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1. 发明公开

EP4294761A1 SYNTHESIS OF ZEOLITES WITH INTERCONNECTED NANOSHEETS 审中-实审
公开(公告)号：EP4294761A1
公开(公告)日：2023-12-27
申请号：EP22706983.8
申请日：2022-02-16
申请人： University of Houston System
发明人： RIMER, Jeffrey, D. , JAIN, Rishabh
IPC分类号： C01B39/36 , C01B39/38 , C01B37/02 , B01J29/00

2. 发明授权

EP1532075B1 PROCESS FOR THE PREPARATION OF DOPED PENTASIL-TYPE ZEOLITES USING DOPED FAUJASITE SEEDS 有权转让
公开(公告)号：EP1532075B1
公开(公告)日：2019-06-19
申请号：EP03790908.2
申请日：2003-08-19
申请人： Albemarle Netherlands B.V.
发明人： RAO, Rajeev, S.
IPC分类号： C01B39/36 , C01B39/38

3. 发明公开

EP3251738A1 SEPARATION MEMBRANE AND METHOD FOR PRODUCING SAME 审中-公开
标题翻译：分离膜及其制造方法
公开(公告)号：EP3251738A1
公开(公告)日：2017-12-06
申请号：EP16742981.0
申请日：2016-01-26
申请人： Zeon Corporation
发明人： OMORI, Shiori , SUZUKI, Takahiro
IPC分类号： B01D71/02 , B01D69/10 , B01D69/12 , C01B39/36
CPC分类号： B01D71/028 , B01D53/228 , B01D67/0051 , B01D67/0083 , B01D69/105 , B01D69/12 , B01D71/027 , B01D2256/24 , B01D2257/7022 , B01D2323/10 , B01D2323/12 , B01D2323/24 , B01J29/40 , C01B39/36 , C01B39/38 , C01P2002/72 , C07B63/00 , C07C7/13 , C07C7/144
摘要： Provided is a separation membrane that when used in membrane separation of a mixture of a linear hydrocarbon and a branched hydrocarbon and/or cyclic hydrocarbon of equivalent carbon number to the linear hydrocarbon, can efficiently separate the linear hydrocarbon and the branched hydrocarbon and/or cyclic hydrocarbon. The separation membrane includes a porous support and a porous separation layer disposed on the porous support and containing an MFI-type zeolite. In an X-ray diffraction pattern obtained through X-ray diffraction measurement of the porous separation layer, the intensities of diffraction peaks attributed to specific MFI-type zeolite crystal planes satisfy specific relationships.
摘要翻译：本发明提供一种分离膜，其用于将直链状烃与同等碳数的支链状烃和/或环状烃的混合物与直链状烃进行膜分离时，能够有效地分离直链状烃与支链状烃和/或环状烃。分离膜包括多孔载体和设置在多孔载体上并含有MFI型沸石的多孔分离层。在通过多孔分离层的X射线衍射测量获得的X射线衍射图中，归因于特定MFI型沸石晶面的衍射峰强度满足特定关系。

4. 发明公开

EP2723685A2 ZEOLITES AND COMPOSITES INCORPORATING ZEOLITES 审中-公开
标题翻译：沸石和接线沸石
公开(公告)号：EP2723685A2
公开(公告)日：2014-04-30
申请号：EP12753167.1
申请日：2012-06-27
申请人： Jones, Susan , Sermon, Paul
发明人： Jones, Susan , Sermon, Paul
IPC分类号： C01B39/04 , C01B39/14 , C01B39/20 , C01B39/22 , C01B39/24 , C01B39/40 , C01B39/36 , C01B39/38
CPC分类号： C01B39/46 , B01D15/36 , B01D53/02 , B01D53/04 , B01D53/92 , B01D2253/108 , B01D2253/25 , B01D2253/342 , B01J20/18 , B01J20/28042 , B01J39/02 , B01J39/14 , C01B39/04 , C01B39/14 , C01B39/145 , C01B39/20 , C01B39/205 , C01B39/22 , C01B39/24 , C01B39/36 , C01B39/38 , C01B39/40 , C07C7/12 , C07C17/389
摘要： According to the invention there is provided a zeolite having a porous structure produced by forming the zeolite on a porous carbon substrate which has been substantially or completely removed, wherein (i) the zeolite was formed on the substrate at a loading of at least 8% by weight and/or (ii) the zeolite has a reinforcing layer.

