一种或多种VIB族金属氧化成一种或多种VIB族金属氧化物; 从一种或多种VIII族金属分离一种或多种VIB族金属氧化物; 将一种或多种VIB族金属氧化物溶解在水中以产生一种或多种VIB族金属氧化物的水溶液; d)通过向该水溶液中加入碱土金属(IIa)族离子,从水溶液中沉淀出一种或多种VIB族金属氧化物; e)任选地过滤和洗涤沉淀物; 和f)通过加入酸形成包含一种或多种VIB族金属的固体金属化合物来转化沉淀物。