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    • 3. 发明公开
    • METHOD FOR MANUFACTURING MOLDED MATERIAL, MOLDED MATERIAL, WAVEFRONT CONTROL ELEMENT, AND DIFFRACTION GRATING
    • 制造模制材料的方法,模制材料,波前控制元件和衍射光栅
    • EP3312300A1
    • 2018-04-25
    • EP16814288.3
    • 2016-06-17
    • Tohoku University
    • Kato HidemiYashiro Wataru
    • C22C45/00C22C5/04C22C28/00C22C30/02C22F1/10C22F1/14C22F1/16G01N23/20C22F1/00
    • Provided is process for producing molded material by which a metallic glass material is molded at a lower viscosity coefficient in a relatively short period of time into the material with a structure having a precisely controlled shape and measuring not more than tens of micrometers; and also provided are the molded material, a wavefront control element and a diffraction grating. A heating step is performed to heat a supercooled metallic glass material or solid metallic glass material, at a temperature increase rate of 0.5 K/s or more, to a temperature which is equal to or higher than a temperature at which a supercooled liquid of the metallic glass material starts to crystallize. A molding step is performed, in the heating step, to subject the metallic glass material to transfer molding, for a period of time starting with the arrival at the glass transition temperature of the metallic glass material and lasting before the completion of the crystallization process of the supercooled liquid of the metallic glass material. For the production of the wavefront control element, the use of a concave-convex mold having periodic concavity-convexity is preferred. For the production of a G 2 diffraction grating for a neutron Talbot interferometer, the use of a Gd-based, Sm-based, Eu-based or Dy-based metallic glass material is preferred.
    • 本发明提供一种用于制造成型材料的方法,通过该成型材料,金属玻璃材料以较低的粘度系数在较短的时间内成型为具有精确控制的形状并测量为不大于几十微米的结构的材料; 还提供了模制材料,波前控制元件和衍射光栅。 进行加热步骤以将过冷金属玻璃材料或固体金属玻璃材料以0.5K / s或更高的升温速率加热到等于或高于过冷却液体的过冷液体温度 金属玻璃材料开始结晶。 在加热步骤中,进行成型步骤以使金属玻璃材料经过一段时间的传递模塑,所述时间段从金属玻璃材料的玻璃化转变温度开始并且在完成结晶过程之前持续 金属玻璃材料的过冷液体。 为了制造波前控制元件,优选使用具有周期性凹凸的凹凸模具。 为了制造用于中子Talbot干涉仪的G2衍射光栅,优选使用Gd基,Sm基,Eu基或Dy基金属玻璃材料。
    • 5. 发明公开
    • FABRICATION METHOD OF STRIPS AND SHEETS MADE OF ZN-CU-TI ALLOYS DESIGNED FOR BUILDING INDUSTRY
    • 用于建筑业的ZN-CU-TI合金制成的条带和片材的制造方法
    • EP3187616A1
    • 2017-07-05
    • EP15460143.9
    • 2015-12-31
    • ZM Silesia S.A.
    • Napiora, TomaszPawlicha, StanislawKnych, TadeuszMamala, AndrzejOsuch, PiotrWalkowicz, MonikaGradkiewicz, LukaszSokol, Radoslaw
    • C22F1/16C22C18/02
    • C22F1/165
    • A fabrication method of flat-rolled products designed for building industry, made of Zn-Cu-Ti alloy with a chemical composition in accordance with EN-988 standard, composed of at least two basic steps - continuous casting process of metal strip and non-integrated rolling process of finished product in form of sheets, wherein after casting step the metal strip with a thickness from 4 mm to 16 mm and width from 500 mm to 2000 mm is heated up to a temperature ranging from 240°C to 270°C before starting the rolling operation and is being rolled in at least five roll passes until the finished product is obtained. The reduction ratios in the last four roll passes of the rolling process are > 40 % and
      The Zn-Cu-Ti contains from 0,08 wt. % to 0,24 wt. % Cu, from 0,06 wt. % to 0,12 wt. % Ti, not more than 0,015 wt. % Al and rest Zn and tramp elements such as Cd, Fe, Pb and Sn.
      The finished product is susceptible to plastic strain in low temperatures ≥ +10 °C.
    • 一种用于建筑行业的平轧产品的制造方法,由化学成分符合EN-988标准的Zn-Cu-Ti合金制成,至少由两个基本步骤组成 - 连续铸造金属带材和非金属带材, 板材成品的整体轧制工艺,其中,在铸造步骤之后,将厚度为4mm至16mm且宽度为500mm至2000mm的金属带材加热至240℃至270℃的温度 在开始轧制操作之前并且在至少五次轧制道次中进行轧制直到获得最终产品。 轧制过程的最后四个轧制道次中的压下率大于40%且小于50%,并且轧制率不小于100mm / min。 最后一次轧制后的板材温度至少为100°C(≥100°C)。 Zn-Cu-Ti含有0.08wt。 %至0.24wt。 %Cu,0.06wt。 %至0.12wt。 %Ti,不超过0.015wt。 %Al,剩余的Zn和不定形元素如Cd,Fe,Pb和Sn。 成品在≥+ 10°C的低温下易受塑性应变影响。