5. 发明公开

EP2130586A1 Process for making crystalline metallosilicates 审中-公开
标题翻译：制造结晶金属硅酸盐的方法
公开(公告)号：EP2130586A1
公开(公告)日：2009-12-09
申请号：EP08157770.2
申请日：2008-06-06
申请人： Total Petrochemicals Research Feluy
发明人： BULUT, Metin , JACOBS, Pierre , MINOUX, Delphine , NESTERENKO, Nikolai , DATH, Jean-Pierre , VAN DONK, Sander
IPC分类号： B01J29/40 , C01B39/36 , C10G11/05
CPC分类号： B01J29/40 , C01B39/38 , C10G11/05 , C10G29/205 , C10G47/04 , C10G50/00 , C10G50/02
摘要： The present invention provides a method for preparing a metallosilicate of MFI type, wherein organic templates, seeding techniques, using low aliphatic alcohols miscible with water or homogeneous starting solutions are not required.
The present invention relates to a process for making a crystalline metallosilicate with high Si/Metal ratio comprising:
a) providing an aqueous medium comprising OH - anions and a metal source,
b) providing an aqueous medium comprising an inorganic water insoluble source of silicon,
c) optionally providing a non aqueous liquid medium comprising optionally an organic source of silica,
d) mixing the medium a), b) and the optional c) at conditions effective to crystallize the desired metallosilicate,
e) recovering the desired metallosilicate,

wherein in the mixture a)+b)+c), before crystallization,
the ratio Si org/Si inorganic is
the molar ratio OH - /SiO 2 is at least 0.3, preferably from 0.3 to 0.6 more preferably from 0.33 to 0.6 .
In another embodiment steps e), f) and g) are inserted before recovering the desired metallosilicate :
e) cooling down the reaction mixture a)+b)+c) to about room temperature,
f) decreasing the pH of the reaction mixture by at least 0.1 preferably by 0.3 to 4, more preferably by 0.5 to 3,
g) subjecting the resulting mixture of step f) at conditions effective to continue the crystallization of the desired metallosilicate.
摘要翻译：本发明提供了制备MFI型金属硅酸盐的方法，其中不需要使用可与水混溶的低级脂族醇或均相起始溶液的有机模板，接种技术。本发明涉及制备具有高Si /金属比率的结晶金属硅酸盐的方法，其包括：a）提供包含OH-阴离子和金属源的水性介质，b）提供包含无机水不溶性硅源的水性介质， c）任选地提供包含任选有机二氧化硅源的非水性液体介质，d）在有效使所需金属硅酸盐结晶的条件下混合介质a），b）和任选c），e）回收所需金属硅酸盐，其中在在结晶之前，混合物a）+ b）+ c）的比例Si org / Si无机物<0.3，有利地<0.2且优选0，OH- / SiO 2的摩尔比至少为0.3，优选为0.3至0.6以上优选从0.33至0.6。在另一个实施方案中，在回收所需的金属硅酸盐之前插入步骤e），f）和g）：e）将反应混合物a）+ b）+ c）冷却至室温，f）通过以下方式降低反应混合物的pH： g）至少0.1，优选0.3至4，更优选0.5至3，g）使得到的步骤f）的混合物在有效继续期望的金属硅酸盐结晶的条件下进行。

6. 发明公开

EP2130584A1 Process for making crystalline metallosilicates 审中-公开
标题翻译： Herstellungsverfahrenfürkristalline Metallsilikate
公开(公告)号：EP2130584A1
公开(公告)日：2009-12-09
申请号：EP08157762.9
申请日：2008-06-06
申请人： Total Petrochemicals Research Feluy
发明人： BULUT, Metin , JACOBS, Pierre , MINOUX, Delphine , NESTERENKO, Nikolai , DATH, Jean-Pierre , VAN DONK, Sander
IPC分类号： B01J29/40 , C01B39/40 , C10G11/05 , C01B39/36
CPC分类号： B01J29/40 , B01J29/06 , B01J29/60 , B01J29/65 , C01B39/02 , C01B39/38 , C01B39/40 , C01B39/44 , C01B39/445 , C01B39/46 , C01B39/48 , C07C2/66 , C07C2/861 , C07C2/864 , C07C5/2737 , C07C6/123 , C07C6/126 , C07C29/10 , C07C37/14 , C07C37/16 , C07C41/06 , C07C2529/06 , C07C2529/86 , C07C2529/87 , C07C2529/88 , C07C2529/89 , C10G11/04 , C10G29/205 , C10G49/02 , C12C11/02 , Y02P20/52 , C07C15/107 , C07C15/085 , C07C15/073 , C07C15/24 , C07C31/125 , C07C39/06 , C07C43/046 , C07C31/04 , C07C31/08
摘要： The present invention relates to a process for making a crystalline metallosilicate composition comprising crystallites having an inner part (the core) and an outer part (the outer layer or shell) such that :
the ratio Si/metal is higher in the outer part than in the inner part,
the crystallites have a continuous distribution of metal and silicon over the crystalline cross-section,
said process comprising :
a) providing an aqueous medium comprising OH - anions and a metal source,
b) providing an aqueous medium comprising an inorganic source of silicon and optionally a templating agent,
c) optionally providing a non aqueous liquid medium comprising optionally an organic source of silica,
d) mixing the medium a), b) and the optional c) at conditions effective to crystallyze the desired metallosilicate,
e) recovering the desired metallosilicate,

wherein in the mixture a)+b)+c), before crystallization,
the ratio Si org/Si inorganic is
the molar ratio OH - /SiO 2 is at least 0.3, preferably from 0.3 to 0.6 .
摘要翻译：本发明涉及一种制备结晶金属硅酸盐组合物的方法，其包含具有内部（芯）和外部（外层或外壳）的微晶，使得外部部分的Si /金属比例高于所述内部部分，所述微晶在结晶横截面上具有金属和硅的连续分布，所述方法包括：a）提供包含OH - 阴离子和金属源的水性介质，b）提供包含无机源的水性介质的硅和任选的模板剂，c）任选地提供包含任选的二氧化硅有机源的非水性液体介质，d）在有效地使所需的金属硅酸盐水解的条件下，将介质a），b）和任选的c））回收所需的金属硅酸盐，其中在混合物a）+ b）+ c）中，在结晶之前，Si org / Si无机物的比例<0.3，有利地<0.2并且优选为0， r比率的OH - / SiO 2为0.3以上，优选为0.3〜0.6。

7. 发明公开

EP1532076A1 PROCESS FOR THE PREPARATION OF DOPED PENTASIL-TYPE ZEOLITE USING DOPED SEEDS 有权转让
标题翻译：用于生产pentasyl型掺杂沸石使用掺杂GERMS
公开(公告)号：EP1532076A1
公开(公告)日：2005-05-25
申请号：EP03790910.8
申请日：2003-08-19
申请人： Albemarle Netherlands B.V.
发明人： BRADY, Mike , LAHEIJ, Erik, Jeroen , O'CONNOR, Paul , STAMIRES, Dennis
IPC分类号： C01B39/36 , C01B39/38
CPC分类号： B01J29/405 , C01B39/36 , C01B39/38 , C01B39/40
摘要： The present invention relates to a process for the preparation of doped pentasiltype zeolite, which process comprises the steps of: a) preparing an aqueous precursor mixture from a silicon source, an aluminium source, and doped non-zeolitic seeds, and b) thermally treating the precursor mixture to form a doped pentasil-type zeolite. The term "non-zeolitic seeds" includes seeds made from materials selected from the group consisting of (i) X-ray amorphous materials, (ii) milled crystalline materials, such as milled zeolites, that have a relative crystallinity of not more than 75%, and (iii) crystalline materials other than zeolites, such as clays (e,g, bentonite and kaolin) and (low) crystalline aluminas.

8. 发明公开

EP1152887A4 ZEOLITE MEMBRANE AND A PROCESS FOR THE PRODUCTION THEREOF 审中-公开
标题翻译：沸石和方法及其
公开(公告)号：EP1152887A4
公开(公告)日：2003-04-02
申请号：EP99967741
申请日：1999-12-29
申请人： CORNING INC
发明人： PIEROTTI KIM D , ST JULIEN DELL J
IPC分类号： B01D53/22 , B01D69/10 , B01D71/02 , B01J20/18 , B01J20/28 , B01J20/30 , B01J35/06 , B01J37/02 , C01B39/02 , C01B39/22 , C01B39/24 , C01B39/36 , C01B39/38 , C01B39/52 , C04B41/50 , C04B41/85 , B32B3/26 , B01J29/00
CPC分类号： B01J20/28033 , B01D63/066 , B01D67/0051 , B01D71/028 , B01D2325/04 , B01D2325/10 , B01D2325/12 , B01D2325/48 , B01J20/18 , B01J20/2803 , B01J20/28042 , B01J20/28069 , B01J20/28085 , B01J35/065 , B01J37/0246 , B01J2229/64 , C04B41/009 , C04B41/5024 , C04B41/85 , C04B2111/00801 , C04B41/0072 , C04B41/4521 , C04B41/4535 , C04B41/4556 , C04B35/10 , C04B35/195 , C04B35/185 , C04B38/0006
摘要： The present invention is directed at a supported zeolite structure comprising substantially-sintered monolithic porous ceramic substrate having coated thereon a uniformly thin, essentially continuous zeolite crystal layer covering at least one surface and associated pores of the porous ceramic material. The zeolite crystal layer is comprised of a single layer or zeolite crystals and is free of any growth enhancing, selectivity enhancing, or reparation layer and exhibits an oriented structure whereby the crystals exhibit a substantially columnar cross-section. Preferably, the porous ceramic substrate support comprises, on an analyzed oxide basis, 10-90 %, by weight alumina and exhibits a crystal phase assemblage selected from the group consisting of cordierite, mullite, alumina, and/or mixtures thereof. A method for forming a zeolite membrane disclosed herein is also provided. The method generally comprises the steps of providing porous ceramic substrate and hydrothermally treating the substrate with an aqueous solution comprising sodium oxide or sodium hydroxide and having an alumina concentration of less than about 0.01 %. The pH of the solution and the treatment time and temperature are such that these reaction conditions result in partial dissolution of the alumina in the substrate and essentially no nucleation in the solution thereby resulting in growth of the zeolite which is essentially continuous over the porous support.

9. 发明公开

EP1118378A1 TRANSMITTABLE FILM, ELECTROLYTIC CAPACITOR, METHOD FOR PREPARING ZEOLITE FILM, MFI TYPE ZEOLITE FILM, AND METHOD FOR SEPARATION 审中-公开
标题翻译：传染性FILM，电解催化剂的方法，用于生产薄膜的沸石，MFI沸石和分离VEFFAHREN
公开(公告)号：EP1118378A1
公开(公告)日：2001-07-25
申请号：EP99940533.5
申请日：1999-08-27
申请人： TORAY INDUSTRIES, INC.
发明人： YOSHIKAWA, Masahito , OZEKI, Yuji , TANIGUCHI, Takashi
IPC分类号： B01D71/02 , C01B39/36 , H01G9/12
CPC分类号： C01B13/0251 , B01D53/228 , B01D65/10 , B01D67/0051 , B01D71/028 , B01D2323/04 , C01B3/503 , H01G9/12
摘要： Atransmittable film having a functional layer which preferably comprises (1) a zeolite and/or an analogue thereto, (2) an inorganic oxide particle, (3) a silicone rubber, a silicone resin or a silicone oil, (4) an organic polymer compound, or (5) carbon, and a porous support; and an electrolytic capacitor having the film. This film exhibits high transmissivity for hydrogen and is much poorly transmittable for steam, gaseous ethylene glycol and gaseous ammonia, and has excellent resistance to heat and chemicals. Also provided are a method for preparing a zeolite film which is suitably used for the above functional layer, an MFI type zeolite film which is an embodiment of the zeolite film, and a method for separating at least one type of molecule from a gaseous or liquid mixture consisting of at least two types of molecule which comprises transmitting the at least one molecule through the aforementioned transmittable film or a MFI type zeolite film.
摘要翻译：具有功能层Atransmittable膜其优选包括（1）沸石和/或成模拟于此，（2）无机氧化物颗粒，（3）硅橡胶，有机硅树脂或硅油，（4）有机聚合物化合物，或（5）的碳，和多孔质支持; 和电解电容器具有膜。这个电影表现出高的透射率为氢并且是非常差的可传输于蒸汽，气态乙烯乙二醇和气态氨，并具有优良的耐热性和化学品。这样提供了用于制备沸石的方法薄膜的所有其适合用于上述功能层MFI型沸石膜的所有这对沸石电影的实施方式，以及用于从气体或液体中分离至少一种类型的分子的方法混合物由至少两种类型的分子，其包含通过上述透射电影或MFI型沸石电影传送所述至少一种分子的。

10. 发明公开

EP0968131A1 VERFAHREN ZUR HERSTELLUNG VON ZEOLITHEN MIT EINEM HOHEN Si/Al-ATOMVERHÄLTNIS 失效
标题翻译：用于生产沸石具有高的Si / Al原子比
公开(公告)号：EP0968131A1
公开(公告)日：2000-01-05
申请号：EP98912366.6
申请日：1998-02-21
申请人： SÜD-CHEMIE AG
发明人： UNGER, Klaus, K. , HAHN, Andreas, F., K.
IPC分类号： C01B39/36 , C01B39/38 , C01B39/40
CPC分类号： C01B39/36
摘要： A process is disclosed for producing zeolites with a high Si/Al atomic ratio from 40 to , in particular zeolites from the pentasile group, by reacting amorphous polysilicic acids with an aluminium ion source and optionally a template at temperatures of up to 100 °C. The process is characterised in that ammonium hydroxide and/or an alkali silicate are added to the reaction solution. The zeolites obtained by this process have (a) an average particle size from about 0.3 to 0.6 νm, 90 % of the particles lying in the range from about 0.1 to 0.7 νm; and (b) more than 95 % crystallinity.

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